The present invention discloses a gas distribution structure for a distillation column. Pressure drop adjusting column tray assemblies are arranged in a left mass transfer region and a right mass transfer region along a column height direction. The gas distribution structure includes column trays, gas-rising pipes, downcomers and cover hoods, wherein a gas flow meter is arranged in a pipe of any gas rising pipe; a feeding port and a liquid collecting port are formed in a column wall; a liquid flow meter, an adjusting valve and a circulation pump are arranged on a circulation pipeline between each liquid collecting port and each feeding port; technological parameters are transmitted to a control system; and the circulation pumps and the adjusting valves are controlled by the control system

The present disclosure provides a method for separating a feed stream in a distillation tower. The method may include forming solids in a controlled freeze zone section of the distillation tower; emitting radiation from a first radiation source in the controlled freeze zone section while the controlled freeze zone section forms no solids; detecting radiation emitted by the first radiation source as a first radiation level; detecting radiation emitted by the first radiation source as a second radiation level after detecting the first radiation level; and determining whether the solids adhered to at least one of on and around a first mechanical component included in the controlled freeze zone section based on the first radiation level and the second radiation level.

The invention provides a process for the separation of MEG and 1,2-BDO from a first mixture comprising MEG and 1,2-BDO, said process comprising the steps of: (i) providing said first mixture comprising MEG and 1,2-BDO as a feed to a distillation column; (ii) providing a feed comprising glycerol to the distillation column above the first mixture; (iii) operating the distillation column at a temperature in the range of from 50 to 250° C. and a pressure in the range of from 0.1 to 400 kPa; (iv) removing a stream comprising MEG and glycerol as a bottoms stream from the distillation column; and (v) (v) removing a stream comprising 1,2-BDO above the point at which the feed comprising glycerol is provided to the distillation column.

A mass transfer column comprising: a shell (12); an open internal region (14) defined by said shell; and a mass transfer assembly (16) positioned in the open internal region (14), the mass transfer assembly (16) comprising: a dividing wall (18) forming first and second sub-regions; one or more zones of mass transfer structures positioned in the first and second sub-regions (22 and 24); and a liquid flow divider (48) positioned above the dividing wall (18) for delivering a volumetric split of liquid to the first and second sub-regions. The liquid flow divider (48) may comprise a moveable weir (68) or a valve (180) in order the change the ratio of liquid flow between the two sub-regions.

A mass transfer column comprising: a shell (12); an open internal region (14) defined by said shell; and a mass transfer assembly (16) positioned in the open internal region (14), the mass transfer assembly (16) comprising: a dividing wall (18) forming first and second sub-regions; one or more zones of mass transfer structures positioned in the first and second sub-regions (22 and 24); and a liquid flow divider (48) positioned above the dividing wall (18) for delivering a volumetric split of liquid to the first and second sub-regions. The liquid flow divider (48) may comprise a moveable weir (68) or a valve (180) in order the change the ratio of liquid flow between the two sub-regions.

A mass transfer assembly has at least one dividing wall, zones of mass transfer structures on opposite sides of the dividing wall, and a vapor flow restrictor that is operable to vary the split of vapor ascending through the zones of mass transfer structures on the opposite sides of the dividing wall.

Embodiments of the invention are directed toward a novel pressurized vapor cycle for distilling liquids. In some embodiments of the invention, a liquid purification system is revealed, including the elements of an input for receiving untreated liquid, a vaporizer coupled to the input for transforming the liquid to vapor, a head chamber for collecting the vapor, a vapor pump with an internal drive shaft and an eccentric rotor with a rotatable housing for compressing vapor, and a condenser in communication with the vapor pump for transforming the compressed vapor into a distilled product. Other embodiments of the invention are directed toward heat management, and other process enhancements for making the system especially efficient.

Embodiments of the invention are directed toward a novel pressurized vapor cycle for distilling liquids. In some embodiments of the invention, a liquid purification system is revealed, including the elements of an input for receiving untreated liquid, a vaporizer coupled to the input for transforming the liquid to vapor, a head chamber for collecting the vapor, a vapor pump with an internal drive shaft and an eccentric rotor with a rotatable housing for compressing vapor, and a condenser in communication with the vapor pump for transforming the compressed vapor into a distilled product. Other embodiments of the invention are directed toward heat management, and other process enhancements for making the system especially efficient.

A pot distillation system, in particular for whiskey, includes a distillation bubble with a base equipped to heat an alcoholic liquid, and a top removing alcohol vapors. The alcoholic liquid in the base is heated by a heating unit having a heat exchanger which is in thermal contact with the alcoholic liquid and heated by water vapor. A condenser having a cooling water circuit recirculating cooling water across the condenser condenses the alcohol vapor supplied from the top. The cooling water circuit includes a separator which removes water vapor from the cooling water circuit. The water vapor removed by the separator is pre-compressed in a mechanical compressor and supplied to an intake port of a steam jet pump which is driven by water vapor from a water vapor source and which further compresses the pre-compressed water vapor, and the steam jet pump supplying the further compressed water vapor to the heat exchanger for heating same.

A pot distillation system, in particular for whiskey, includes a distillation bubble with a base equipped to heat an alcoholic liquid, and a top removing alcohol vapors. The alcoholic liquid in the base is heated by a heating unit having a heat exchanger which is in thermal contact with the alcoholic liquid and heated by water vapor. A condenser having a cooling water circuit recirculating cooling water across the condenser condenses the alcohol vapor supplied from the top. The cooling water circuit includes a separator which removes water vapor from the cooling water circuit. The water vapor removed by the separator is pre-compressed in a mechanical compressor and supplied to an intake port of a steam jet pump which is driven by water vapor from a water vapor source and which further compresses the pre-compressed water vapor, and the steam jet pump supplying the further compressed water vapor to the heat exchanger for heating same.