A method of manufacturing a membrane-electrode assembly including an electrolyte membrane and a catalyst layer-formed gas diffusion layer bonded to the electrolyte membrane, the method including: a liquid application step of applying, in the atmosphere, a liquid to only a surface of the catalyst layer before bonding; and a thermocompression bonding step of bonding, to the electrolyte membrane, the catalyst layer-formed gas diffusion layer to which the liquid is applied, by thermocompression bonding. Provided is a method of manufacturing a membrane-electrode assembly including a polymer electrolyte membrane and a catalyst layer-formed gas diffusion layer bonded to the polymer electrolyte membrane, in which the manufacturing method can achieve both the relaxation of thermocompression bonding conditions and the improvement of adhesion between the catalyst layer-formed gas diffusion layer and the electrolyte membrane with high productivity.

A polymer electrolyte membrane (PEM) fuel cell assembly, and a method for making the assembly, are provided. An exemplary method includes forming a functionalized zeolite templated carbon (ZTC), including forming a CaX zeolite, depositing carbon in the CaX zeolite using a chemical vapor deposition (CVD) process to form a carbon/zeolite composite, treating the carbon/zeolite composite with a solution including hydrofluoric acid to form a ZTC, and treating the ZTC to add catalyst sites, forming the functionalized ZTC. The method further includes incorporating the functionalized ZTC into electrodes, forming a membrane electrode assembly (MEA), and forming the PEM fuel cell assembly

A method of providing a cleaned gas diffusion layer for electrochemical applications includes providing a gas diffusion layer such that a first side of the gas diffusion layer is arranged on a first vacuum conveyor belt, cleaning an exposed second side of the gas diffusion layer, the second side being situated opposite the first side of the gas diffusion layer, transferring the partially cleaned gas diffusion layer to a second vacuum conveyor belt partially situated opposite the first vacuum conveyor belt, wherein the first vacuum conveyor belt and the second vacuum conveyor belt have a transfer region in which the gas diffusion layer is transferred from the first vacuum conveyor belt to the second vacuum conveyor belt such that the first side of the gas diffusion layer is exposed, and cleaning the first side of the gas diffusion layer.

A proton exchange membrane fuel cell that uses hydrogen peroxide as an oxidant is disclosed. The proton exchange membrane fuel cell includes an anode gas diffusion layer, an anode catalyst layer, a proton exchange membrane and a cathode catalyst layer arranged sequentially. The proton exchange membrane fuel cell further includes a single electrode plate, and does not include a cathode gas diffusion layer. A cell stack including the proton exchange membrane fuel cell is also disclosed, as well as a method for preparing the proton exchange membrane fuel cell.

Disclosed are a manufacturing method of a membrane electrode assembly capable of increasing the interfacial adhesion between a polymer electrolyte membrane and a catalyst layer, improving substance delivery and performance, and enhancing hydrogen permeation resistance or oxygen permeability; a membrane electrode assembly manufactured thereby; and a fuel cell comprising the membrane electrode assembly. The manufacturing method of the present invention comprises the steps of: adding a catalyst and a first ionomer to a solvent and dispersing the same, thereby producing a dispersed mixture; adding a second ionomer to the dispersed mixture, thereby producing a coating composition; and applying the coating composition directly onto at least one side of the polymer electrolyte membrane.

A method of producing electrodes includes selecting a palladium alloy, annealing the palladium alloy at a first temperature above 350° C., cold working the palladium alloy into a desired electrode shape, and annealing the palladium alloy at a second temperatures and for a time sufficient to produce a grain size between about 5 microns and about 100 microns. The method further includes etching the palladium alloy, rinsing the palladium alloy with at least one of water and heavy water, and storing the palladium alloy in an inert environment.

Disclosed are an electrode for gas generation, a method of preparing the electrode, and a device including the electrode for gas generation. The electrode includes a gas generating electrode layer and a three-dimensional (3D) super-aerophobic layer formed on at least one portion of the gas generating electrode layer and including porous hydrogel.

The present invention provides a catalysed ion-conducting membrane comprising an ion-conducting membrane, an electrocatalyst layer having two opposing faces, and a layer A comprising an ion-conducting material and a carbon containing material. Also provided are methods for preparing the catalysed ion-conducting membrane.

The present invention provides a method of preparing a catalyst material which comprises electrocatalyst particles, a support material, and graphitic carbon nitride, wherein the method comprises applying graphitic carbon nitride to a catalyst material precursor. Also provided is a catalyst material comprising graphitic carbon nitride.

The present invention provides a method of preparing a catalyst material, said catalyst material comprising a support material and an electrocatalyst dispersed on the support material; said method comprising the steps: i) providing a support material; then ii) 10 depositing a silicon oxide precursor on the support material; then iii) carrying out a heat treatment step to convert the silicon oxide precursor to silicon oxide; then iv) depositing said electrocatalyst or a precursor of said electrocatalyst on the support material; then v) removal of at least some of the silicon oxide.