A device may include a memory storing instructions and a processor configured to execute the instructions to determine an initial mass of a sample; distill the sample up to at least a thermal destruction temperature; record, at a set of time points during the distilling, vapor temperature values, liquid temperature values, and vapor pressure values associated with the sample; and determine a residual mass of the sample. The processor may be further configured to generate a pressure curve based on the vapor pressure values; calculate a summary integral surface for the generated pressure curve; and generate a distillation curve that relates the vapor temperature values and the liquid temperature values to mass percentage of the sample that has evaporated, based on the calculated summary integral surface, the initial mass of the sample, and the residual mass of the sample.

A vaporizer includes an outer tube configured to receive a flow of heated gas and an inner tube disposed at least partially within the outer tube. The inner tube is spaced apart from the outer tube such that the flow of heated gas is channeled through an annular space therebetween. The vaporizer also includes a crucible disposed at least partially within the inner tube. The crucible is extendable and retractable relative to the inner tube and within the outer tube. The crucible is configured to hold a molten metal such that a surface area of the molten metal exposed to the flow of heated gas is adjustable based on the position of the crucible relative to the inner tube. A heater is configured to vaporize the molten material and the vapor mixes with the flow of heated gas.

An apparatus and method for purification and recovery of an organic liquid. The apparatus includes a distillation kettle and a receiver tank connected by a distillation pipe, and a vacuum pump, wherein a vacuum storage tank is arranged between the receiver tank and the vacuum pump; the vacuum storage tank is connected to the receiver tank by a vacuum regulating pipe, a first vacuum regulating valve being arranged on the vacuum regulating pipe; and the vacuum storage tank is connected to the vacuum pump by an evacuation pipe, a second vacuum regulating valve being arranged on the evacuation pipe. By arranging a vacuum storage tank between the receiver tank and the vacuum pump, the vacuum degree in the receiver tank is regulated by the vacuum storage tank, such that the organic liquid is recovered in a sealed environment under reduced pressure.

Methods and systems for removing drilling fluid from wet drill cuttings are described. According to some embodiments, the method comprises: at a pressure above atmospheric pressure: using an internal combustion engine, combusting an air-fuel mixture comprising air and a hydrocarbon-based fuel, thereby producing a combustion exhaust at a first temperature; providing the combustion exhaust to the wet drill cuttings to contact and directly heat the wet drill cuttings by convection so that at least some fluid is evaporated therefrom and at least some dry solid drill cuttings remain, the evaporated fluid comprising drilling fluid and water; condensing at least a portion of the evaporated fluid to produce condensed drilling fluid, water and non-condensable inert gas; and separately recovering the condensed drilling fluid, the water and the dry solid drill cuttings.

Systems and methods for removing drilling fluid from wet drill cuttings are described. According to some embodiments, the method comprises, at a pressure above atmospheric pressure: combusting a rich air-fuel mixture at a rich combustion temperature, thereby producing a generally low oxygen, inert rich exhaust; providing said rich exhaust to the wet drill cuttings to contact and directly heat the wet drill cuttings by convection so that at least a portion of the drilling fluid is evaporated therefrom and at least some dry solid drill cuttings remain; condensing at least a portion of the evaporated drilling fluid to produce condensed drilling fluid; and separately recovering the condensed drilling fluid and the dry solid drill cuttings.

An abatement system for pyrophoric chemicals where the materials are captured or controlled by a hazard volume and fed to a vaporizer in an oxygen deprived environment. Materials are heated until vaporized while mixed with nitrogen. The mixture exits the system through a reaction column. The system is monitored by oxygen sensors, smoke detectors and temperature sensors.

A system includes a first separator configured to receive waste water, retain a first portion of the waste water, and separate the first portion of the waste water into a first vapor and a first solid material; and a second separator in fluid communication with the first separator, the second separator being configured to receive a second portion of the waste water from the first separator and to separate the second portion of the waste water into a second vapor and a second solid material, the second separator including a first condenser, a heating element, and a first electrocoagulation unit. Related apparatus, systems, techniques and articles are also described.

A system and method for decontaminating a fluid and recovered vapor, particularly processing and recycling water used in an oil zone steam process, utilizing a vaporizer-desalination unit to separate a contaminated water flow into a contaminated disposal flow and a clean water vapor flow. The contaminated water flow is recovered after separation from a combined oil and water flow from an oil well. The clean water vapor flow is preferably passed through a steam generator to produce the steam used in the oil zone steam process. The steam is injected into the oil zone of a designated well and then extracted as the combined oil and water flow. Once primed with sufficient external water, the system and method is designed to operate continuously with minimal replenishment because of the water/vapor/steam cycle.

An incinerator system includes an evaporator tank having a fluid inlet, a steam vent, and an evaporation cavity and a heating assembly having a plurality of heating rods mounted on a rod spacing mechanism and disposed in the evaporation cavity of the evaporator tank. The rod spacing mechanism is configured to move the plurality of heating rods within the evaporation cavity. The incinerator system also includes a sensor system having a plurality of sensors positioned to perform one or more sensor measurements in the evaporation cavity and a programmable logic controller communicatively coupled to the sensor system and the heating assembly. The programmable logic controller is configured to instruct the rod spacing mechanism to move at least one of the plurality of heating rods based on the one or more sensor measurements.

The invention refers to a distillation apparatus (100) for extraction of volatile components from biological material (50), especially from plants, comprising a housing (10) defining a sample chamber (S), a drum (30) arranged in the sample chamber (S), the drum (30) defining a receiving chamber (R) for receiving the biological material (50), and at least one microwave generator (70) for irradiating the biological material (50) with microwave radiation when received in the drum (30); wherein the drum (30) is rotatably arranged in the sample chamber (S) about a rotation axis (H) which is oriented substantially horizontally.