The invention relates to a system and micro monitor apparatus, a space-, time-, and cost-efficient device to concentrate, identify, and quantify organic compounds in gas environments. The invention further relates to a method centered on gas chromatography for identifying and quantifying organic compounds in gas environments, using air as the carrier gas, without the need for a compressed pre-bottled purified carrier gas.

The invention relates to a system and micro monitor apparatus, a space-, time-, and cost-efficient device to concentrate, identify, and quantify organic compounds in gas environments. The invention further relates to a method centered on gas chromatography for identifying and quantifying organic compounds in gas environments, using air as the carrier gas, without the need for a compressed pre-bottled purified carrier gas.

A sample introduction device 10 includes a tube holding section 21 and a sample removing mechanism 40. The sample removing mechanism 40 removes a sample 6 in a sample tube 2 held by the tube holding section 21. Thus, in the sample introduction device 10, the sample 6 in the sample tube 2 held by the tube holding section 21 can be automatically removed. As a result, the operator no longer needs to perform an operation of taking out the sample 6 from the sample tube 2. Thus, a work load on the operator can be reduced.

Systems and methods are described to maintain a liquid sample segment of a sample transmitted through a transfer line from a remote sampling to an analysis system. A system, embodiment includes, but is not limited to, a sample transfer line configured to transport a liquid sample from a remote sampling system via gas pressure; a sample loop fluidically coupled with the sample transfer line, the sample loop configured to hold a sample fluid; and a backpressure chamber fluidically coupled with a gas pressure source and with the sample transfer line, the backpressure chamber configured to supply a backpressure against the liquid sample during transport through the sample transfer line.

A gas analyzer system (100, 200, 300) and methods of reducing sample carryover in a gas sample selector (102, 202, 302). The gas analyzer system (100, 200, 300) includes a gas chromatograph (104, 204, 304) and a gas sample selector (102, 202, 302). The gas sample selector (102, 202, 302) includes a multi-position selector valve (130, 230, 330), a flush valve (140, 240, 340), and a purge valve (150, 250, 350), as well as conduits providing flowpaths between them. When switching the flush valve (140, 240, 340) to connect the flush valve (140, 240, 340) vent and flush valve (140, 240, 340) outlet and flowing purge gas through the purge valve (150, 250, 350) port, the purge gas will flow to the selector (102, 202, 302) exit and to the flush valve (140, 240, 340) vent to remove sample gas from the flowpaths.

A gas analyzer system (100, 200, 300) and methods of reducing sample carryover in a gas sample selector (102, 202, 302). The gas analyzer system (100, 200, 300) includes a gas chromatograph (104, 204, 304) and a gas sample selector (102, 202, 302). The gas sample selector (102, 202, 302) includes a multi-position selector valve (130, 230, 330), a flush valve (140, 240, 340), and a purge valve (150, 250, 350), as well as conduits providing flowpaths between them. When switching the flush valve (140, 240, 340) to connect the flush valve (140, 240, 340) vent and flush valve (140, 240, 340) outlet and flowing purge gas through the purge valve (150, 250, 350) port, the purge gas will flow to the selector (102, 202, 302) exit and to the flush valve (140, 240, 340) vent to remove sample gas from the flowpaths.

The exemplary embodiments may provide liquid chromatography systems that are smaller in size and with reduced extra-column volume than conventional liquid chromatography systems. The exemplary embodiments may reduce the size of the liquid chromatography systems enough that the liquid chromatography systems of the exemplary embodiments may be deployed adjacent to automated sample preparation robotics, adjacent to a process stream, or adjacent to the inlet of a mass spectrometer. In addition, the exemplary embodiments may reduce the extra-column volume of the liquid chromatography system by eliminating many of the connection tubes found in conventional liquid chromatography systems and by situating components of the liquid chromatography system in closer proximity.

The exemplary embodiments may provide liquid chromatography systems that are smaller in size and with reduced extra-column volume than conventional liquid chromatography systems. The exemplary embodiments may reduce the size of the liquid chromatography systems enough that the liquid chromatography systems of the exemplary embodiments may be deployed adjacent to automated sample preparation robotics, adjacent to a process stream, or adjacent to the inlet of a mass spectrometer. In addition, the exemplary embodiments may reduce the extra-column volume of the liquid chromatography system by eliminating many of the connection tubes found in conventional liquid chromatography systems and by situating components of the liquid chromatography system in closer proximity.

A liquid chromatography system includes a solvent delivery system, a sample manager including a sample delivery system in fluidic communication with the solvent delivery system, the sample delivery system configured to inject a sample from a sample-vial into a chromatographic flow stream, a liquid chromatography column located downstream from the sample delivery system, and a detector located downstream from the liquid chromatography column. The sample delivery system further includes a first needle drive including a first sample needle configured to extract the sample from the sample-vial and deliver the sample to the liquid chromatography column, and a first syringe in communication with the first sample needle configured to meter extraction of the sample from the sample-vial. The sample manager further includes a sample automation system that includes a second needle drive including a second sample needle configured to add a volume of reagent to the sample-vial.

A liquid chromatography system includes a solvent delivery system, a sample manager including a sample delivery system in fluidic communication with the solvent delivery system, the sample delivery system configured to inject a sample from a sample-vial into a chromatographic flow stream, a liquid chromatography column located downstream from the sample delivery system, and a detector located downstream from the liquid chromatography column. The sample delivery system further includes a first needle drive including a first sample needle configured to extract the sample from the sample-vial and deliver the sample to the liquid chromatography column, and a first syringe in communication with the first sample needle configured to meter extraction of the sample from the sample-vial. The sample manager further includes a sample automation system that includes a second needle drive including a second sample needle configured to add a volume of reagent to the sample-vial.