Patent classifications
B01J3/04
Intermediate gas concentration-regulating piston pressure device for high-temperature autoclave and gas distribution method
A piston pressure device includes a gas concentration-regulating piston pressure device and a high temperature autoclave. In the gas concentration-regulating piston pressure device, the proportion and concentration of corrosive gases can be accurately adjusted, intermediate gases can be stored and filled into the high temperature autoclave according to experimental needs, and an actual corrosion process in oilfield is accurately simulated. Meanwhile, the corrosive gases can be supplemented in real time during the experiment, and dynamic gas distribution in a high-temperature high-pressure corrosion experiment process is realized. The present invention has the advantages as follows: the piston pressure device is resistant to high temperature and high pressure, corrosion-resistant, simple in structure and convenient to operate; the concentration and proportion of the corrosive gases are accurately controlled to be invariable in the high-temperature high-corrosion experiment process; and reliability of high-temperature high-pressure corrosive experimental results is increased.
Intermediate gas concentration-regulating piston pressure device for high-temperature autoclave and gas distribution method
A piston pressure device includes a gas concentration-regulating piston pressure device and a high temperature autoclave. In the gas concentration-regulating piston pressure device, the proportion and concentration of corrosive gases can be accurately adjusted, intermediate gases can be stored and filled into the high temperature autoclave according to experimental needs, and an actual corrosion process in oilfield is accurately simulated. Meanwhile, the corrosive gases can be supplemented in real time during the experiment, and dynamic gas distribution in a high-temperature high-pressure corrosion experiment process is realized. The present invention has the advantages as follows: the piston pressure device is resistant to high temperature and high pressure, corrosion-resistant, simple in structure and convenient to operate; the concentration and proportion of the corrosive gases are accurately controlled to be invariable in the high-temperature high-corrosion experiment process; and reliability of high-temperature high-pressure corrosive experimental results is increased.
Process and apparatus for urea production
There is provided a process and an apparatus for urea production in which preheating of raw material ammonia or heating in a medium-pressure decomposition step can be performed at a relatively low pressure while preventing decrease in an overall heat transfer coefficient. A process for urea production includes: a synthesis step of generating a urea synthesis solution; a high-pressure decomposition step of heating the urea synthesis solution to separate a gaseous mixture containing ammonia and carbon dioxide from the urea synthesis solution; a condensation step of condensing the gaseous mixture; a medium-low-pressure steam generation step of reducing a pressure of medium-pressure steam condensate obtained in the high-pressure decomposition step to a medium-low pressure to generate medium-low-pressure steam and medium-low-pressure steam condensate; and one or both of a medium-pressure decomposition step and an ammonia preheating step.
Process and apparatus for urea production
There is provided a process and an apparatus for urea production in which preheating of raw material ammonia or heating in a medium-pressure decomposition step can be performed at a relatively low pressure while preventing decrease in an overall heat transfer coefficient. A process for urea production includes: a synthesis step of generating a urea synthesis solution; a high-pressure decomposition step of heating the urea synthesis solution to separate a gaseous mixture containing ammonia and carbon dioxide from the urea synthesis solution; a condensation step of condensing the gaseous mixture; a medium-low-pressure steam generation step of reducing a pressure of medium-pressure steam condensate obtained in the high-pressure decomposition step to a medium-low pressure to generate medium-low-pressure steam and medium-low-pressure steam condensate; and one or both of a medium-pressure decomposition step and an ammonia preheating step.
Integrated waste conversion system and method
An entirely water-based, energy self-sufficient, integrated in-line waste management system is provided for comprehensive conversion of all organic fractions of municipal and wider community waste to fuels suitable for use in transportation, with all solid residues converted to high nutrition compost. The system is based on a combination of pre-treatment, involving alkaline hydrolysis and saponification; three-way separation of the pre-treated waste into different streams that are each directed to suitable further processing including fuel production; which includes biodiesel generation in a continuous-flow catalytic esterification unit, and anaerobic digestion to produce methane or other small molecule biofuel. Remaining solids are converted to compost in a quasi-continuous process.
Integrated waste conversion system and method
An entirely water-based, energy self-sufficient, integrated in-line waste management system is provided for comprehensive conversion of all organic fractions of municipal and wider community waste to fuels suitable for use in transportation, with all solid residues converted to high nutrition compost. The system is based on a combination of pre-treatment, involving alkaline hydrolysis and saponification; three-way separation of the pre-treated waste into different streams that are each directed to suitable further processing including fuel production; which includes biodiesel generation in a continuous-flow catalytic esterification unit, and anaerobic digestion to produce methane or other small molecule biofuel. Remaining solids are converted to compost in a quasi-continuous process.
Autoclave Reactor System Comprising an Agitator with Polycrystalline Diamond Bearings
An autoclave reactor having polycrystalline diamond bearings. The autoclave reactor can include a housing for containing at least one reaction material therein, a motor disposed within the housing, an agitator connected to the motor for stirring the at least one material within the housing, the agitator having a shaft connected to the motor at one end thereof, and at least one bearing disposed adjacent to the shaft or adjacent to the connection of the shaft to the motor, the at least one bearing being made of polycrystalline diamond. A process for making low density polyethylene (LDPE) can include introducing ethylene to the autoclave reactor disclosed herein and polymerizing the ethylene within a housing of the reactor to provide the low density polyethylene.
Autoclave Reactor System Comprising an Agitator with Polycrystalline Diamond Bearings
An autoclave reactor having polycrystalline diamond bearings. The autoclave reactor can include a housing for containing at least one reaction material therein, a motor disposed within the housing, an agitator connected to the motor for stirring the at least one material within the housing, the agitator having a shaft connected to the motor at one end thereof, and at least one bearing disposed adjacent to the shaft or adjacent to the connection of the shaft to the motor, the at least one bearing being made of polycrystalline diamond. A process for making low density polyethylene (LDPE) can include introducing ethylene to the autoclave reactor disclosed herein and polymerizing the ethylene within a housing of the reactor to provide the low density polyethylene.
THERMAL CONVERSION OF CBDA AND OTHER CARBOXYLIC CANNABINOIDS
This invention is for improving the manufacturing pharmaceutical grade CBD and other cannabinoids following current Good Manufacturing Practices (cGMP) of the US FDA for use in clinical trials for CNS and other indications by the NIH and other researchers. The major cannabinoids in marijuana (Cannabis) and hemp originate from Cannabigerolic Acid (CBGA) present in the biomass of the plant. Plant enzymes that are specific to different strains of biomass converts CBGA to different carboxylic acids of cannabinoids including Cannabidiolic Acid (CBDA) and Δ9-Tetrahydrocannabinolic Acid (Δ9-THCA). These are relatively stable in the growing and fresh-cut plants. These are converted by thermal decarboxylation to Cannabidiol (CBD) and Δ9-Tetrahydrocannabinol (Δ9-THC), carbon dioxide and water. Cannabinoids can be manufactured by first heating the Cannabis biomass to convert carboxylic acids prior to extraction and purification. Alternatively, and preferably because of manufacturing cost and product stability, the carboxylic acids can be first extracted and purified. They can be utilized in the carboxylic acid form or stored in a stable manner until converted to cannabinoids for use in medicine. This invention provides an efficient method for their conversion utilizing a high-pressure reactor under inert conditions.
THERMAL CONVERSION OF CBDA AND OTHER CARBOXYLIC CANNABINOIDS
This invention is for improving the manufacturing pharmaceutical grade CBD and other cannabinoids following current Good Manufacturing Practices (cGMP) of the US FDA for use in clinical trials for CNS and other indications by the NIH and other researchers. The major cannabinoids in marijuana (Cannabis) and hemp originate from Cannabigerolic Acid (CBGA) present in the biomass of the plant. Plant enzymes that are specific to different strains of biomass converts CBGA to different carboxylic acids of cannabinoids including Cannabidiolic Acid (CBDA) and Δ9-Tetrahydrocannabinolic Acid (Δ9-THCA). These are relatively stable in the growing and fresh-cut plants. These are converted by thermal decarboxylation to Cannabidiol (CBD) and Δ9-Tetrahydrocannabinol (Δ9-THC), carbon dioxide and water. Cannabinoids can be manufactured by first heating the Cannabis biomass to convert carboxylic acids prior to extraction and purification. Alternatively, and preferably because of manufacturing cost and product stability, the carboxylic acids can be first extracted and purified. They can be utilized in the carboxylic acid form or stored in a stable manner until converted to cannabinoids for use in medicine. This invention provides an efficient method for their conversion utilizing a high-pressure reactor under inert conditions.