The invention relates to a method for preparing a sample for chromatographic separation processes, in which a sample vessel (1) is partially filled with a substance to be examined and is closed, the substance to be examined is subjected to a thermo-chemical reaction in which at least one sample component is converted into another substance, and in which by means of a removing device samples are removed from the sample vessel (1) for analytical examination, characterized in that the sample vessel (1) forms a cavity, into which the substance to be examined is introduced as a core and a heating section for indirect heat transfer is applied along the filling of substance to be examined.

The invention relates to a method for preparing a sample for chromatographic separation processes, in which a sample vessel (1) is partially filled with a substance to be examined and is closed, the substance to be examined is subjected to a thermo-chemical reaction in which at least one sample component is converted into another substance, and in which by means of a removing device samples are removed from the sample vessel (1) for analytical examination, characterized in that the sample vessel (1) forms a cavity, into which the substance to be examined is introduced as a core and a heating section for indirect heat transfer is applied along the filling of substance to be examined.

A sample injector for chromatography 10 where air or moisture can be prevented from getting mixed in when a sample is injected is provided with a syringe 11, a syringe drive unit 13, a turret 12 in which sample vials 4 are placed, a turret drive unit 14, and a control unit 30 that controls the syringe and turret drive units 13 and 14. The configuration includes a housing 15 having a gas introduction port 15a and a gas discharge port 15b that communicate with the inner space, where the syringe 11 sucks a sample from a sample vial 4, the sucked sample is injected into the sample vaporizing chamber 23 in a chromatograph 20, and a predetermined gas is introduced through the gas introduction port 15a, and at the same time, a predetermined gas is discharged through the gas discharge port 15b when a sample is analyzed.

A sample injector for chromatography 10 where air or moisture can be prevented from getting mixed in when a sample is injected is provided with a syringe 11, a syringe drive unit 13, a turret 12 in which sample vials 4 are placed, a turret drive unit 14, and a control unit 30 that controls the syringe and turret drive units 13 and 14. The configuration includes a housing 15 having a gas introduction port 15a and a gas discharge port 15b that communicate with the inner space, where the syringe 11 sucks a sample from a sample vial 4, the sucked sample is injected into the sample vaporizing chamber 23 in a chromatograph 20, and a predetermined gas is introduced through the gas introduction port 15a, and at the same time, a predetermined gas is discharged through the gas discharge port 15b when a sample is analyzed.

A device for a gas chromatograph system includes an injector, a conduit assembly, a flow restrictor, and a pressure controller. The injector is connected to a carrier gas source and an auxiliary gas source. The conduit assembly surrounds the input end of an analytical column. A carrier gas is supplied at a constant pressure through a flow restrictor to the injector. A pressure controller is configured to control the pressure of an auxiliary gas supplied to the injector from the auxiliary source. The pressure controller is configured to operate in a first mode to provide a first auxiliary gas pressure sufficient to force a flow of the auxiliary gas and a sample onto the analytical column during an inject phase and to operate in a second mode to provide a second auxiliary gas pressure below a threshold necessary to flow auxiliary gas into the analytical column during a resolving phase.

A device for a gas chromatograph system includes an injector, a conduit assembly, a flow restrictor, and a pressure controller. The injector is connected to a carrier gas source and an auxiliary gas source. The conduit assembly surrounds the input end of an analytical column. A carrier gas is supplied at a constant pressure through a flow restrictor to the injector. A pressure controller is configured to control the pressure of an auxiliary gas supplied to the injector from the auxiliary source. The pressure controller is configured to operate in a first mode to provide a first auxiliary gas pressure sufficient to force a flow of the auxiliary gas and a sample onto the analytical column during an inject phase and to operate in a second mode to provide a second auxiliary gas pressure below a threshold necessary to flow auxiliary gas into the analytical column during a resolving phase.

A sample injector for an analytical device includes a needle seat configured to receive a needle for injecting a sample into an injector path. The needle seat is mounted in a floating manner so that the orientation of the needle seat is aligned automatically with respect to the orientation of the approaching needle. The sample injector may be provided in an analytical device such as a chromatographic device.

A configurable injector for injecting a fluidic sample in a separation path of a sample separation apparatus includes a sample accommodation volume for accommodating the fluidic sample to be injected into the separation path, a valve arrangement fluidically couplable with the separation path, fluidically coupled with the sample accommodation volume, and being controllable for injecting the fluidic sample into the separation path, an input interface configured for receiving input data indicative of an injection profile of an injector to be emulated by the configurable injector, and a control unit configured for controlling the configurable injector, in particular the valve arrangement, so that the configurable injector is operated in accordance with the injection profile to thereby emulate the injector to be emulated.

A configurable injector for injecting a fluidic sample in a separation path of a sample separation apparatus includes a sample accommodation volume for accommodating the fluidic sample to be injected into the separation path, a valve arrangement fluidically couplable with the separation path, fluidically coupled with the sample accommodation volume, and being controllable for injecting the fluidic sample into the separation path, an input interface configured for receiving input data indicative of an injection profile of an injector to be emulated by the configurable injector, and a control unit configured for controlling the configurable injector, in particular the valve arrangement, so that the configurable injector is operated in accordance with the injection profile to thereby emulate the injector to be emulated.

When injecting a sample into carrier-liquid channels (3A and 3B), injection shock is prevented. Septa 13 and 14 constitute the upper wall and the lower wall of a sample injection part (11) of the carrier-liquid channels (3A and 3B). A needle (27) can vertically penetrate the septum (13) on the upper wall side and also penetrate the septum (14) on the lower wall side. A needle moving unit (28) induces the needle (27) to penetrate the septum (14) on the lower wall side and induces the tip of the needle to face the inside of a sample vessel (26). A measurement pump (29) is operated for drawing and as a result a sample is drawn into the needle (27). Next, the needle (27) is extracted from the septum (14) on the lower wall side, the tip of the needle is induced to face the inside of the sample injection part (11), the measurement pump (29) is caused to discharge and as a result the sample within the needle (27) is injected.