A chromatographic system for rapid analysis of fluid components having a wide molecular range in a single sample is disclosed. A single isothermal oven having a switching valve controls the flow between a single column module and a dual column module. The single column module contains a shielded column with an input receiving components from a sample input and output to a detector via the valve. The dual column module contains two shielded columns wrapped adjacent one another on a single ring with separate inputs and outputs and in communication with one another and detectors through the switching valve. One or both columns in the dual column module can be heated and monitored with one or more sensor wires.

The pyrolysis reactor system for the conversion and analysis of organic solid waste is a dual gas-liquid separation system, allowing for the conversion of organic solid waste, as well as analysis of the conversion products. A pyrolysis reactor is provided for converting the organic solid waste into a solid product and a gas-liquid product mixture through pyrolysis. A source of carrier gas is in fluid communication with the pyrolysis reactor for degrading the organic solid waste. A first gas-liquid separator is in fluid communication with the pyrolysis reactor and receives the gas-liquid product mixture therefrom, separating a portion of gas therefrom. A second gas-liquid separator is in fluid communication with the first gas-liquid separator and receives the gas-liquid product mixture therefrom and separates the remainder of the gas therefrom. The remainder of the gas and the separated liquid are each collected separately from one another, in addition to the char.

An improved liquid vaporization and conditioning system, and associated method, for efficiently vaporizing a liquid sample for accurately determining the constituent components thereof providing enhanced flow rate, pressure and thermal control, the improvement including a combination of a resistance temperature detector, a sweeping bend to, an in-line thermal break, a flow buffering input manifold, enhanced multi-path heater vaporizer construction with four heater units, a vaporizer output mixing manifold and control elements providing a capability for partial shutdown in the event of compromised heating or flow anomalies without risk of flow loss/volume capacity beyond a permissible threshold and an improved, modular heat vaporizer enclosure.

A method of detecting an analyte by: providing a derivatizing agent that is reactive with the analyte; delivering the derivatizing agent into a chamber; delivering a sample of a gas suspected of containing the analyte into the chamber before or after delivering the derivatizing agent, while the chamber is maintained at a temperature that retains the derivatizing agent and any analyte and that allows reaction between the derivatizing agent and any analyte in the chamber to form a derivatized analyte; warming the chamber to cause evaporation of any derivatized analyte; and delivering the derivatized analyte in the chamber into a gas chromatograph column.

An inductive flash desorber includes: an induction coil that includes a coil; an substrate disposed through the induction coil; and a flow tube interposed between the induction coil and the substrate such that the flow tube: is encircled by the coil; surrounds the substrate within the coil; receives a carrier fluid that entrains the desorbed analyte from the substrate; and forms an analytical composition comprising the carrier fluid and the desorbed analyte, the flow tube including: a first end that receives the carrier fluid; and a second end opposing the first end through which the analytical composition flows.

A housing is provided with an internal space for accommodating an insert and a cylindrical cap attachment part provided, at the distal end surface thereof, with an opening part communicating with the internal space. An inclined groove that is inclined from the distal end side to the proximal end side of the cap attachment part along the circumferential direction of the cap attachment part is provided on the outer circumferential surface of the cap attachment part. A cap fixing part for attaching a seal cap to the cap attachment part has a cap holding part for holding the outer peripheral surface of the seal cap and an elastic part connected to the cap holding part. The elastic part is provided with a protrusion that is fit into the inclined groove of the outer peripheral surface of the cap attachment part.

Detection sensitivity of a single-filament thermal conductivity detector is to be increased. A thermal conductivity detector is a single-filament thermal conductivity detector, and includes a measurement cell, a phase switching mechanism, and a measurement section. The measurement section starts measurement of thermal conductivity of a sample gas after a lapse of a sample gas measurement start time that is set in advance, after a reference phase is switched to a sample phase by the phase switching mechanism, and starts measurement of thermal conductivity of a reference gas after a lapse of a reference gas measurement start time that is set in advance as a length of time different from the sample gas measurement start time, after the sample phase is switched to the reference phase by the phase switching mechanism.

A vacuum-assisted coated fiber located in a capillary tube system for sampling and delivering materials to an analytical device and a method for sampling analytes is disclosed. A sorbent comprising polypyrrole/graphene oxide is coated on a fiber inserted within an interior space of the capillary tube to entrap an analyte within a sample. The vacuum-assisted coated fiber located in a capillary tube device also includes a vacuum device configured to vacuum the extraction vial. This may improve the extraction of the analytes vapors from the sample, matrix to the sorbent bed.

In a sample vaporization chamber, a liquid sample is vaporized therein to produce a sample gas. A split flow path is configured to discharge the sample gas in the sample vaporization chamber. A valve is provided in the split flow path and opens/closes to adjust a flow rate of the sample gas flowing through the split flow path. A filler material is provided at a filling position in the sample vaporization chamber or in the split flow path. The controller is configured to control a degree of opening of the valve so that when the sample gas in the sample vaporization chamber is discharged from the split flow path, a pressure in the sample vaporization chamber decreases at a pressure gradient smaller than a pressure gradient at which the filler material is displaced from the filling position.

A gas-blowing liquid sample infusing device includes a sample introducing tube 17 made from a liquid-sample inner tube 40 and a nebulizing-gas outer tube 41 for nebulizing and supplying a liquid sample, and an exhaust sealing tube 18 provided on the circumference of the sample introducing tube 17, and a cushion member 43 that is mounted on the opening of a sample container 19 (the body of an infusion container 21), that allows the sample introducing tube 17 to pass through and has a contact surface for contacting the lower end of the exhaust sealing tube 18, and an engaging member (lid) 20 that includes a cushion admitting concave part 42 in which an engaging part 44 that is mounted on the opening of the sample container 19 and prevents the upward movement of the cushion member 43 is provided on the lateral surface of the inner circumference.