B01D9/0036

Continuous crystallization of cannabinoids in a stirred-tank reactor

Disclosed herein is a method for continuously preparing crystalline cannabinoid particles. The method includes preparing a cannabinoid-rich solution that comprises a first cannabinoid and inducing the cannabinoid-rich solution to a supersaturated state in which the first cannabinoid has a supersaturated concentration that is greater than a corresponding saturation concentration of the first cannabinoid. The method includes flowing the cannabinoid-rich solution into a continuous stirred-tank reactor (CSTR) in a continuous manner, mixing the cannabinoid-rich solution under turbulent mixing conditions to form a plurality of crystalline cannabinoid particles and a cannabinoid-depleted solution within the CSTR, and discharging the plurality of crystalline cannabinoid particles and the cannabinoid-depleted solution from the CSTR in a continuous manner to provide a flow rate through the CSTR. The method includes separating crystalline cannabinoid particles from the plurality of crystalline cannabinoid particles and the cannabinoid-depleted solution in a continuous manner.

Systems and methods to recover value-added materials from gypsum

Disclosed herein are systems and methods from processing flue gas desulfurization (FGD) gypsum feedstock and ash feedstocks, either separately or together. FGD gypsum conversion comprises reacting FGD gypsum (calcium sulfate) feedstock or phosphogypsum, in either batch or continuous mode, with ammonium carbonate reagent to produce commercial products comprising ammonium sulfate and calcium carbonate. A process to separate the impurities and convert the calcium carbonate to a pure precipitated calcium carbonate is disclosed. These impurities include a concentrate of valuable Rare Earth Elements, and radioactive thorium and uranium. A process to convert calcium sulfite to calcium sulfate using oxygen and a catalyst is also disclosed. Ash conversion comprises a leach process followed by a sequential precipitation process to selectively precipitate products at predetermined pHs resulting in metal hydroxides which may be converted to oxides or carbonates. The processes may be controlled by use of one or more processors.

METHOD OF PREPARING ALUMINA
20240059577 · 2024-02-22 ·

A process for preparing high purity alumina from aluminium-bearing materials is provided. The process digesting an aluminium bearing material to provide an aluminium chloride liquor, a first crystallisation vessel for crystallising aluminium chloride hexahydrate solids from the aluminium chloride liquor, optionally one or more subsequent crystallisation vessels for dissolving and recrystallising the aluminium chloride hexahydrate solids, and thermal treatment means for thermally treating the aluminium chloride hexahydrate solids to provide high purity alumina.

SODIUM HYPOCHLORITE PENTAHYDRATE CRYSTAL GRAINS HAVING HIGH BULK DENSITY AND METHOD FOR PRODUCING SAME

Provided are sodium hypochlorite pentahydrate crystal gains that have high bulk density and increase bulk density in a container and improve transport efficiency by controlling the shape of the sodium hypochlorite pentahydrate crystals, and a production method thereof.

As a result of stirring or circulating by pump an aqueous solution of sodium hypochlorite pentahydrate in a crystallization tank in a crystallization step, sodium hypochlorite pentahydrate crystal grains are obtained having an average aspect ratio of 2.5 or less.

Method for Resolution of Baclofen Salts

The invention relates to the field of resolution of chiral compounds existing in the form of two optical antipodes (enantiomers), such as Baclofen. More particularly, the invention relates to the production of the pure enantiomer (R)() Baclofen, of chemical nomenclature (R)-4-amino-3-(4-chlorophenyl)-butanoic acid, and the hydrogen maleate salt thereof. More specifically, the invention relates to the resolution of hydrogen maleate salts of racemic Baclofen by preferential crystallisation and particularly by the AS3PC method (auto-seeded and programmed polythermal preferential crystallisation).

MICROFLUIDIC DEVICES FOR INVESTIGATING CRYSTALLIZATION
20190346347 · 2019-11-14 ·

Microfluidic devices and methods for investigating crystallization and/or for controlling a reaction or a phase transition are disclosed. In one embodiment, the microfluidic device includes a reservoir layer; a membrane disposed on the reservoir layer; a wetting control layer disposed on the membrane; and a storage layer disposed on the wetting control layer, wherein the wetting control layer and the storage layer define a microfluidic channel comprising an upstream portion, a downstream portion, a first fluid path in communication with the upstream and the downstream portions, and a storage well positioned within the first fluid path, wherein the wetting control layer includes a fluid passageway in communication with the storage well and the membrane, and wherein the wetting control layer wets a first fluid introduced into the microfluidic channel, the first fluid comprising a hydrophilic, lipophilic, fluorophilic or gas phase as the continuous phase in the microfluidic channel.

Method for purifying ethylene carbonate through dynamic crystallization

The present invention relates to the technical field of chemical industry, and in particular to a method for purifying ethylene carbonate through dynamic crystallization, which includes the following steps: adding an ethylene carbonate-containing raw material into a cavity of a crystallization device under a condition of stirring for dynamic crystallization, wherein the crystallization device further includes a jacket attached and circumferentially disposed along the outer wall of the cavity, the jacket is provided with cooling water therein, a temperature of the cooling water is 1-2.5? C. lower than the temperature in the cavity until a granular ethylene carbonate crystal is generated. The present invention using a rake dryer as the crystallization device to realize dynamic crystallization at a certain rotating speed. The technical solution is simple to operate and short in processing cycle, which facilitates improvement in production efficiency and product quality and is suitable for industrial application.

SYSTEMS AND METHODS FOR SEPARATING SURFACE MATERIALS FROM A FLUID USING ACOUSTIC PRESSURE SHOCK WAVES
20190330082 · 2019-10-31 · ·

A method of separating material, such as foam, sludge, oil or grease, at a fluid's surface, by applying acoustic pressure shock waves to the material and the fluid's surface such that acoustic pressure shock waves are propagated in liquid medium of the fluid and in gas medium above the fluid surface.

SYSTEMS AND METHODS FOR ACTIVATING AND DEWATERING SLUDGE USING ACOUSTIC PRESSURE SHOCK WAVES
20190330083 · 2019-10-31 · ·

A method of activating and dewatering sludge through application of acoustic pressure shock waves to wastewater.

Membrane cleaning and desalination with a membrane using acoustic pressure shock waves
10457571 · 2019-10-29 · ·

Acoustic pressure shock waves are applied to a membrane in a fluid to prevent attachment of or dislodge biological or solid matter for membrane cleaning or desalination with a membrane.