A distillation column comprises at least one wall enclosing a chamber and at least one feed input, at least one condensate removal point and at least one vapor take-off point; wherein the column further comprises a polygonal cross-section component that is mounted within the chamber; and wherein the polygonal component is configured to rotate within the chamber in use.

A distillation column comprises at least one wall enclosing a chamber and at least one feed input, at least one condensate removal point and at least one vapor take-off point; wherein the column further comprises a polygonal cross-section component that is mounted within the chamber; and wherein the polygonal component is configured to rotate within the chamber in use.

PROBLEM To provide a composition comprising highly enriched PUFA or its alkyl esters while containing fatty acid esters of 3-MCPD at adequately low concentrations and to provide an efficient method for producing the composition. MEANS FOR SOLVING A composition that contains fatty acids or fatty acid alkyl esters as its major component, the composition containing highly unsaturated fatty acid or alkyl ester thereof, wherein the proportion of the highly unsaturated fatty acid in the constituent fatty acids of the composition is 50 area % or more and wherein the concentration of 3-MCPD as found upon analyzing the composition by American Oil Chemists' Society official method Cd 29b-13 assay A is less than 1.80 ppm.

PROBLEM To provide a composition comprising highly enriched PUFA or its alkyl esters while containing fatty acid esters of 3-MCPD at adequately low concentrations and to provide an efficient method for producing the composition. MEANS FOR SOLVING A composition that contains fatty acids or fatty acid alkyl esters as its major component, the composition containing highly unsaturated fatty acid or alkyl ester thereof, wherein the proportion of the highly unsaturated fatty acid in the constituent fatty acids of the composition is 50 area % or more and wherein the concentration of 3-MCPD as found upon analyzing the composition by American Oil Chemists' Society official method Cd 29b-13 assay A is less than 1.80 ppm.

The present invention relates to a process for preparing di- and polyamines of the diphenylmethane series (MDA), a system for producing MDA and a process for operating a system for preparing MDA. The invention enables optimization of production standstills during operation of the MDA process with respect to time expenditure and optionally also with respect to energy and material consumption by means of a so-called recirculation mode for individual system components. During interruption of the process or interruption of the operation of individual system components, formaldehyde is not introduced into the reaction and the system components that are not affected by a revision, repair, or cleaning measure are operated in so-called recirculation mode. This enables, among other things, that only the affected system component can be put in standstill during the time period of the measure, which is advantageous in terms of productivity and economy of the process as well as in terms of the quality of the products produced.

To provide a composition comprising highly enriched PUFA or its alkyl esters while containing fatty acid esters of 3-MCPD at adequately low concentrations and to provide an efficient method for producing the composition. MEANS FOR SOLVING A composition that contains fatty acids or fatty acid alkyl esters as its major component, the composition containing highly unsaturated fatty acid or alkyl ester thereof, wherein the proportion of the highly unsaturated fatty acid in the constituent fatty acids of the composition is 50 area % or more and wherein the concentration of 3-MCPD as found upon analyzing the composition by American Oil Chemists' Society official method Cd 29b-13 assay A is less than 1.80 ppm.

A cannabis oil extraction apparatus may include an extraction unit, condenser, winterization unit, micron filter, preheater, short-path distillation unit, and condenser. The extraction unit may utilize cellular disruption in a food grade solvent to extract cannabis oil from plant material. The short-path distillation unit may utilize molecular distillation. The short-path distillation unit may include a recirculation loop for multiple passes through the short-path distillation unit to separate extract components by weight. In one example, multiple short-path distillation units may be aligned is series to incrementally separate extract components by weight.

A cannabis oil extraction apparatus may include an extraction unit, condenser, winterization unit, micron filter, preheater, short-path distillation unit, and condenser. The extraction unit may utilize cellular disruption in a food grade solvent to extract cannabis oil from plant material. The short-path distillation unit may utilize molecular distillation. The short-path distillation unit may include a recirculation loop for multiple passes through the short-path distillation unit to separate extract components by weight. In one example, multiple short-path distillation units may be aligned is series to incrementally separate extract components by weight.

A distillation head of embodiments of the disclosed technology has a vertical tube which extends to and partially through a fraction collector. The vertical tube is mostly filled with a distillation key which is attached to a top side of the fraction collector and extends downwards through the vertical tube without coming into contact with same. A class housing or shell surrounds the vertical tube, which in turn, surrounds the distillation key or, at least a majority of each while the vertical tube extends past an area circumscribed by the shell and the distillation key extends past an area circumscribed by the vertical tube in some embodiments of the disclosed technology.

A distillation head of embodiments of the disclosed technology has a vertical tube which extends to and partially through a fraction collector. The vertical tube is mostly filled with a distillation key which is attached to a top side of the fraction collector and extends downwards through the vertical tube without coming into contact with same. A class housing or shell surrounds the vertical tube, which in turn, surrounds the distillation key or, at least a majority of each while the vertical tube extends past an area circumscribed by the shell and the distillation key extends past an area circumscribed by the vertical tube in some embodiments of the disclosed technology.