A system of interlocks for controlling flow of low temperature process streams in a manufacturing process through a cold box to equipment or piping not specified for such temperatures by opening and closing valves and starting and stopping pumps. At least one interlock affects streams heated in the cold box. At least one interlock affects the streams cooled in the cold box. The interlocks are activated by temperatures of process lines to prevent exposure of equipment and piping to low temperatures while preventing the shutdown of the cold box. An override controller including a predictive failure capability is also provided.

An apparatus and process for distillation of methanol, which may also be used in distillation of other products, such as ethanol. The present apparatus and process have the purpose of reducing the consumption of energy and of cooling water and/or electricity in a distillation process of crude intermediate products, comprising a pre-treatment stage, known as stabilizing stage, for the removal of the volatile components, and a concentration stage, including one or more columns for distillation.

The present system is for simultaneous recovery of purified water and dissolved solids from impure high TDS water (1) which is achieved in a single step and eliminates the use of external thermal energy for making the system significantly efficient. It eliminates the use of boiler, cooling tower that reduces the overall capital cost and continuous requirement of external thermal energy for making system efficient. The simultaneous recovery of the purified water and solids from high TDS input effluent reduce the energy intensity of the system. Said system provides a vacuum system as heat pump which enables the system to be self-sufficient in thermal energy requirements for evaporation process and reduces GHG emissions significantly.

The present system is for simultaneous recovery of purified water and dissolved solids from impure high TDS water (1) which is achieved in a single step and eliminates the use of external thermal energy for making the system significantly efficient. It eliminates the use of boiler, cooling tower that reduces the overall capital cost and continuous requirement of external thermal energy for making system efficient. The simultaneous recovery of the purified water and solids from high TDS input effluent reduce the energy intensity of the system. Said system provides a vacuum system as heat pump which enables the system to be self-sufficient in thermal energy requirements for evaporation process and reduces GHG emissions significantly.

The invention relates to a method for predicting flooding in a distillation column by machine learning including a constructing and training phase of a machine learning model obtained from previously collected data and from a set of sensors, an operational phase for predicting flooding(s), by collecting a current data flow until a buffer is filled, pre-processing data from the data buffer by predetermined cleansing and classification, synchronizing the data of the current set of clean and classified data, determining a value of a current variable representative of at least one current performance of the at least one distillation column, forming a current set of transformed data by calculating predetermined derivatives, and predicting the current state of said distillation column by applying said learning model to said current set of transformed data.

A purification system for nitrogen gas and xenon gas in water and a static isotopic analysis method thereof are provided. The system includes a sample container, a carbon dioxide ice cold trap, a gas delivery main pipe and a mass spectrometer for noble gas communicated sequentially. The gas delivery main pipe is provided with branch pipelines communicated with a cryo pump and a vacuum pump set respectively, the mass spectrometer for noble gas is communicated with the vacuum pump set, and the cryo pump adsorbs or releases nitrogen gas and/or xenon gas by setting different temperatures of the cryo pump. Inlet and outlet sides of the carbon dioxide ice cold trap are respectively provided with a first valve and a second valve. Fourth and fifth valves are respectively disposed between the gas delivery main pipe and the vacuum pump set, and between the gas delivery main pipe and the cryo pump.

An improved process for the recovery of high-purity ethylene-oxide water feed streams to EO purification and MEG reaction units when both are operating in EO plants that incorporate EO Stripper bypass technology, by installing a second lights stripper to exclusively degasify the diluted EO feed to the MEG reactor, thus permitting the use of additional bypassed (gasified) EO absorbate as the diluent and resulting in a substantial increase in the total amount of EO absorbate that can bypass the EO Stripper.

The invention relates to a process for the continuous production of acrylic acid, in the absence of organic solvent and in the absence of chemical treatment of the aldehydes, and without employing a dividing-wall column, from a gaseous reaction mixture comprising acrylic acid obtained by gas-phase oxidation of a precursor of acrylic acid.

Provided is a method for purifying a waste solvent by removing carbon dioxide contained in a waste solvent derived from supercritical waste liquid generated after supercritical drying by a decompression process, and removing ammonia by a multi-stage distillation process to obtain a solvent of high purity, which can be reused in producing silica aerogel or a silica aerogel blanket.

A multi-stage flash reversal unit includes a housing; plural stages located inside the housing; an evaporation port that receives a water feed having a first temperature; a condensation port that outputs a concentrated water feed having a second temperature, which is lower than the first temperature; and a cooling unit that cools down the concentrated water feed.