To cool a digestion vessel (2) of a calorimeter (3) by means of a liquid coolant, a recess (4) over which the digestion vessel (2) is invented during the cooling possess and which has one or more ports (10) for a cooling liquid by means of which the inside of the digestion vessel (2) is wetted in such a way that the coolant runs down over part or the entireties of this inside of the digestion vessel (2) so as to remove the heat thereof is provided.

Analysis instruments and sensors, particularly micro-electro mechanical sensor (MEMS) devices, for molecular analysis of chemicals and other materials, including, for example, polymers, drugs, nanomaterials, biological samples including proteins, and environmental samples including water suspected of contamination, and the like in vapor, liquid, and/or solid form.

A method for testing a heat transfer fluid based on a charged wire test (CWT) includes applying and measuring discharge current through a test circuit formed when a cathode and an anode are at least partially immersed in the heat transfer fluid in a container and a voltmeter coupled to the cathode and the anode is turned on during the CWT. The method includes measuring temperature of the heat transfer fluid during the CWT, determining a current profile based on the measured discharge current, and determining a temperature profile based on the measured temperature. The method includes determining a pass/fail status and/or a rank status of the heat transfer fluid based on pass/fail criteria based on the current profile and the temperature profile during an entire duration of the CWT.

Analysis instruments and sensors, particularly micro-electro mechanical sensor (MEMS) devices, for molecular analysis of chemicals and other materials, including, for example, polymers, drugs, nanomaterials, biological samples including proteins, and environmental samples including water suspected of contamination, and the like in vapor, liquid, and/or solid form.

An apparatus and method for initiating thermochemical events in an adiabatic reaction calorimeter are provided. The apparatus and method may be used in safety research of lithium battery and reactive chemical thermal runaways. The apparatus comprises a motor-driven conductive heating element in thermal contact with the outer surface of the reaction in the sample container for heat transfer during heating ramp. The heating element is heated and coupled to the sample container to initiate thermal runaway and decoupled once thermal runaway is initiated, which is much faster than many existing slow heating methods used to initiate thermal runaway. Alternatively, when the heating element is kept attached until the completion of the thermal event, a power-compensation DSC curve is resulted.

A thermal testing tool comprises a base, a back plate, a heating assembly and a first sealing member. The back plate is arranged on the base and, together with the base, encloses a first accommodating recess and a second accommodating recess. The second accommodating recess is located at a periphery of the first accommodating recess. The heating assembly comprises a heating sheet. At least a portion of the heating sheet is located in the first accommodating recess. The first sealing member is arranged in the second accommodating recess and located at a periphery of at least a portion of the heating sheet.

Various embodiments of the teachings herein include a method of ascertaining a progression of curing on application of an electrical insulation layer of an insulation material in a liquid state to an electrical product. An example includes: providing a temperature progression that the electrical product undergoes in the course of application and curing of the insulation layer; providing a reaction model of the insulation material to give a progression of curing of the insulation material on the basis of a temperature progression as input parameter and modeled on the basis of measured enthalpies of reaction of the insulation material at two different heating rates; and ascertaining the progression of curing using the reaction model with the temperature progression.

Provided herein is technology relating to calorimetry and particularly, but not exclusively, to apparatuses, methods, and systems for making high-resolution thermodynamic measurements of reactions between gas phase reactants and nanomaterials. For example, the technology can provide thermodynamic measurements with a high heat flow resolution and long term stability at a wide range of temperatures and reaction pressures. The technology is used, for example, to study the thermodynamics of surface reactions and phase transformations in nanomaterials.

An apparatus and method for initiating thermochemical events in an adiabatic reaction calorimeter are provided. The apparatus and method may be used in safety research of lithium battery and reactive chemical thermal runaways. The apparatus comprises a motor-driven conductive heating element in thermal contact with the outer surface of the reaction in the sample container for heat transfer during heating ramp. The heating element is heated and coupled to the sample container to initiate thermal runaway and transitions to a non-heating configuration once thermal runaway is initiated, which is much faster than many existing slow heating methods used to initiate thermal runaway.