B01D3/10

Methods for purifying polyols containing oxyalkylene units to reduce 2-methyl-2-pentenal content
11572440 · 2023-02-07 · ·

Disclosed are methods for purifying polyols containing oxyalkylene units that is an alkali metal catalyzed alkoxylation reaction product of an alkylene oxide and an H-functional starter. The methods include neutralizing the alkali metal ions with an aqueous solution comprising water and sulfuric acid, in which: (i) the sulfuric acid is present in an amount of no more than 5% by weight, based on the total weight of the aqueous solution, and (ii) the sulfuric acid is used in an amount of 2% to 10% more than the theoretical amount necessary to neutralize all of the alkali metal ions present. The methods can produce polyols having a low content of 2-methyl-2-pentenal.

Methods for purifying polyols containing oxyalkylene units to reduce 2-methyl-2-pentenal content
11572440 · 2023-02-07 · ·

Disclosed are methods for purifying polyols containing oxyalkylene units that is an alkali metal catalyzed alkoxylation reaction product of an alkylene oxide and an H-functional starter. The methods include neutralizing the alkali metal ions with an aqueous solution comprising water and sulfuric acid, in which: (i) the sulfuric acid is present in an amount of no more than 5% by weight, based on the total weight of the aqueous solution, and (ii) the sulfuric acid is used in an amount of 2% to 10% more than the theoretical amount necessary to neutralize all of the alkali metal ions present. The methods can produce polyols having a low content of 2-methyl-2-pentenal.

Ammonia Mediated Carbon Dioxide (CO2) Sequestration Methods and Systems
20230029844 · 2023-02-02 ·

Methods of sequestering carbon dioxide (CO.sub.2) are provided. Aspects of the methods include contacting an aqueous capture ammonia with a gaseous source of CO.sub.2 under conditions sufficient to produce an aqueous ammonium carbonate. The aqueous ammonium carbonate is then combined with a cation source under conditions sufficient to produce a solid CO.sub.2 sequestering carbonate and an aqueous ammonium salt. The aqueous capture ammonia is then regenerated from the from the aqueous ammonium salt. Also provided are systems configured for carrying out the methods.

Ammonia Mediated Carbon Dioxide (CO2) Sequestration Methods and Systems
20230029844 · 2023-02-02 ·

Methods of sequestering carbon dioxide (CO.sub.2) are provided. Aspects of the methods include contacting an aqueous capture ammonia with a gaseous source of CO.sub.2 under conditions sufficient to produce an aqueous ammonium carbonate. The aqueous ammonium carbonate is then combined with a cation source under conditions sufficient to produce a solid CO.sub.2 sequestering carbonate and an aqueous ammonium salt. The aqueous capture ammonia is then regenerated from the from the aqueous ammonium salt. Also provided are systems configured for carrying out the methods.

METHOD AND DEVICE FOR PREPARING ADIPONITRILE

Provided are a method and device for preparing adiponitrile. The method of the present disclosure comprises the steps of a first hydrocyanation reaction, an isomerization reaction and a second hydrocyanation reaction, wherein online Raman spectroscopy is used for detecting the content of a specific component in the system; and the reaction conditions are regulated based on the detection results, so as to achieve precise control of the materials in each step of the reaction system. The method of the present disclosure can reduce an amount of butadiene, thereby reducing the subsequent energy consumption needed for recycling butadiene and equipment investment after reaction; by monitoring the content of hydrocyanic acid in real time, the residue of hydrocyanic acid is reduced to a lower level, and the operation safety and the stability of a catalyst during reaction are improved; and the loss of the catalyst is reduced.

SYSTEMS AND METHODS FOR CANNABIS CBD EXTRACTION
20230034720 · 2023-02-02 ·

Systems and methods for extracting a compound of interest from plant material, such as a cannabidiol (CBD) from cannabis, are provided. Particularly, the disclosed systems and methods utilize a crude oil to separate water and impurities including fats, sugars, resin glues, chlorophyll, and proteins prior to preparation of a CBD distillate. The systems and methods are operable to remove the impurities from the crude oil with a brine solution and at least one acid prior to distillation. The systems and methods are operable with conventional solvents containing between about 5 wt % and about 8 wt % water.

SYSTEMS AND METHODS FOR CANNABIS CBD EXTRACTION
20230034720 · 2023-02-02 ·

Systems and methods for extracting a compound of interest from plant material, such as a cannabidiol (CBD) from cannabis, are provided. Particularly, the disclosed systems and methods utilize a crude oil to separate water and impurities including fats, sugars, resin glues, chlorophyll, and proteins prior to preparation of a CBD distillate. The systems and methods are operable to remove the impurities from the crude oil with a brine solution and at least one acid prior to distillation. The systems and methods are operable with conventional solvents containing between about 5 wt % and about 8 wt % water.

Low energy ejector desalination system

A system to treat and desalinate wastewater using a low energy ejector desalination system (LEEDS), which employs a static liquid-gas ejector and maximum heat integration in the water treatment system.

SIMULTANEOUS DISTILLATION AND ALLOYING

A device for producing a target material from starting material comprises a chamber, at least one trough, at least a first heating element being configured to heat the chamber such that starting material is vaporized, and at least one collecting vessel being configured to receive a condensate that will constitute the target material. The device optionally comprises at least a first source of negative pressure or at least a first supply device being in connection with the chamber being configured to evacuate the chamber or to supply an inert gas to the chamber. The device further comprises at least one condensation device, wherein said condensation device is configured to condensate the vaporized starting material, whereby the condensate is formed, and/or at least a first gate device being in connection with the chamber such, that the starting material is introducible into the chamber via said first gate device.

SIMULTANEOUS DISTILLATION AND ALLOYING

A device for producing a target material from starting material comprises a chamber, at least one trough, at least a first heating element being configured to heat the chamber such that starting material is vaporized, and at least one collecting vessel being configured to receive a condensate that will constitute the target material. The device optionally comprises at least a first source of negative pressure or at least a first supply device being in connection with the chamber being configured to evacuate the chamber or to supply an inert gas to the chamber. The device further comprises at least one condensation device, wherein said condensation device is configured to condensate the vaporized starting material, whereby the condensate is formed, and/or at least a first gate device being in connection with the chamber such, that the starting material is introducible into the chamber via said first gate device.