B01D9/0018

CONTINUOUS CRYSTALLIZATION OF CANNABINOIDS IN A STIRRED-TANK REACTOR
20220249976 · 2022-08-11 ·

Disclosed herein is a method for continuously preparing crystalline cannabinoid particles. The method includes preparing a cannabinoid-rich solution that comprises a first cannabinoid and inducing the cannabinoid-rich solution to a supersaturated state in which the first cannabinoid has a supersaturated concentration that is greater than a corresponding saturation concentration of the first cannabinoid. The method includes flowing the cannabinoid-rich solution into a continuous stirred-tank reactor (CSTR) in a continuous manner, mixing the cannabinoid-rich solution under turbulent mixing conditions to form a plurality of crystalline cannabinoid particles and a cannabinoid-depleted solution within the CSTR, and discharging the plurality of crystalline cannabinoid particles and the cannabinoid-depleted solution from the CSTR in a continuous manner to provide a flow rate through the CSTR. The method includes separating crystalline cannabinoid particles from the plurality of crystalline cannabinoid particles and the cannabinoid-depleted solution in a continuous manner.

MINERAL RECOVERY FROM CONCENTRATED BRINES
20220249983 · 2022-08-11 · ·

The present disclosure is directed to a new and improved separation process that isolates individual minerals from brines containing a mixture of minerals. The brines may be derived from seawater, brackish water, oilfield brines, solution mining, mine run-off, and other sources. Typically, the minerals are recovered as chlorides using a variety of processing steps including evaporation, centrifugation, elutriation, filtration, electrocogulation, crystallization, adsorption, and chromatography.

Method for the Production of Lithium Carbonate
20220289584 · 2022-09-15 ·

A process for the production of lithium carbonate from an aqueous salt solution at least containing lithium ions, chloride ions and calcium ions; the aqueous salt solution with a lithium content of at least 0.005% by weight and a maximum 0.2% by weight is condensed in a first evaporation step at a temperature between 40° C. and 160° C. until a concentrate I with a water content of ≤70% by weight and >60% by weight is formed. In a second evaporation step, the concentrate I is evaporated at a temperature between 60° C. and 180° C. until a concentrate II with a water content of ≤60% by weight is formed. In a Li concentration step, the lithium content is raised to at least 0.14% by heating the concentrate II to a temperature of at least 60° C. and thus a lithium-rich concentrate III and a residue III are formed.

PROCESS FOR PRODUCING SALT FROM WASTE AQUEOUS STREAMS OF ORGANIC PEROXIDES PRODUCTION

Process for producing a salt comprising NaCl and/or KCl from the aqueous effluents from one or more organic peroxide production processes, said process comprising the following steps (a) ensuring the pH of the aqueous effluents to be in the range from about 1-5, (b) separating the effluents in a liquid organic layer and an aqueous layer, (c) removing the organic layer, (d) raising the pH of the aqueous layer to a value in the range from about 6-14, and (e) crystallizing the salt from the aqueous layer having a pH in the range from about 6-14.

Method for Bleaching Sugar With Effluent Recycling
20220098684 · 2022-03-31 ·

The invention relates to a method for treating sugar comprising: placing a coloured sugar juice in contact with an ion exchange resin so as to charge the resin with colouring agents and to collect a bleached sugar juice; regenerating the colouring-charged resin, comprising: placing the charged resin in contact with a regeneration brine comprising a chloride salt; and collecting a regeneration effluent, the regeneration effluent comprising at least three fractions A, B and C, fraction A having a higher concentration of chloride salt than fractions B and C; and recycling the regeneration effluent, comprising: nanofiltration of fraction A of the regeneration effluent in order to obtain a first permeate and a first retentate; diafiltration of the first retentate, said diafiltration comprising: dilution of the first retentate with the fraction B of the regeneration effluent; nanofiltration of the mixture in order to obtain a second permeate and a second retentate; mixing of the first permeate with the second permeate and fraction C of the regeneration effluent,

METHOD AND SYSTEM FOR EXTRACTING LONG CHAIN DICARBOXYLIC ACID

The present disclosure provides a system for extracting long chain dicarboxylic acid, the system comprising: a primary membrane filtration unit, a first crystallization unit, a first separation unit, a first dissolution tank, a secondary membrane filtration unit, a second separation unit, a second crystallization unit and a third separation unit. By the system for extracting long chain dicarboxylic acid of an embodiment of the present invention, the resulted long chain dicarboxylic acid product has a high purity, very low and even no residual alkane residue, and organic solvent-free.

PURIFICATION AND SEPARATION TECHNIQUES FOR CANNABINOIDS
20210268402 · 2021-09-02 ·

This disclosure relates to techniques and methods to isolate and purify cannabinoids, such as CBDV, CBD, CBC, THCV, THC, CBN, CBG, CBDA, THCA, or CBGA. Evaporation and sonicating techniques are used to isolate and purify cannabinoids, such as CBDV, CBD, CBC, THCV, THC, CBN, CBG, CBDA, THCA, or CBGA. The resulting compounds find further use within the devices and compositions described herein as well as for preparative and analytical methods.

Method for Extracting Lithium from Salt Lake Brine and Simultaneously Preparing Aluminum Hydroxide
20210221697 · 2021-07-22 ·

The present disclosure relates to a method for extracting lithium from salt lake brine and simultaneously preparing aluminum hydroxide. This method includes: a. adding an aluminum salt to the brine to obtain a mixed salt solution A, adding an alkali solution to the mixed salt solution A for co-precipitation reaction, then subjecting to crystallization reaction and solid-liquid separation at the end of the reaction to obtain magnesium-aluminum hydrotalcite solid product and lithium-containing brine, wherein in step a, the alkali solution is an alkali solution free of carbonate ion; b. evaporating and concentrating the lithium-containing brine to obtain a lithium-rich brine, adding an aluminum salt to the lithium-rich brine to obtain a mixed salt solution B, adding an alkali solution dropwise to the mixed salt solution B to perform a co-precipitation reaction and solid-liquid separation after the end of the reaction to obtain a lithium-containing liquid and a lithium-containing layered material filter cake, wherein in step b, the alkali solution is an alkali solution free of carbonate ion; c. dispersing the lithium-containing layered material filter cake in deionized water to form a suspension slurry, then adjusting the pH value of the suspension slurry so as to carry out a lithium deintercalation reaction; d. filtering the slurry obtained after the lithium deintercalation reaction to obtain a lithium-containing solution and aluminum hydroxide filter cake; e. washing the aluminum hydroxide filter cake with deionized water and drying to obtain aluminum hydroxide solid.

CANNABIS PRODUCTION SYSTEMS AND METHODS
20210251157 · 2021-08-19 ·

A vertically-integrated Cannabis-related product production method is described, the method comprises, producing a distilled cannabinoid and/or a crystallized cannabinoid from Cannabis plants, comprising: in a farming system, growing the Cannabis plants, the Cannabis plants comprise a cannabinoid; in an extraction system, extracting the cannabinoid from the Cannabis plants; in a purification system, purifying the cannabinoid to produce a purified cannabinoid; and in a distillation and/or a crystallization system, distilling and/or crystallizing the purified cannabinoid to produce the distilled cannabinoid and/or the crystallized cannabinoid. Various ways to purify, distill, and process the cannabinoids are described. An insect pest management system may be integrated with the farming system to grow the Cannabis plants in the presence of predatory mites which feed on insects and/or spider mites.

SPRAY-DRIED 3-FUCOSYLLACTOSE
20210171992 · 2021-06-10 ·

Disclosed is a method for the manufacture of a spray-dried powder consisting essentially of 3-fucosyllactose, the spray-dried powder, its use for the manufacture of nutritional compositions, and nutritional compositions containing the spray-dried powder.