A distillation apparatus for use in microwave-assisted pyrolysis includes a microwave, a pyrolysis reactor, a microwave-absorbent bed, and a condenser. The pyrolysis reactor is located within the microwave and configured to receive a liquid input stream and to output a vapor. The microwave-absorbent bed is located within the pyrolysis reactor that converts microwave energy provided by the microwave to thermal energy to initiate pyrolysis within the pyrolysis reactor, wherein the pyrolysis reactor provides a vapor output. The condenser is configured to receive the vapor output of the pyrolysis reactor and to cool and condense the vapor into a recoverable product.

The present invention provides a method and a system for preparing fuel using high-acid-value biological grease, which can be processed through triple deoxidization steps, i.e., thermal cracking deoxygenation-catalytic cracking deoxygenation-catalytic hydrodeoxygenation. By use of the method and system of the invention, the raw material of the high-acid-value biological grease can be gradually deoxidized to reduce the acid value and thereby prepare a clean fuel with equivalent fuel components as those obtained from crude oil refining or direct hydrodeoxygenation for biological grease.

A reactor for coating particles includes one or more motors, a rotary vacuum chamber configured to hold particles to be coated, wherein the rotary vacuum chamber is coupled to the motors, a controller configured to cause the motors to rotate the rotary vacuum chamber about an axial axis of the rotary vacuum chamber such that the particles undergo tumbling agitation, a vacuum port to exhaust gas from the rotary vacuum chamber, a paddle assembly including a rotatable drive shaft extending through the rotary vacuum chamber and coupled to the motors and at least one paddle extending radially from the drive shaft, such that rotation of the drive shaft by the motors orbits the paddle about the drive shaft in a second direction, and a chemical delivery system including a gas outlet on the paddle configured inject process gas into the particles.

Methods for creating nanostructured surface features on polymers and polymer composites involve application of low pressure during curing of solid polymer material from a solvent solution. The resulting nanoscale surface features significantly decrease bacterial growth on the surface. Polymer materials having the nanoscale structuring can be used in implantable medical devices to inhibit bacterial growth and infection.

Systems for manufacturing bulked continuous carpet filament from polymer, where the systems are configured for: (1) passing polymer flakes through a crystalliers; (2) melting the polymer to create a first single stream of polymer melt; (3) separating the first single stream of polymer melt into multiple streams of polymer melt; (4) exposing the multiple streams of polymer melt to a pressure of between about 0 millibars and about 25 millibars in a chamber; (5) recombining the multiple streams of polymer melt into a second single stream of polymer melt; and (6) providing the second single stream of polymer melt to one or more spinning machines that are configured to form the second single stream of polymer melt into bulked continuous carpet filament.

The present invention provides a highly effective method of removal of gases from the chemical reactor (01) by use of a suction unit employed near the inlet, outlet or both ends of the chemical reactor. The suction of entrapped air from the reaction mixture helps avoid fluctuation in the temperature or pressure requirement or formation of other by-products in the reaction mixture.

Provided is an integrated device for preparing magnesium hydride powder and a method for preparing magnesium hydride powder. The device comprises a heating chamber for heating a magnesium-based metal material to produce metal droplets; a powder-making chamber comprising an atomizing means used for atomizing the metal droplets which are then cooled to form a metal powder; and a reaction chamber used for performing a hydrogenation reaction on the metal powder to form the magnesium hydride powder. The device is an integrated structure monolithic with a simple structure and a convenient operation; and the entire process of preparing magnesium hydride powder can be completed in this single device and can realize automated control. The preparation method is simple and easy to operate and produces a product that has a moderate size, uniform particles, and excellent performance.

A graphene manufacturing device using Joule heating includes: a chamber having a space provided therein so as to synthesize graphene; and a first roller portion and a second roller portion disposed inside the chamber to be spaced from each other such that same support a catalyst metal penetrating the interior of the chamber and are supplied with an electric current for graphene synthesis, thereby Joule-heating the catalyst metal. In order to compensate for a temperature deviation of the catalyst metal passing between the first roller portion and the second roller portion, a first area of the catalyst metal, which is close to the first roller portion, and a second area of the catalyst metal, which is close to the second roller portion, are disposed to have movement paths facing each other.

Disclosed herein is a method and device for production of a new long-term storage-stable allotropic modification of oxygen, tetraoxygen O.sub.4, using a combination of known chemical reactions into one technological sequence, including chemical interaction of negative and positive oxidation state oxygen compounds. The method involves production of dioxygen difluoride by oxidation of molecular oxygen with fluorine, followed by the reaction of dioxygen difluoride with alkali metal peroxide, forming tetraoxygen O.sub.4. Tetraoxygen is stable in its liquid state up to a temperature of +40° C. and can be used for the oxidation of rocket fuel, long-term compact storage of oxygen, and many other purposes.

A system and a method for producing silicon from a SiO.sub.2-containing material that includes solid SiO.sub.2. The method uses a reaction vessel including a first section and a second section in fluid communication with said first section. The method includes: heating the SiO.sub.2-containing material that includes the solid SiO.sub.2 to a SiO.sub.2-containing material that includes liquid SiO.sub.2, at a sufficient temperature to convert the solid SiO.sub.2 into the liquid SiO.sub.2; converting, in the first section, the liquid SiO.sub.2 into gaseous SiO.sub.2 that flows to the second section by reducing the pressure in the reaction vessel to a subatmospheric pressure; and reducing, in the second section, the gaseous SiO.sub.2 into liquid silicon using a reducing gas. The reducing of the pressure is performed over a continuous range of interim pressure(s) sufficient to evaporate contaminants from the SiO.sub.2-containing material, and removing by vacuum, the one or more evaporated gaseous contaminants.