A method of separating an organic solvent which may easily separate and recover an organic solvent from a mixed solution containing the organic solvent, and an organic solvent separation system capable of performing the same are disclosed herein. In some embodiments, the method includes introducing a first mixed solution into a first distillation column to recover an organic solvent and discharge a first fraction containing an unrecovered organic solvent and a high boiling point compound A to a bottom of the column, introducing a second mixed solution into a second distillation column to recover organic solvent and discharge a second fraction containing an unrecovered organic solvent and a high boiling point compound B, and introducing the first fraction and the second fraction into a third distillation column to recover an organic solvent-rich fraction and a high boiling point compound-rich fraction.

A method for producing a high-purity hydrogen chloride gas comprises performing a purification process that includes the steps 1) to 3) below on a byproduct hydrogen chloride gas: 1) a crude hydrochloric acid generation step of allowing water to absorb the byproduct hydrogen chloride gas; 2) a volatile organic impurity-removed hydrochloric acid generation step of bringing the crude hydrochloric acid obtained in the step 1) into contact with an inert gas at a liquid temperature of 20 to 45° C. to dissipate volatile organic impurities; and 3) a high-purity hydrogen chloride gas generation step of supplying the volatile organic impurity-removed hydrochloric acid obtained in the step 2) to a distillation column and performing distillation under conditions of a column bottom temperature of higher than 60° C. and 108° C. or lower and a column top temperature of 60° C. or lower to distill out a high-purity hydrogen chloride gas.

A method for producing a high-purity hydrogen chloride gas comprises performing a purification process that includes the steps 1) to 3) below on a byproduct hydrogen chloride gas: 1) a crude hydrochloric acid generation step of allowing water to absorb the byproduct hydrogen chloride gas; 2) a volatile organic impurity-removed hydrochloric acid generation step of bringing the crude hydrochloric acid obtained in the step 1) into contact with an inert gas at a liquid temperature of 20 to 45° C. to dissipate volatile organic impurities; and 3) a high-purity hydrogen chloride gas generation step of supplying the volatile organic impurity-removed hydrochloric acid obtained in the step 2) to a distillation column and performing distillation under conditions of a column bottom temperature of higher than 60° C. and 108° C. or lower and a column top temperature of 60° C. or lower to distill out a high-purity hydrogen chloride gas.

An apparatus and method for purification and recovery of an organic liquid. The apparatus includes a distillation kettle and a receiver tank connected by a distillation pipe, and a vacuum pump, wherein a vacuum storage tank is arranged between the receiver tank and the vacuum pump; the vacuum storage tank is connected to the receiver tank by a vacuum regulating pipe, a first vacuum regulating valve being arranged on the vacuum regulating pipe; and the vacuum storage tank is connected to the vacuum pump by an evacuation pipe, a second vacuum regulating valve being arranged on the evacuation pipe. By arranging a vacuum storage tank between the receiver tank and the vacuum pump, the vacuum degree in the receiver tank is regulated by the vacuum storage tank, such that the organic liquid is recovered in a sealed environment under reduced pressure.

A process for hydrocracking a petroleum feedstock involves: (a) hydrocracking the feedstock to obtain a hydrocracked effluent; (b) liquid/gas separation of the effluent to obtain a gaseous effluent and a liquid effluent; (c) fractionating the liquid effluent at a pressure P1, producing a first distillate and a first residue, (d) recycling a first portion of the first residue to hydrocracking, (e) rectifying a second portion of the first residue at a pressure P2 lower than or equal to the pressure P1, to obtain a secondary distillate, a secondary residue and a vapor stream, (f) purging a portion of the secondary residue, and (g) recycling all or part of the secondary distillate to hydrocracking.

A process for hydrocracking a petroleum feedstock involves: (a) hydrocracking the feedstock to obtain a hydrocracked effluent; (b) liquid/gas separation of the effluent to obtain a gaseous effluent and a liquid effluent; (c) fractionating the liquid effluent at a pressure P1, producing a first distillate and a first residue, (d) recycling a first portion of the first residue to hydrocracking, (e) rectifying a second portion of the first residue at a pressure P2 lower than or equal to the pressure P1, to obtain a secondary distillate, a secondary residue and a vapor stream, (f) purging a portion of the secondary residue, and (g) recycling all or part of the secondary distillate to hydrocracking.

In some implementations, a control system may obtain historical data associated with usage of a distillation column during a historical time period. The control system may configure a prediction model to monitor the distillation column for a hazardous condition. The prediction model may be trained based on training data that is associated with occurrences of the hazardous condition. The control system may monitor, using the prediction model, the distillation column to determine a probability that the distillation column experiences the hazardous condition within a threshold time period. The prediction model may be configured to determine the probability based on measurements from a set of sensors of the distillation column. The control system may perform, based on the probability satisfying a probability threshold, an action associated with the distillation column to reduce a likelihood that the distillation column experiences the hazardous condition within the threshold time period.

Commercially beneficial carbon-containing fractions can be recovered from hydrothermal liquefaction reactions in various types of processors. Feedstock slurry from waste solids is placed into a pressurized processor where it is maintained at temperature and pressure for a predetermined period. On discharge from the processor the processed discharge is separated into liquid and solid fractions. Gaseous fractions including carbon dioxide can also be removed or off-taken from the processor. New molecular structures are created in this reaction, resulting in fractions including biogas, biofuels, biosolids and biocrude. Silica, phosphates, potash and low concentration nitrogen based fertilizer, along with carbonaceous material can also be recovered.

Commercially beneficial carbon-containing fractions can be recovered from hydrothermal liquefaction reactions in various types of processors. Feedstock slurry from waste solids is placed into a pressurized processor where it is maintained at temperature and pressure for a predetermined period. On discharge from the processor the processed discharge is separated into liquid and solid fractions. Gaseous fractions including carbon dioxide can also be removed or off-taken from the processor. New molecular structures are created in this reaction, resulting in fractions including biogas, biofuels, biosolids and biocrude. Silica, phosphates, potash and low concentration nitrogen based fertilizer, along with carbonaceous material can also be recovered.

An oil dehydrator, comprising; a vacuum chamber, a vacuum pump arranged at an upper end region of the vacuum chamber for establishing a negative pressure within the vacuum chamber and for fluid transportation of water and air out from the vacuum chamber through an outlet opening, and a pipe for fluid transportation of oil into and/or out from the vacuum chamber, where the pipe is connected to a lower end region of the vacuum chamber, wherein the vacuum chamber at the lower end region has at least one flow channel fluidly connecting the vacuum chamber and the pipe, wherein an orifice check valve is arranged between the vacuum chamber and the pipe for controlling the flow of oil into and out from the vacuum chamber through the at least one flow channel.