An NMR rotor comprises a receptacle for inserting a sample container into a homogeneous region of an NMR magnetic field with flux density B, the field vector of which in the homogeneous region extends in the vertical direction along a z-axis. The rotor passes through regions with inhomogeneous magnetic field components and a flux density gradient dB/dz when the sample container is introduced. The rotor includes at least two different materials, one with diamagnetic properties and another with non-diamagnetic properties. The different materials are arranged to be geometrically distributed in the rotor so that the magnetic force on the rotor under the effect of a product t of magnetic flux density B and flux density gradient dB/dz, the magnitude of which exceeds 1400 T.sup.2/m, either acts in the same direction as the weight force of the rotor or is smaller in magnitude than the weight force of the rotor.

An NMR rotor comprises a receptacle for inserting a sample container into a homogeneous region of an NMR magnetic field with flux density B, the field vector of which in the homogeneous region extends in the vertical direction along a z-axis. The rotor passes through regions with inhomogeneous magnetic field components and a flux density gradient dB/dz when the sample container is introduced. The rotor includes at least two different materials, one with diamagnetic properties and another with non-diamagnetic properties. The different materials are arranged to be geometrically distributed in the rotor so that the magnetic force on the rotor under the effect of a product t of magnetic flux density B and flux density gradient dB/dz, the magnitude of which exceeds 1400 T.sup.2/m, either acts in the same direction as the weight force of the rotor or is smaller in magnitude than the weight force of the rotor.

Methods for determining a volume of stored gas within a rock sample includes loading a rock sample into an overburden cell. A hydrocarbon gas at a gas pressure is applied to the rock sample and a confining fluid at a confining pressure is applied to the overburden cell. The confining pressure and the gas pressure are increased until a first pressure and temperature condition is met. With the rock sample maintained at the first temperature and pressure condition, a nuclear magnetic resonance spectrometer is used to scan the rock sample and measure a hydrocarbon gas volume within the rock sample. This measured hydrocarbon gas volume is then corrected using a Real Gas Index to determine the volume of stored gas within the rock sample.

Methods for determining a volume of stored gas within a rock sample includes loading a rock sample into an overburden cell. A hydrocarbon gas at a gas pressure is applied to the rock sample and a confining fluid at a confining pressure is applied to the overburden cell. The confining pressure and the gas pressure are increased until a first pressure and temperature condition is met. With the rock sample maintained at the first temperature and pressure condition, a nuclear magnetic resonance spectrometer is used to scan the rock sample and measure a hydrocarbon gas volume within the rock sample. This measured hydrocarbon gas volume is then corrected using a Real Gas Index to determine the volume of stored gas within the rock sample.

A composition is provided. The composition includes a magnetic resonance (MR) probe and a glassification agent. The glassification agent includes lactic acid.

Among the various aspects of the present disclosure is the provision of systems and spherical rotors suitable for use in magic angle spinning (MAS) nuclear magnetic resonance (NMR) spectroscopy and methods of use thereof.

Among the various aspects of the present disclosure is the provision of systems and spherical rotors suitable for use in magic angle spinning (MAS) nuclear magnetic resonance (NMR) spectroscopy and methods of use thereof.

A cooling system, an apparatus for producing hyperpolarized samples, where the apparatus includes the cooling system, and a method for assembling and using the cooling system are disclosed. The cooling system includes a cryogenic chamber, a cooling plate, a sample sleeve, a thermal switch, and an interposer. Also, the cryogenic chamber includes a cryogenic fluid and the cooling plate is disposed in the cryogenic chamber, in contact with the cryogenic fluid. Further, the sample sleeve is configured to receive a sample. The sample sleeve is at least partially inserted in the cryogenic chamber. The thermal switch is disposed between the cooling plate and the sample sleeve. Moreover, the interposer is disposed between at least one of (i) the thermal switch and the cooling plate and (ii) the thermal switch and the sample sleeve. The interposer includes a gallium indium tin alloy.

A cooling system, an apparatus for producing hyperpolarized samples, where the apparatus includes the cooling system, and a method for assembling and using the cooling system are disclosed. The cooling system includes a cryogenic chamber, a cooling plate, a sample sleeve, a thermal switch, and an interposer. Also, the cryogenic chamber includes a cryogenic fluid and the cooling plate is disposed in the cryogenic chamber, in contact with the cryogenic fluid. Further, the sample sleeve is configured to receive a sample. The sample sleeve is at least partially inserted in the cryogenic chamber. The thermal switch is disposed between the cooling plate and the sample sleeve. Moreover, the interposer is disposed between at least one of (i) the thermal switch and the cooling plate and (ii) the thermal switch and the sample sleeve. The interposer includes a gallium indium tin alloy.

A system for providing a magnetic field for a sample includes a first contact surface for thermally contacting the sample and a second contact surface, which is in thermal contact with at least one magnetic element.