Patent classifications
G01R33/448
DETERMINING GRAIN DENSITY OF A ROCK SAMPLE
Techniques for determining grain density of a rock sample include identifying an untreated rock sample that includes a solid matrix and a fluid entrained within the solid matrix; measuring, using a gas porosimeter, a grain density of the untreated rock sample; measuring, using nuclear magnetic resonance (NMR), a volume of the fluid entrained within the solid matrix; and determining, based on the measured grain density of the untreated rock sample and the measured volume of the fluid, a grain density of the solid matrix of the untreated rock sample.
Fast measurement and interpretation of downhole multi-dimensional measurement
Downhole properties of a geological formation may be determined using nuclear magnetic resonance (NMR) measurements obtained by a moving tool. To do so, an interpretation of the NMR data obtained by the moving data may take into account a moving model, characterization, or calibration of the downhole NMR tool. Additionally or alternatively, a partial interpretation mask may exclude interpretation of certain areas of data (e.g., T1-T2 data points or diffusion-T2 data points) that are expected to be less likely to describe downhole materials of interest.
METHOD FOR MEASURING THE SPATIAL WATER PERMEABILITY PROFILE OF POROUS MEDIA BY USING NON-DESTRUCTIVE NUCLEAR MAGNETIC RESONANCE TECHNIQUE
A method includes deriving spatial permeability along a core axis by saturating the rock with an aqueous solution, performing T.sub.2 NMR on the saturated rock to detect spatial NMR data along the core axis, desaturating the rock, performing T.sub.2 NMR on the desaturated rock to detect spatial NMR data along the core axis, determining the spatial cutoff data for the saturated and desaturated rock along the core axis, and analyzing the spatial NMR data. The method further includes deriving spatial permeability along a second core axis by additionally performing T.sub.2 NMR on the saturated rock to detect spatial NMR data along a second core axis, performing T.sub.2 NMR on the desaturated rock to detect spatial NMR data along a second core axis, and determining the spatial cutoff data for the saturated and desaturated rock along the second core axis.
IN SITU, REAL-TIME IN-LINE DETECTION OF FILLING ERRORS IN PHARMACEUTICAL PRODUCT MANUFACTURING USING WATER PROTON NMR
A method of using the transverse relaxation rate (R.sub.2) of solvent NMR signal to detect filling errors of an alum-containing product in real-time in-line during manufacturing, for example during a fill-finish unit operation. This technique can be used for quality control in vaccine manufacturing to ensure the delivery of the correct concentration of alum-containing product to the product container such as a vial or pre-filled syringe.
METHOD AND SYSTEM FOR DETERMINING GEOLOGICAL MODELS USING SPATIAL PROPERTIES BASED ON NUCLEAR MAGNETIC RESONANCE DATA
A method may include obtaining first nuclear magnetic resonance (NMR) data for a saturated core sample regarding a geological region of interest. The method may further include determining, using the first NMR data, spatial porosity data based on the saturated core sample. The spatial porosity data may describe various porosity values as a function of a sampling position of the saturated core sample. The method may further include obtaining second NMR data for a desaturated core sample regarding the geological region of interest. The method may further include determining, using the second NMR data, spatial permeability data based on the desaturated core sample. The method may further include determining a geological model for the geological region of interest using the spatial porosity data, the spatial permeability data, and a fitting process.
Characterizing Effects Of CO2 Chemical Reaction With Rock Minerals During Carbon Capture And Sequestration
A method for measuring a carbon capture and sequestration site. The method may comprise acquiring one or more core samples from a carbon capture and sequestration site, performing a nuclear magnetic resonance (NMR) measurement on the one or more core samples to form a first NMR measurementperforming a surface roughness measurement on the one or more core samples to determine a Rs,.sub.before wherein the Rs,.sub.before is a surface roughness of the one or more core samples before the one or more core samples are aged in a cell, and determining at least one property of the one or more core samples from at least the first NMR measurement and the Rs,.sub.before.
SYSTEMS AND METHODS FOR DETERMINING SURFACTANT IMPACT ON RESERVOIR WETTABILITY
Implementations described and claimed herein provide systems and methods for determining surfactant impact on reservoir wettability. In one implementation, a nuclear magnetic resonance T1 measurement of a sample is obtained before surfactant imbibition is applied to the sample, and a second nuclear magnetic T2 measurement of the sample is made after forced imbibition of the surfactant. Moreover, another nuclear magnetic resonance T1 measurement (e.g., omitting surfactant imbibition) can be obtained simultaneously with the nuclear magnetic resonance T2 measurement using a twin core sample. The nuclear magnetic resonance T1 measurement and the nuclear magnetic resonance T2 measurement are captured under simulated reservoir conditions. A fluid typing map is generated using the nuclear magnetic resonance T1 measurement and the nuclear magnetic resonance T2 measurement. An impact of the surfactant on fluid producibility is determined based on the fluid typing map.
NUCLEAR MAGNETIC RESONANCE SYSTEMS AND METHODS FOR NONINVASIVE AND IN-VIVO MEASUREMENTS USING A UNILATERAL MAGNET
An apparatus for non-invasive evaluations and in-vivo diagnostics includes an open magnet, an RF antenna, and an NMR analytics logical circuit communicatively coupled to the RF antenna, wherein the open magnet is shaped to generate a static magnetic field that extends unilaterally into an object or internal organ of a subject when the open magnet is positioned against or in proximity to the object or subject, the static and RF magnetic fields shaped to generate a sensitive volume within a target region. The RF antenna or antenna array is configured to transmit RF pulses into the target region of the object or internal organ and receive sets of NMR signals generated by hydrogen or other elements, and the NMR analytics logical circuit is configured to obtain and analyze sets of NMR signals.
Measuring Gas in Shale Reservoirs
Methods for determining a volume of stored gas within a rock sample includes loading a rock sample into an overburden cell. A hydrocarbon gas at a gas pressure is applied to the rock sample and a confining fluid at a confining pressure is applied to the overburden cell. The confining pressure and the gas pressure are increased until a first pressure and temperature condition is met. With the rock sample maintained at the first temperature and pressure condition, a nuclear magnetic resonance spectrometer is used to scan the rock sample and measure a hydrocarbon gas volume within the rock sample. This measured hydrocarbon gas volume is then corrected using a Real Gas Index to determine the volume of stored gas within the rock sample.
Methods for quantitative characterization of asphaltenes in solutions using two-dimensional low-field NMR measurement
A method for determining the concentration of asphaltenes in a solution is described. A model is first established for estimating the concentration of asphaltenes in a solution based on multiple samples of solutions of asphaltenes in the solvent in which the concentrations are known. The multiple samples have varying concentrations of asphaltenes. The diffusivity and relaxation time are measured for each sample using two-dimensional NMR. The ratio of diffusivity to relaxation time for each sample is then calculated. A linear equation is determined to fit the relationship between the ratio of diffusivity to relaxation time and the asphaltene concentration by weight for the multiple samples, thus creating the model. For a given solution sample for which the concentration of asphaltenes is desired to be determined, diffusivity and relaxation time are determined using two-dimensional NMR, and the ratio of diffusivity to relaxation time is calculated. This ratio is then used with the model, so that the linear equation can be solved for the asphaltene concentration in the given solution sample.