Disclosed is a hydrothermal synthesis device for continuously preparing an inorganic slurry using a hydrothermal method. The hydrothermal synthesis device includes a mixer to mix at least one precursor solution for preparing an inorganic material, injected via at least one supply tube, to prepare an intermediate slurry, a connection tube provided at a side of the mixer, continuously discharging the prepared intermediate slurry to a reactor, and having a hydrophobic coating on an inner surface of a portion thereof adjacent to the reactor, and the reactor performing hydrothermal reaction of the intermediate slurry supplied from the connection tube by receiving a liquid stream heated to supercritical or subcritical conditions using a heat exchanger and connected to the connection tube into which the intermediate slurry prepared from the mixer is introduced and to at least one injection tube into which the heated liquid stream is injected.

Disclosed is a hydrothermal synthesis device for continuously preparing an inorganic slurry using a hydrothermal method. The hydrothermal synthesis device includes a mixer to mix at least one precursor solution for preparing an inorganic material, injected via at least one supply tube, to prepare an intermediate slurry, a connection tube provided at a side of the mixer, continuously discharging the prepared intermediate slurry to a reactor, and having a hydrophobic coating on an inner surface of a portion thereof adjacent to the reactor, and the reactor performing hydrothermal reaction of the intermediate slurry supplied from the connection tube by receiving a liquid stream heated to supercritical or subcritical conditions using a heat exchanger and connected to the connection tube into which the intermediate slurry prepared from the mixer is introduced and to at least one injection tube into which the heated liquid stream is injected.

A vacuum chamber may include an ambient side and a vacuum side. The vacuum chamber may be configured to carry a feedthrough that may include a hollow tube, a first O-ring captured by a first recess within the hollow tube and a rod extending through the hollow tube. The outer circumference of the rod may be configured to contact an entirety of an inner circumference of the first O-ring. A vacuum fitting having an inner circumference may be fixedly secured to the hollow tube. The rod may be operable to be linearly movable within the hollow tube and may be rotatably movable about an axis within the hollow tube. An object may be secured to the rod and may be linearly and rotatably moved within the vacuum chamber.

A feedthrough for use in a vacuum chamber is provided and includes a hollow tube having a length, an inner circumference, and a first recess located within the inner circumference. The feedthrough also includes a first O-ring captured by the first recess within the hollow tube. The feedthrough further includes a rod extending through an entirety of the length of the hollow tube. An outer circumference of the rod is configured to contact an entirety of an inner circumference of the first O-ring, and a vacuum fitting is fixedly secured to the hollow tube.

A system for treatment of a biomass material, said system comprising: a first vessel (3) in which said biomass material is treated under a first pressure; a second vessel (5) in which said biomass material is received and held at a second pressure which is lower than the first pressure; a transporting pipe (7) connecting an outlet (9) of the first vessel (3) with an inlet (11) of the second vessel (5) for transporting the biomass material from the first vessel to the second vessel; and a valve (15; 15′; 15) arranged in said transporting pipe (7), said valve being configured for controlling the flow of biomass material and fluid in the transporting pipe (7), wherein said transporting pipe (7) is asymmetrically connected to an outlet (33′; 33) of said valve (15; 15′; 15) such that a generated jet stream of biomass material delivered out from the outlet (33′; 33) of the valve (15; 15′; 15) is received closer to a transporting pipe longitudinal central axis (A1) than if the outlet (33′; 33) of the valve (15; 15′; 15) and the transporting pipe (7) would have been connected symmetrically.

A bulk HPP container (10) includes a flexible body portion (12) having closed off ends (14), at least one of which is depicted as being recessed to enable the containers (10) to be positioned end-to-end in an efficient manner, for example, when placed into an HPP pressure vessel, such as a wire wound vessel. One or more openings are provided in the body portion of the container with n appropriate closure for pumpable product to enter and exit the container. In this regard, an inlet valve (16) or other type of closure may be located at the opening in one or both of the ends of the container. Also, one or more outlet valves (18) or other type of closure are located at an opening on the body portion (12) of the container for emptying the container, for example, after HPP. The body portion 12) is composed of sufficient flexural strength and sufficient flexural modulus to enable the container to reduce in volume by from 0 to at least 30% while being rigid enough for reuse over a desired number of HPP cycles.

An autoclave system comprises an autoclave vessel 210, for performing a leaching operation on sacrificial ceramic cores (not shown) and a storage vessel 220 for containing caustic leaching fluid 230. Interposed in a fluid flow path between the vessel 210 and the tank 220 is a heat exchange unit 240, comprising a body 250 containing a thermal exchange medium, in the form of water 260, and first and second thermal exchange conduits represented at 270 and 280. A thermal exchange medium inlet pipe 290a and a thermal exchange medium outlet pipe 290b are provided to the body so that the medium 260 can be replenished, preferably substantially continuously, to optimize thermal transfer efficiency.

An autoclave system comprises an autoclave vessel 210, for performing a leaching operation on sacrificial ceramic cores (not shown) and a storage vessel 220 for containing caustic leaching fluid 230. Interposed in a fluid flow path between the vessel 210 and the tank 220 is a heat exchange unit 240, comprising a body 250 containing a thermal exchange medium, in the form of water 260, and first and second thermal exchange conduits represented at 270 and 280. A thermal exchange medium inlet pipe 290a and a thermal exchange medium outlet pipe 290b are provided to the body so that the medium 260 can be replenished, preferably substantially continuously, to optimize thermal transfer efficiency.

The invention relates to a pressure vessel, having: a reaction chamber (2) as a pressure space for the initiation and/or facilitation of chemical and/or physical pressure reactions of samples (P) accommodated in the reaction chamber (2); a fluid inlet (20) with a feed valve (21) which is adjustable between an open position, for the feed of a fluid, preferably a flushing gas, into the reaction chamber (2), and a closed position, for stopping the feed of the fluid; a fluid outlet (30) with a discharge valve (31), which is adjustable between an open position, for the discharge of a fluid out of the reaction chamber (2), and a closed position, for stopping the discharge of the fluid out of the reaction chamber (2); and an oxygen sensor (33) for detecting an oxygen content in the reaction chamber (2). The pressure vessel (1) furthermore has a control device which is configured to control the feed valve (21) and the discharge valve (31) on the basis of the oxygen content detected by the oxygen sensor (33), such that the reaction chamber (2) is flushed via the feed and discharge valves (21, 31) situated in the open position, and at least the discharge valve (31) switches from the open position into the closed position as soon as a predetermined oxygen content is undershot. The invention also relates to a corresponding method.

The invention relates to a pressure vessel, having: a reaction chamber (2) as a pressure space for the initiation and/or facilitation of chemical and/or physical pressure reactions of samples (P) accommodated in the reaction chamber (2); a fluid inlet (20) with a feed valve (21) which is adjustable between an open position, for the feed of a fluid, preferably a flushing gas, into the reaction chamber (2), and a closed position, for stopping the feed of the fluid; a fluid outlet (30) with a discharge valve (31), which is adjustable between an open position, for the discharge of a fluid out of the reaction chamber (2), and a closed position, for stopping the discharge of the fluid out of the reaction chamber (2); and an oxygen sensor (33) for detecting an oxygen content in the reaction chamber (2). The pressure vessel (1) furthermore has a control device which is configured to control the feed valve (21) and the discharge valve (31) on the basis of the oxygen content detected by the oxygen sensor (33), such that the reaction chamber (2) is flushed via the feed and discharge valves (21, 31) situated in the open position, and at least the discharge valve (31) switches from the open position into the closed position as soon as a predetermined oxygen content is undershot. The invention also relates to a corresponding method.