The present invention discloses a general sample injector, comprising a sample injection port mechanism, a sample injector shell, a vaporizing chamber, a heater, a temperature control unit, a carrier gas channel, a septum purge channel, a flow splitting channel, a coolant channel, a multichannel flow control valve and a temperature control unit. The general sample injector, equivalent to a programmed temperature vaporizer injector combining splitting/no splitting with cold column head sample injection, gives full play to the advantages of various sample injection modes, overcomes a plurality of disadvantages, and has higher practicability and better flexibility.

A supercritical fluid separation apparatus performs feedback control of output of a heater so that a separation part temperature becomes a set temperature, based on both output of a first temperature sensor that measures a heating block temperature and output of a second temperature sensor that measures the separation part temperature. When a difference between the separation part temperature and the set temperature is large (equal to or more than a predetermined value), output of the heater is adjusted based on the heating block temperature. When a difference between the separation part temperature and the set temperature becomes small (less than a predetermined value), the output of the heater is adjusted based on the difference.

A supercritical fluid separation apparatus performs feedback control of output of a heater so that a separation part temperature becomes a set temperature, based on both output of a first temperature sensor that measures a heating block temperature and output of a second temperature sensor that measures the separation part temperature. When a difference between the separation part temperature and the set temperature is large (equal to or more than a predetermined value), output of the heater is adjusted based on the heating block temperature. When a difference between the separation part temperature and the set temperature becomes small (less than a predetermined value), the output of the heater is adjusted based on the difference.

A sample vial adapter for use in liquid chromatography includes a body structure extending between a top end and a bottom end and defining a channel for receiving a sample vial having a cylindrical sample vial body such that the channel at least partially encircles the received sample vial, the body structure including a channel opening configured to receive the sample vial, the body structure including an extension reducing a width of the channel opening, at least one of the extension and the body structure configured to elastically deform during the process of receiving the sample vial.

A sample vial adapter for use in liquid chromatography includes a body structure extending between a top end and a bottom end and defining a channel for receiving a sample vial having a cylindrical sample vial body such that the channel at least partially encircles the received sample vial, the body structure including a channel opening configured to receive the sample vial, the body structure including an extension reducing a width of the channel opening, at least one of the extension and the body structure configured to elastically deform during the process of receiving the sample vial.

A device for a gas chromatograph system includes an injector, a conduit assembly, a flow restrictor, and a pressure controller. The injector is connected to a carrier gas source and an auxiliary gas source. The conduit assembly surrounds the input end of an analytical column. A carrier gas is supplied at a constant pressure through a flow restrictor to the injector. A pressure controller is configured to control the pressure of an auxiliary gas supplied to the injector from the auxiliary source. The pressure controller is configured to operate in a first mode to provide a first auxiliary gas pressure sufficient to force a flow of the auxiliary gas and a sample onto the analytical column during an inject phase and to operate in a second mode to provide a second auxiliary gas pressure below a threshold necessary to flow auxiliary gas into the analytical column during a resolving phase.

The present invention addresses to an automated gas injection system in vials with rubber septa, for simultaneous injection of gas in 24 or more positions, with injection pressure control and/or overpressure detection, applied to mass spectrometry analyses and/or gas chromatography. The present invention can be used, for example, in isotopic analyses of geological materials in equipment with carbonate extraction units, in the cleaning and decontamination of tubes to be used in isotopic or chromatographic analyses, and in the removal of contaminants from steam drag or by continuous flow, or coming from the free space of vials or tubes in the analyses of organic and inorganic materials. The application of this invention allows reducing the current times of routine purge (flush) of at very least 3 minutes for every 2 positions (72 positions in total and final time of 108 minutes, in a batch of samples) to a total of 96 positions in 3 minutes, with a reduction of 12 times or more in the flush time, which implies greater analytical capacity to the laboratory, lower external costs of sending samples, less time to obtain results, with technology that is easy to implement in universities and research centers in general, in addition to increasing the lifespan of rubber septa.

The present invention addresses to an automated gas injection system in vials with rubber septa, for simultaneous injection of gas in 24 or more positions, with injection pressure control and/or overpressure detection, applied to mass spectrometry analyses and/or gas chromatography. The present invention can be used, for example, in isotopic analyses of geological materials in equipment with carbonate extraction units, in the cleaning and decontamination of tubes to be used in isotopic or chromatographic analyses, and in the removal of contaminants from steam drag or by continuous flow, or coming from the free space of vials or tubes in the analyses of organic and inorganic materials. The application of this invention allows reducing the current times of routine purge (flush) of at very least 3 minutes for every 2 positions (72 positions in total and final time of 108 minutes, in a batch of samples) to a total of 96 positions in 3 minutes, with a reduction of 12 times or more in the flush time, which implies greater analytical capacity to the laboratory, lower external costs of sending samples, less time to obtain results, with technology that is easy to implement in universities and research centers in general, in addition to increasing the lifespan of rubber septa.

A needle receiving assembly includes a fluid conducting element housing, a sealing element configured to receive a needle, and a fluid conducting element. The needle receiving assembly is configured to connect to a needle of a needle assembly. The fluid conducting element housing comprises an aligning component configured to contact a needle housing of the needle assembly and to increase alignment between the needle and the needle receiving assembly. The fluid conducting element housing comprises a lateral protruding portion including an inner lateral surface that laterally surrounds a cavity of the fluid conducting element housing and a central protruding portion protruding beyond a base of the fluid conducting element housing and the central protruding portion. The aligning component comprises an aligning inner surface formed by a portion of the inner lateral surface of the lateral protruding portion.

A needle receiving assembly includes a fluid conducting element housing, a sealing element configured to receive a needle, and a fluid conducting element. The needle receiving assembly is configured to connect to a needle of a needle assembly. The fluid conducting element housing comprises an aligning component configured to contact a needle housing of the needle assembly and to increase alignment between the needle and the needle receiving assembly. The fluid conducting element housing comprises a lateral protruding portion including an inner lateral surface that laterally surrounds a cavity of the fluid conducting element housing and a central protruding portion protruding beyond a base of the fluid conducting element housing and the central protruding portion. The aligning component comprises an aligning inner surface formed by a portion of the inner lateral surface of the lateral protruding portion.