A bulk permanent magnetic material may include between about 5 volume percent and about 40 volume percent Fe.sub.16N.sub.2 phase domains, a plurality of nonmagnetic atoms or molecules forming domain wall pinning sites, and a balance soft magnetic material, wherein at least some of the soft magnetic material is magnetically coupled to the Fe.sub.16N.sub.2 phase domains via exchange spring coupling. In some examples, a bulk permanent magnetic material may be formed by implanting N+ ions in an iron workpiece using ion implantation to form an iron nitride workpiece, pre-annealing the iron nitride workpiece to attach the iron nitride workpiece to a substrate, and post-annealing the iron nitride workpiece to form Fe.sub.16N.sub.2 phase domains within the iron nitride workpiece.

The invention relates to a method for manufacturing a component able to rotate about an axis, comprising a step of incorporating a magnetic material into the powder during the manufacture of the rotating component, in at least one predefined zone of the component formed. The invention also relates to a rotating component obtained using this method and to a system for measuring rotation of the rotating component obtained by this method, by using at least one sensor able to detect the passage of the zone into which the magnetic material is incorporated.

There are provided a rare-earth permanent magnet and a manufacturing method of a rare-earth permanent magnet capable of preventing deterioration of magnet properties. In the method, magnet material is milled into magnet powder. Next, a mixture 12 is prepared by mixing the magnet powder and a binder, and the mixture 12 is formed into a sheet-like shape to obtain a green sheet 14. Thereafter, magnetic field orientation is performed to the green sheet 14, which is then held for several hours in a non-oxidizing atmosphere at a pressure higher than normal atmospheric pressure, at 200 through 900 degrees Celsius for calcination. Thereafter, the calcined green sheet 14 is sintered at a sintering temperature. Thereby a permanent magnet 1 is manufactured.

The present invention provides a producing method of a rare earth sintered magnet which is suitable as a producing method of a high performance rare earth sintered magnet which can reduce the number of steps for reusing defective molded bodies generated in a wet molding step of the rare earth sintered magnet, and which has a small content amount of oxygen. The invention also provides a slurry recycling method used for the producing method, and a slurry recycling apparatus. Each of the methods includes a crushing step of crushing, in mineral oil and/or synthetic fluid, a molded body in which slurry formed from alloy powder for a rare earth sintered magnet and mineral oil and/or synthetic fluid is wet molded in magnetic field, and recycling the crushed molded body into slurry.

There are provided a rare-earth permanent magnet and a manufacturing method of a rare-earth permanent magnet capable of preventing deterioration of magnet properties. In the method, magnet material is milled into magnet powder. Next, a mixture 12 is prepared by mixing the magnet powder and a binder, and the mixture 12 is formed into a sheet-like shape to obtain a green sheet 14. Thereafter, magnetic field orientation is performed to the green sheet 14, which is then held for several hours in a non-oxidizing atmosphere at a pressure higher than normal atmospheric pressure, at 200 through 900 degrees Celsius for calcination. Thereafter, the calcined green sheet 14 is sintered at a sintering temperature. Thereby a permanent magnet 1 is manufactured.

A method for producing a sintered R-iron (Fe)-boron (B) magnet, the method including: (1) producing a sintered magnet R1-FeB-M, where R1 is neodymium (Nd), praseodymium (Pr), terbium (Tb), dysprosium (Dy), gadolinium (Gd), holmium (Ho), or a combination thereof; M is titanium (Ti), vanadium (V), chromium (Cr), manganese (Mn), cobalt (Co), nickel (Ni), gallium (Ga), calcium (Ca), copper (Cu), Zinc (Zn), silicon (Si), aluminum (Al), magnesium (Mg), zirconium (Zr), niobium (Nb), hafnium (Hf), tantalum (Ta), tungsten (W), molybdenum (Mo), or a combination thereof; (2) removing oil, washing using an acid solution, activating, and washing using deionized water the sintered magnet, successively; (3) mixing a superfine terbium powder, an organic solvent, and an antioxidant to yield a homogeneous slurry, coating the homogeneous slurry on the surface of the sintered magnet; and (4) sintering and aging the sintered magnet.

The present invention relates to an anisotropic complex sintered magnet including MnBi with magnetic characteristics enhanced and an atmospheric sintering method for preparing the same. The anisotropic complex sintered magnet including MnBi according to the present invention may implement excellent magnetic characteristics, and thus may replace rare earth bond magnets in the related art, and a continuous process is enabled because the magnet is prepared by an atmospheric sintering method, and a sintering method used in the permanent magnet process in the related art is used as it is, so that the anisotropic complex sintered magnet is economical.

A method comprising sintering a Mn and Bi powder compact at a first temperature for a first predetermined duration, based on the first temperature, and sintering the compact at a second temperature, less than the first temperature, for a second predetermined duration, greater than the first duration, is disclosed. The sintering at a first temperature for a first predetermined duration generates a predetermined MnBi LTP transition driving force to decrease a formation energy barrier for transition to MnBi LTP. Sintering the compact at the second temperature for the second predetermined duration forms a magnet containing the MnBi LTP.

Disclosed are an MnBi sintered magnet exhibiting excellent thermal stability as well as excellent magnetic characteristics at high temperature, an MnBi anisotropic complex sintered magnet, and a method of preparing the same.

Techniques are disclosed for milling an iron-containing raw material in the presence of a nitrogen source to generate anisotropically shaped particles that include iron nitride and have an aspect ratio of at least 1.4. Techniques for nitridizing an anisotropic particle including iron, and annealing an anisotropic particle including iron nitride to form at least one -Fe.sub.16N.sub.2 phase domain within the anisotropic particle including iron nitride also are disclosed. In addition, techniques for aligning and joining anisotropic particles to form a bulk material including iron nitride, such as a bulk permanent magnet including at least one -Fe.sub.16N.sub.2 phase domain, are described. Milling apparatuses utilizing elongated bars, an electric field, and a magnetic field also are disclosed.