B01D11/04

Conduit contactor and method of using the same

A conduit contactor for conducting chemical reactions or chemical extractions between immiscible liquids includes a conduit having a hollow interior, a first open end, and a second open end opposite the first open end; a separator in fluid communication with and proximate the second open end; and a plurality of fibers disposed within the conduit. A total surface area of the fibers per volume of the hollow interior of the conduit is from 100 cm.sup.2/cm.sup.3 to 490 cm.sup.2/cm.sup.3.

Technetium 99m isolation system and technetium 99m isolation method

An initial introduction control part introduces an aqueous solution containing molybdenum 99 and technetium 99m, and an organic solvent being capable of dissolving the technetium 99m into an extraction tank. A micro-mixing control part micro-mixes the aqueous solution and the organic solvent by heating and stirring a mixed solution of the aqueous solution and the organic solvent introduced into the extraction tank with a heater, while applying ultrasonic to the mixed solution. A separation control part separates the mixed solution micro-mixed into two phases of aqueous solution and an organic solvent. A taking-out introduction control part passes the organic solvent separated into two phases through an adsorption column be capable of adsorbing molybdenum 99 and introduces the organic solvent into an evaporation elution tank. An evaporation control part evaporates the organic solvent and leaves residue by reducing pressure inside the evaporation elution tank and heating the organic solvent introduced into the evaporation elution tank with a heater, while applying ultrasonic to the organic solvent. An elution control part introduces physiological saline solution into the residue and elutes technetium 99m into the physiological saline solution from the residue.

Method and apparatus for continuous post-treatment of benzotriazole synthetic fluid
20220194905 · 2022-06-23 ·

The present invention belongs to the technical field of petrochemical engineering, and relates to a method for continuous post-treatment of benzotriazole (abbreviated as BTA) synthetic fluid. In particular, the present invention relates to a method for synthesizing BTA, including subjecting the BTA synthetic fluid to post-treatment steps of continuous acidification, water washing, extraction, back-extraction, dehydration, and distillation and the like. The method utilizes the difference in solubility of the BTA in water under different pHs to achieve separation by extraction without consuming a large amount of evaporation energy. The present invention is easy to operate, has little environmental pollution, high economic efficiency and low energy consumption, and is easily industrialized.

METHOD FOR RESOLVING OPTICAL ISOMER BY USING SUPERCRITICAL FLUID EXTRACTION TECHNOLOGY
20220195471 · 2022-06-23 ·

Provided is a method for resolving an optical isomer from a racemate by using supercritical fluid extraction technology. The method is mainly applied to the separation of a product obtained after enzymatic resolution. Taking a preparation process of D-pantolactone as an example, the key point is to separate D-pantolactone and L-pantolactone from an enzymatic resolution liquid by means of supercritical fluid extraction.

Catalytic Carbon Fiber Contactor
20220193647 · 2022-06-23 · ·

A fiber bundle contactor may include: a flow path defined by a conduit; a catalytic carbon fiber bundle disposed in the conduit; and an inlet allowing fluid flow into the flow path. A method may include: introducing into vessel a hydrocarbon comprising mercaptan sulfur, an aqueous caustic solution, and an oxidizer; reacting at least a portion of the mercaptan sulfur and the aqueous caustic solution to produce a mercaptide; and reacting the mercaptide and the oxidizer in the presence of a catalytic carbon fiber bundle to produce a disulfide oil.

HIGH SHEAR MIXER
20220186171 · 2022-06-16 ·

Spent stillage remaining after the fermentation of a feedstock for ethanol production may be processed to recover, use, and/or recycle the constituent components of the stillage. Stillage may be mixed, heated, and held at a desired temperature for a period of time. The stillage may then be cooled and treated with an enzyme. The enzymatically treated stillage may be emulsified with oil and water, and then permitted to settle into discrete layers. Individual layers may then be processed. A system and method for separating stillage after the fermentation process of ethanol production has concluded are provided.

AN ALCOHOL RECOVERY SOLUTION, AND METHOD OF USE THEREFOR
20220185754 · 2022-06-16 ·

The present invention is directed to a composition for use in recovering an alcohol from an aqueous solution the composition comprising: a) a recovery solution comprising at least one tertiary amine containing compound and at least one enolisable carbonyl; and, b) an aqueous process solution comprising the alcohol, wherein the recovery solution and the aqueous process solution are in direct contact, not miscible and at least a portion of the alcohol migrates from the aqueous process solution into the recovery solution.

AUTOMATED GROUP SEPARATIONS OF COMPLEX MIXTURES WITH GEL FILTRATION PIPETTE TIPS
20220184525 · 2022-06-16 ·

A device for automated or manual group separations of complex biological mixtures and methods of use are described. The device is a gel filtration pipette tip having a size exclusion media therein and held in place by a filter at the distal end of the pipette tip and an optional removable or pierceable barrier at the proximal end of the pipette tip. The size exclusion media is wetted by aspirating a solvent from the bottom of the pipette tip and equilibrating the solvent with the size exclusion media. The solvent is then allowed to gravity drain from the pipette tip, allowing the size exclusion media to settle and reproducibly pack into a homogenous gel. Gel filtration separations can then be performed with the gelled size exclusion media.

Method of inhibiting degradation of DSX extractant by auxiliary means

A method of inhibiting degradation of an extractant by utilizing several auxiliary means in the DSX process: includes (a) preparing adjustment of the concentration of an extractant of a DSX solvent to a certain range; (b) extracting a metal contained in a pregnant leached solution by adjusting the ratio of the extractant and the diluent in the DSX solvent to a certain range; (c) measuring the pH of the aqueous phase solution by separating mixture into the aqueous phase solution and the organic phase solvent using a settler after step of extracting; (d) controlling the pH by adding soda ash (Na.sub.2CO.sub.3) so as to maintain the pH of the aqueous phase solution to be 3 to 7; and (e) scrubbing with scrubbing solution having a zinc concentration of 2 to 20 g/L by zinc sulfate (ZnSO.sub.4) to remove the manganese from the organic phase solvent containing the extracted metal.

Method of inhibiting degradation of extractant by anhydrous environment avoiding and metal stripping

Provided is a method of inhibiting degradation of an extractant by an anhydrous environment avoiding and metal stripping, the method including the steps of: (a) stopping the addition of soda ash (Na.sub.2CO.sub.3) to an extracting reaction tank; (b) starting solution recirculation and stopping solvent recirculation of a settler; (c) supplying a solvent from a loaded organic tank to a scrubbing reaction tank, in which the scrubbing reaction tank, stripping reaction tank and extracting reaction tank are connected for circulation and operating stirrers of the scrubbing reaction tank, stripping reaction tank and extracting reaction tank; (d) supplying a sulfuric acid solution having a controlled concentration with a diluting solution to the stripping reaction tank; (e) transferring the solvents of the settler, the loaded organic tank and all the pipes to the scrubbing reaction tank; and (f) stopping the step (e) and initiating solvent recirculation.