A steam autoclave process chamber in the form of an open metal tank fitted with the necessary technical means to fix the closing lid and to connect the necessary accessories characterised in that there is at least one heater (4) inside the tank walls (1,2,3), where the heater is integrally incorporated with the wall into a single inseparable element.

The method of producing a steam autoclave process chamber which consists in the making of an open metal tank with walls in the form of a single casting of any desired shape under a known casting method, followed by subsequent stages which involve mechanical machining of the casting and fitting it with necessary chamber accessories characterised in that before the casting is initiated, there is at least one pipe heater (4) placed in the casting mould so that it is found inside the cast wall of the tank, and that the ends (10) of the heater pipes extend outside the casting mould, whereupon the mould is filled with molten metal in which the pipe heater (4) gets sunk.

This disclosure relates to systems and processes for cooling polymer product mixtures manufactured at high pressure. The processes of the invention involve cooling and then subsequently reducing the pressure of the product mixture from the reactor. In the systems of the invention, a product cooler is located downstream of the high pressure reactor and upstream of a high pressure let down valve.

This disclosure relates to systems and processes for cooling polymer product mixtures manufactured at high pressure. The processes of the invention involve cooling and then subsequently reducing the pressure of the product mixture from the reactor. In the systems of the invention, a product cooler is located downstream of the high pressure reactor and upstream of a high pressure let down valve.

The present invention relates to a pressure vessel system (1), comprising: —a pressure vessel (2) having a reaction chamber (3) in the form of a pressure chamber for initiating and/or promoting chemical and/or physical pressurized reactions of samples (P) received in the reaction chamber (3); and —a rail (50), which is rigidly connected to one pail of the pressure vessel (2) and has a first connection point (51) for admitting fluid, a second connection point (52) for discharging fluid and a fluid line (53), which fluidically connects the first connection point (51) to the second connection point (52), the fluid line (53) being fluidically connected to the reaction chamber (3) via the second connection point (52), and the rail (50) comprising at least one third connection point (55), which is fluidically connected to the fluid line (53) and can be connected to a device (56) such that the device (56) is fluidically connected to the fluid line (53) and thus to the reaction chamber (3).

The present invention relates to a pressure vessel system (1), comprising: —a pressure vessel (2) having a reaction chamber (3) in the form of a pressure chamber for initiating and/or promoting chemical and/or physical pressurized reactions of samples (P) received in the reaction chamber (3); and —a rail (50), which is rigidly connected to one pail of the pressure vessel (2) and has a first connection point (51) for admitting fluid, a second connection point (52) for discharging fluid and a fluid line (53), which fluidically connects the first connection point (51) to the second connection point (52), the fluid line (53) being fluidically connected to the reaction chamber (3) via the second connection point (52), and the rail (50) comprising at least one third connection point (55), which is fluidically connected to the fluid line (53) and can be connected to a device (56) such that the device (56) is fluidically connected to the fluid line (53) and thus to the reaction chamber (3).

A structural improvement for microwave-assisted high temperature high-pressure chemistry vessel systems is disclosed that among other advantages offers dynamic venting and resealing while a reaction proceeds and eliminates the risk of cross contamination associated with systems that use a common pressurized chamber. The improvement includes a relatively thin-walled disposable liner cylinder that includes one closed end and one open end defining a mouth, and a liner cap positioned in the mouth of the rigid liner cylinder for closing the rigid liner cylinder. The liner cap includes a depending column that engages the inside diameter of the rigid liner cylinder, and a disk at one end of the depending column having a diameter sufficient to rest upon the rigid liner cylinder without falling into the rigid cylinder liner so that the cylindrical liner cap can rest in the rigid liner cylinder at the mouth of the rigid liner cylinder. The depending column, includes a passage to provide a gas venting space, and a dynamic venting action, between the liner cap and the rigid liner cylinder.

A thermal process system includes a retort assembly, a heating assembly, and a vessel housing. The retort assembly includes a retort chamber and is configured to substantially form a containment boundary to contain one or more gases in the retort chamber during a thermal process. The heating assembly includes one or more heating elements and is configured to heat the retort chamber. The vessel housing is positioned around the retort chamber and the one or more heating elements and configured to form a pressure boundary to maintain a pressure within the retort chamber and reduce a pressure across the retort chamber.

A method for synthesizing an alkali metal-based phosphorous compound includes contacting an elemental alkali metal with elemental phosphorous to create a mixture and applying a pressure of less than 20 gigapascals to the mixture for forming the alkali metal-based phosphorous compound.

A method for synthesizing an alkali metal-based phosphorous compound includes contacting an elemental alkali metal with elemental phosphorous to create a mixture and applying a pressure of less than 20 gigapascals to the mixture for forming the alkali metal-based phosphorous compound.

Systems and methods related to centrifuge energy harvesting chambers (CEHCs) for gas production simulation are provided. Certain CEHCs may include a high-pressure chamber, high-pressure syringe pumps, cooling systems, an actuator and surcharge, backpressure control inside the wellbore, a heating element on the wellbore, water gas separation systems, and flow measurement systems. Certain CEHCs may also provide software operably connected to sensors and instrumentation, comprising a module to continuously, in real-time, periodically, or asynchronously, measure and monitor simulation variables.