A reaction assembly separating plant material from water includes a first annular filter element defining an axis. The first annular filter element is defined by an outer annular coil of flat wire and an optional second filter element is defined by an inner annular coil of flat wire, being generally helical in the axial direction. A cylindrically or frustoconical filter membrane is concentrically disposed between the first and second annular filter element. The filter membrane is porous having aperture size of less than a nano-particulate size of the plant material, but greater than a nano-particulate size of the water molecule. The second annular filter includes adjustable porosity for selectively preventing particles from reaching the filter membrane and selectively cleaning the membrane by reversed flow of water through the membrane. The assembly generates radial and distal flows and differential pressure forces, for use in high throughput industrial, agricultural and municipal facilities.

The present disclosure is related to the continuous liquid-liquid chromatographic separation of chemical species using multiple liquid phases and related systems and articles.

A method for separating aromatic hydrocarbons by an extractive distillation, comprising introducing a hydrocarbon mixture containing aromatic hydrocarbons into the middle of an extractive distillation column (8); introducing an extraction solvent into the upper part of the extractive distillation column; after an extractive distillation, a raffinate containing benzene is discharged from the top of the column, wherein the benzene content is 3-40% by mass, and sent to the lower part of the extraction column (10); the extraction solvent is introduced to the upper part of the extraction column for a liquid-liquid extraction; a raffinate liquid free of aromatic hydrocarbons is discharged from the top of the extraction column; a rich solvent containing benzene is discharged from the bottom of the column and enters the upper-middle part of the extractive distillation column; the rich solvent obtained at the bottom of the extractive distillation column is sent to the solvent recovery column to separate the aromatic hydrocarbons and the solvent. By combining an extractive distillation with a liquid-liquid extraction ingeniously, the method can achieve the separation of aromatic hydrocarbons with a high purity and a high recovery rate, and a significant decrease of the energy consumption in the extraction and separation process.

The invention relates to a system and a method for the processing of minerals containing the lanthanide series and the production of rare earth oxides, which allow a completely closed and continuous treatment of the different materials and desorbent agents involved in the process, thus improving the efficiency in the extraction and avoiding environmental risks associated. The method comprising the steps of: reception and conditioning of the raw material; desorption of valuable product through a plurality of mixing and reaction stages in which the raw material is contacted in countercurrent with a stream of desorbent solution; separation of fine solids; precipitation of secondary minerals through the use of a first reactive solution; precipitation of rare earth carbonates through the use of a second reactive solution; and drying and roasting of the rare earth carbonates to obtain rare earth oxides; wherein the method further comprises a secondary process that allows further processing of the residual mineral, and a dewatering and washing step wherein the residual mineral from the desorption step is washed and a lanthanide-containing liquid is recovered.

A countercurrent extraction device for spinning includes an extraction box containing extraction liquid, and the extraction box is provided with a plurality of partition assemblies, and the extraction box is partitioned into a plurality of extraction chambers by the partition assemblies; each of the partition assemblies includes a first plate and a second plate, two ends of the first plate are fixedly connected to two sidewalls of the extraction box, and a first gap is provided between a lower edge of the first plate and a bottom wall of the extraction box; a lower edge of the second plate is connected to the bottom wall of the extraction box, a second gap is provided between a top edge of the second plate and a top wall of the extraction box, and heights of a plurality of second plates are gradually decreased along a flow direction of the extraction liquid.

The present invention relates to a method for the chlorination of a sucrose-6-acylate to produce a 4,1,6-trichloro-4,1,6-trideoxy-galactosucrose-6-acylate wherein said method includes steps of: (i) combining the sucrose-6-acylate with a chlorinating agent in a reaction vehicle comprising a tertiary amide to afford a mixture; (ii) heating said mixture for a heating period in order to provide chlorination of sucrose-6-acylate at the 4,1 and 6 positions thereof; and (iii) quenching the product stream of (ii) to produce a 4,1,6-trichloro-4,1,6-trideoxy-galactosucrose-6-acylate;
wherein before said quenching, a portion of said tertiary amide is removed by extraction into a solvent in which said tertiary amide is at least partially soluble.

An apparatus for enhancing phase contact and chemical reactions is provided. The apparatus comprises at least one high-turbulence mixing stage and at least one high-shear-stress and high-cavitation stage. The stages are adapted to cause an increase in relative sliding speeds of phases involved in a multiphase flow passing through the stages. The high-shear-stress and high-cavitation stage comprises a rotor having radial teeth housed in a cavitation chamber surrounded by a stator having radial teeth. The facing surfaces of the radial teeth have a parabolic profile in circumferential direction. For each tooth, the parabolic profile lies along a curve of a parabola of which a vertex is arranged at a rear edge of the tooth, with respect to a direction of rotation of the rotor, and along a radius extending from the rear edge to a center of the rotor. The focus of the parabola is also located on the radius.

An extractor suitable for using a solvent to separate a compound from a solid or semisolid substance containing the compound. The extractor includes a conveying assembly having an inclined conveyor for receiving the substance from a substance inlet and moving the substance through the solvent, an inclined upper surface associated with the first conveyor and an inclined lower surface associated with the first conveyor. The conveyor is configured to move the substance downward through the solvent along the upper surface toward a lower end of the conveyor and upward through the solvent along the lower surface toward an upper end of the conveyor.

Process for isolating pure 1,3-butadiene from a crude C.sub.4 fraction by extractive distillation using a selective solvent, wherein (a) the crude C.sub.4 fraction is introduced into a predistillation column, a first low boiler fraction comprising C.sub.3-hydrocarbons is taken off as overhead stream, a gaseous C.sub.4 fraction is taken off as side stream and a first high boiler fraction is taken off as bottom stream, (b) the gaseous C.sub.4 fraction is brought into contact with a selective solvent in at least one extraction column, giving an overhead fraction comprising butanes and butenes and a bottom fraction comprising 1,3-butadiene and selective solvent, (c) crude 1,3-butadiene is desorbed from the bottom fraction in at least one stripping column, with a stripped selective solvent being obtained and the stripped selective solvent being recirculated to the extraction column, and (d) at least part of the crude 1-3-butadiene is fed to a pure distillation column and a second high boiler fraction is separated off and a gaseous purge stream is taken off. Gaseous purge streams from the columns which are necessary in order to keep the concentration of molecular oxygen below a predetermined concentration limit are consolidated with output streams which are in any case provided for discharging other components in the process. The recirculation of the second high boiler fraction to a lower section of the predistillation column creates a further degree of freedom in operation of the pure distillation column.

The specification provides methods for extracting juice, anthocyanin, pectin, proanthocyanidin, and/or other phenolic compounds, from fruit material such as cranberry fruit, presscake, and/or pomace, through a sequential extraction procedure.