A liquid separator and concentrator is disclosed. An example liquid separator and concentrator includes a separator column. A spray chamber has a sprayer nozzle to spray an influent within the spray chamber and create a falling film in the separator column. A heating jacket surrounds the separator column, wherein the heating jacket heats the falling film to evaporate at least one portion of the falling film and leaves a concentrate. A concentrate collection vessel receives the concentrate from the separator column.

A water based distillation equipment includes a lower boiling vessel for containing plant material and water/steam, and having an open top portion; a heat source for heating the plant material within the lower boiling vessel; and a condenser mechanically connected to the lower boiling vessel so as to cover the open top portion of the lower boiling vessel; and a collection vessel connected to the distillation equipment. The inside walls of the condenser include gutters for collecting hydrolate and condensate within the distillation equipment, and the collection vessel is coupled to the gutters for receiving the collected condensate. The surface area of the condenser is at least about 1.5 times a surface area of the lower boiling vessel.

Processes for removing carbon disulfide from product streams containing a sulfide compound are performed by contacting the product stream with an alkanolamine and converting the carbon disulfide to a higher boiling point product, thereby reducing or eliminating carbon disulfide from the product stream. Subsequent removal of the higher boiling point product via distillation can lead to a purified sulfide stream with high purity.

A high efficiency distillation head and methods of use has a distillation head that may be used for efficient fractional distillation of high boiling point compounds, and includes a lower insulated jacket surrounding a fractionating column and an upper insulated jacket surrounding a condenser. An exit path of equal or greater cross sectional area to the fractionating column is located at or below the top of the fractionating column.

A high efficiency distillation head and methods of use has a distillation head that may be used for efficient fractional distillation of high boiling point compounds, and includes a lower insulated jacket surrounding a fractionating column and an upper insulated jacket surrounding a condenser. An exit path of equal or greater cross sectional area to the fractionating column is located at or below the top of the fractionating column.

The present disclosure relates to the determination of analytes in a sample using chromatography. The present disclosure provides methods of separating an analyte from a sample. A mobile phase is flowed through a chromatography column. The mobile phase includes about 0.005% (v/v) to about 2.50% (v/v) difluoroacetic acid and less than about 100 ppb of any individual impurity, especially metal impurities. A sample including the analyte is injected into the mobile phase. The analyte is separated from the sample.

The present disclosure relates to the determination of analytes in a sample using chromatography. The present disclosure provides methods of separating an analyte from a sample. A mobile phase is flowed through a chromatography column. The mobile phase includes about 0.005% (v/v) to about 2.50% (v/v) difluoroacetic acid and less than about 100 ppb of any individual impurity, especially metal impurities. A sample including the analyte is injected into the mobile phase. The analyte is separated from the sample.

The present patent application relates to a compact device with a modular design, and to a method for extracting volatile oils and herbal distillates contained in organic matter, using the extraction technique of steam distillation. The device is formed by a lower cylindrical module on top of which an upper hemispherical module may be disposed, and both modules may be secured to form a single hermetic body. The lower module may contain a hot-water boiler, a heat conducting disc, a steam-heating chamber, a still of raw material, and a valve for regulating the steam flow. The upper module may contain a conical steam condenser, a hemispherical cover, a ring for collecting distilled liquid, and a tube for removing the distilled liquid. The distillation method of internal steam distillation may integrate, in a single physical body, a semi-closed steam flow circuit that may include all the functions of distillation.

The present patent application relates to a compact device with a modular design, and to a method for extracting volatile oils and herbal distillates contained in organic matter, using the extraction technique of steam distillation. The device is formed by a lower cylindrical module on top of which an upper hemispherical module may be disposed, and both modules may be secured to form a single hermetic body. The lower module may contain a hot-water boiler, a heat conducting disc, a steam-heating chamber, a still of raw material, and a valve for regulating the steam flow. The upper module may contain a conical steam condenser, a hemispherical cover, a ring for collecting distilled liquid, and a tube for removing the distilled liquid. The distillation method of internal steam distillation may integrate, in a single physical body, a semi-closed steam flow circuit that may include all the functions of distillation.

Disclosed is a method for the recovery of filtering agents and rolling oil from a mixture containing used rolling oil and filtering agents coated with used rolling oil in which the mixture containing rolling oil and filtering agents is subjected to vacuum distillation under agitation in a reactor equipped with an agitator and vapour precipitator. The vacuum during distillation is regulated with an inert gas flow, the rolling oil is condensed and collected, and a rolling oil which can be reused for rolling and a powder filtering agent which can be reused are obtained.