An improved gas chromatography system is presented. The system comprises: an enclosure having an inlet and an outlet, such that the ventilation flow is from the inlet to the outlet; a chamber disposed in the enclosure; a monolithic gas analyzer disposed in the chamber and a temperature control unit disposed in physical contact with the chamber. The monolithic gas analyzer operates to separate and detect molecules from a gas; whereas, the temperature control unit is configured to control temperature inside the chamber.

An improved gas chromatography system is presented. The system comprises: an enclosure having an inlet and an outlet, such that the ventilation flow is from the inlet to the outlet; a chamber disposed in the enclosure; a monolithic gas analyzer disposed in the chamber and a temperature control unit disposed in physical contact with the chamber. The monolithic gas analyzer operates to separate and detect molecules from a gas; whereas, the temperature control unit is configured to control temperature inside the chamber.

A method for applying a heating sequence for a modulator includes, during a first period of time, heating a first heating zone disposed along a length of the modulator without heating a second heating zone to cause a sample trapped from a first transfer line at an entrance of the modulator to move from the first heating zone to the second heating zone. The method also includes, during a second time period, withdrawing the heating of the first heating zone to prevent the sample from entering the modulator from the first transfer line. During a third time period, the method includes heating the second heating zone without heating the first heating zone to reinject the sample into a second transfer line.

A method for applying a heating sequence for a modulator includes, during a first period of time, heating a first heating zone disposed along a length of the modulator without heating a second heating zone to cause a sample trapped from a first transfer line at an entrance of the modulator to move from the first heating zone to the second heating zone. The method also includes, during a second time period, withdrawing the heating of the first heating zone to prevent the sample from entering the modulator from the first transfer line. During a third time period, the method includes heating the second heating zone without heating the first heating zone to reinject the sample into a second transfer line.

The present invention relates to a method for separating a sample comprising a nucleic acid, the method comprising: (a) loading a sample comprising a nucleic acid onto an anion-exchange column; and (b) eluting the sample from the anion-exchange column using a salt gradient, wherein a mobile phase used in the eluting step comprises a mild ion-pairing cation, and wherein a column temperature of the anion-exchange column is greater than 30° C. The present invention also relates to a method for determining one or more calorimetric properties of a nucleic acid using anion-exchange chromatography.

A chromatography analysis system includes a liquid delivery pump (2), an autosampler (4), a separation column (12), a column oven (6), a detector (8). The chromatography analysis system further comprising a shutdown execution part (22) configured to start shutdown to finally stop driving of the liquid delivery pump (2) and temperature control operation of the column oven (6) at a time when a predetermined situation occurs, by controlling operation of the liquid delivery pump (2) and the column oven (6), and a column protection temperature setter (24) configured to set a column protection temperature for preventing deterioration of the separation column (12) due to overheating. The shutdown execution part (22) is configured to stop driving of the heater (14) in a state where the liquid delivery pump (2) is driven when the shutdown is started, and then, stop driving of the liquid delivery pump (2) after a temperature of the internal space detected by the temperature sensor (18) becomes equal to or less than the column protection temperature.

A liquid chromatograph includes a liquid feeding portion, a sample injection portion, a separation column, a first temperature adjustment device which raises temperature of the separation column to a first temperature, a detector, a second temperature adjustment device which is provided upstream of the separation column and adjusts temperature of a mobile phase to a second temperature lower than the first temperature, and a control device which controls at least one of the liquid feeding portion and the second temperature adjustment device. The control device controls at least one of the liquid feeding portion and the second temperature adjustment device such that the mobile phase adjusted to the second temperature is fed to the separation column before a next sample is injected after separation of sample components by the separation column ends.

Provided is a gas chromatograph device capable of appropriately determining that a temperature of an entirety of a heating target has stabilized after cooling the heating target in a column oven to a target temperature after a temperature-rising analysis. A gas chromatograph device capable of performing a temperature-rising analysis cools an inside of a column oven by a cooling mechanism. When a detection temperature by a temperature sensor for detecting a temperature of the heating target has reached a target temperature after the inside of the column oven has been cooled, the heating target is heated by a heater. Upon reaching of the detection temperature of the temperature sensor to the target temperature, it is determined whether or not the temperature of the entirety of the heating target has stabilized based on power consumption of the heater.

A system and method for performing field-portable GC/MS measurements for the rapid sampling and measurement of high temperature boiling semi-volatile organic compounds in environmental samples, wherein other column bundles have cold spots that may prevent high temperature boiling semi-volatile components from eluting the GC column, this new design may eliminate those cold spots on the GC column.

A gas chromatograph is provided which is capable of effectively reducing the amount consumed of a carrier gas, reducing the time and effort required for an operator to manually set parameters, and preventing damages to a column and a detector due to a setting mistake. In a case where a stop operation for the power supply of the gas chromatograph is performed (Yes in step S101), the flow rate of a carrier gas to be supplied to a sample vaporization chamber is decreased and the temperatures of the column and the detector are sufficiently lowered (steps S102 to S104), and then the power supply of the gas chromatograph is switched over from an ON state to an OFF state (step S106).