The disclosure is directed to a method for recovering products from a fermentation broth. The disclosure relates to the use of extractive distillation and/or dehydration to recover products which have close boiling points, such as ethanol and isopropanol, from a fermentation broth. In an embodiment, the recovery of product is completed in a manner that minimizes stress on the microbial biomass, such that it remains viable, at least in part, and may be recycled and reused in the fermentation process, which may result in increased efficiency in the fermentation process. The extractive distillation vessel and/or dehydration reactor may be used downstream of a distillation vessel. To minimize stress on the microbial biomass the distillation vessel may be under vacuum. The extractive distillation vessel may be used alongside a separation vessel such that the separation vessel is capable of recycling extractive distillation agent.

Described is a method for the production of substantially spherical calcium phosphate particles that involves subjecting a composition comprising calcium phosphate to dual asymmetric centrifugation (DAC). Also described are products of the method.

Described is a method for the production of substantially spherical calcium phosphate particles that involves subjecting a composition comprising calcium phosphate to dual asymmetric centrifugation (DAC). Also described are products of the method.

In the coating apparatus for granular bodies is disposed a rotatable hollow cylindrical drum in which there is an introduction apparatus for granular bodies and at least one movable separating element therein, with which a cycle zone can be partly separated from a downstream cycle zone and a movement of the at least one separating element that leads to release is achievable. An interior of the drum is divided into at least one cycle zone and a further cycle zone. A spray apparatus is disposed in one cycle zone, and an outlet in a cycle zone arranged downstream. A separating element is movable from a closed position into an open position. A separating element has a clear space above the closed subregion and an opening between one cycle zone and a cycle zone arranged thereafter, through which granular bodies can pass.

In the coating apparatus for granular bodies is disposed a rotatable hollow cylindrical drum in which there is an introduction apparatus for granular bodies and at least one movable separating element therein, with which a cycle zone can be partly separated from a downstream cycle zone and a movement of the at least one separating element that leads to release is achievable. An interior of the drum is divided into at least one cycle zone and a further cycle zone. A spray apparatus is disposed in one cycle zone, and an outlet in a cycle zone arranged downstream. A separating element is movable from a closed position into an open position. A separating element has a clear space above the closed subregion and an opening between one cycle zone and a cycle zone arranged thereafter, through which granular bodies can pass.

A method is described for preparing a sorbent including the steps of: (i) mixing together a particulate copper sulphide material, a particulate support material and one or more binders, (ii) shaping the mixture, and (iii) drying the shaped mixture to form a dried sorbent.

A method is described for preparing a sorbent including the steps of: (i) mixing together a particulate copper sulphide material, a particulate support material and one or more binders, (ii) shaping the mixture, and (iii) drying the shaped mixture to form a dried sorbent.

An apparatus for coating pharmaceutical particles such as drug dosage forms or pellets is provided which includes a drum assembly mounted for rotation about a cylindrical axis of the drum and which includes an outer drum section and an inner perforated drum section mounted concentrically on an interior of the outer drum section such that an annular chamber is formed between the perforated inner drum section and the outer drum section. Two or more baffle plates are attached between an outer surface of the inner perforated drum and an inner surface of the outer drum which are configured to act as baffles to restrain or regulate the flow of air which define two or more compartments depending on the number of baffle plates. One end of the drum assembly includes an end plate with a central aperture for use in loading pellets into the drum and provide access to coating constituents that are pumped into the drum interior during the coating process. An air distribution plate is attached at the other end of the drum and has air flow passageways and is interfaced with an air introduction plate having air inlet and outlet passageways. As the drum rotates the air flow passageways in the distribution plate alternately come into flow communication with the air inlet and outlet passageways in the air introduction plate thereby providing a flow path of air into the perforate inner drum and out of the drum assembly.

An apparatus for coating pharmaceutical particles such as drug dosage forms or pellets is provided which includes a drum assembly mounted for rotation about a cylindrical axis of the drum and which includes an outer drum section and an inner perforated drum section mounted concentrically on an interior of the outer drum section such that an annular chamber is formed between the perforated inner drum section and the outer drum section. Two or more baffle plates are attached between an outer surface of the inner perforated drum and an inner surface of the outer drum which are configured to act as baffles to restrain or regulate the flow of air which define two or more compartments depending on the number of baffle plates. One end of the drum assembly includes an end plate with a central aperture for use in loading pellets into the drum and provide access to coating constituents that are pumped into the drum interior during the coating process. An air distribution plate is attached at the other end of the drum and has air flow passageways and is interfaced with an air introduction plate having air inlet and outlet passageways. As the drum rotates the air flow passageways in the distribution plate alternately come into flow communication with the air inlet and outlet passageways in the air introduction plate thereby providing a flow path of air into the perforate inner drum and out of the drum assembly.

Methods and system for increasing the water solubility and availability of zinc in granular fertilizers using acid treatments. The treatment of granular fertilizers with an acidic solution increases an amount of water-soluble zinc, which in turn, increases the efficiency of zinc uptake and reduces the costs and equipment otherwise needed to mitigate zinc deficiencies.