Multi-component particles comprising inorganic nanoparticles distributed in an organic matrix and processes for making and using same. A flowing aerosol is generated that includes droplets of a precursor medium dispersed in a gas phase. The precursor medium contains a liquid vehicle and at least one precursor. At least a portion of the liquid vehicle is removed from the droplets of precursor medium under conditions effective to convert the precursor to the nanoparticles or the matrix and form the multi-component particles.

Disclosed is a method for preparing a nanoparticle composition. The method includes forming a nanoparticle aerosol in a low pressure reactor, wherein the aerosol comprises MX-functional nanoparticles entrained in a gas, where M is an independently selected Group IV element and X is a functional group independently selected from H and a halogen atom. The method further includes collecting the MX-functional nanoparticles of the aerosol in a capture fluid, where the capture fluid is in fluid communication with the low pressure reactor. The capture fluid includes a polar aprotic fluid immiscible with water and having a viscosity of from 5 to 200 centipoise at 25? C. The capture fluid further includes a functionalization compound miscible with the polar aprotic fluid, the functionalization compound comprising a functional group Y reactive with the functional group X of the MX-functional nanoparticles.

Disclosed here is a method for making an architected three-dimensional aerogel, comprising providing a photoresin comprising a solvent, a photoinitiator, a crosslinkable polymer precursor, and a precursor for graphene, metal oxide or metal chalcogenide; curing the photoresin using projection microstereolithography layer-by-layer to produce a wet gel having a pre-designed three dimensional structure; drying the wet gel to produce a dry gel; and pyrolyzing the dry gel to produce an architected three-dimensional aerogel. Also disclosure is a photoresin for projection microstereolithography, comprising a solvent, a photoinitiator, a crosslinkable polymer precursor, and graphene oxide.

A method of manufacturing a flowable and dispersible powder includes solubilizing a lipophilic substance in a terpene to form a mixture and treating the mixture to form a nanoemulsion dispersed in an aqueous solution. The aqueous solution includes at least one functional excipient. The nanoemulsion is then spray dried, thereby evaporating first the aqueous portion and then the terpene to form a dry powder formed from solid particles comprising the lipophilic substance.

The invention relates to a device and a method for separating particles from aerosols for conditioning test aerosols for penetration measurement on filters. The device for separating particles from aerosols for conditioning test aerosols for penetration measurement on filters is characterised in particular by being able to generate test aerosols for penetration measurement having particular and defined properties. For this purpose, at least one sieve, which fills the aerosol-conducting cross section of the component, is located in an aerosol-conducting, preferably tubular, component having an inlet and an outlet for the aerosol, for impingement and/or impaction of particles from the aerosol. Furthermore, the aerosol-conducting, preferably tubular, component has at least one port for supplying or removing air in the direction of flow of the aerosol upstream of the sieve for impingement and/or impaction of particles from the aerosol or a part supplying aerosol to the component.

A method of creating aerosols includes drawing a fluid from a fluid source through a first nip, the first nip defined between a first roller and an inner surface of a ring, the first nip having an upstream side and a downstream side, drawing the fluid from the fluid source through a second nip, the second nip defined between a second roller and the inner surface of the ring, the second roller positioned adjacent to and spaced apart from the first roller in a circular configuration, the second nip having an upstream side and a downstream side, stretching the fluid between diverging surfaces of the first roller and the inner surface of the ring on the downstream side of the first nip to form a first fluid filament, stretching the fluid between diverging surface of the second roller and the inner surface of the ring on the downstream side of the second nip to form a second fluid filament, causing the first fluid filament to break into a plurality of first droplets, and causing the second fluid filament to break into a plurality of second droplets.

In one aspect, the present invention relates to a method of making multi-phase particles that include nanoparticulates and matrix, which maintains the nanoparticulates in a dispersed state. A flowing gas dispersion is generated that includes droplets of a precursor medium dispersed in a gas phase. The precursor medium contains liquid vehicle and at least a first precursor to a first material and a second precursor to a second material. The multi-phase particles are formed from the gas dispersion by removing at least a portion of the liquid vehicle from the droplets of precursor medium. The nanoparticulates in the multi-phase particles include the first material and the matrix in the multi-phase particles includes the second material.

The present disclosure provides methods for functionalizing the surfaces of cellulose nanoparticles. In embodiments, nanoparticles are aerosolized, and then passed through a flow reactor where they are contacted with gaseous reactants to functionalize the surface of the nanoparticles. In other embodiments, the nanoparticles are aerosolized, and then passed through a plasma reactor where they are contacted with gaseous reactants to functionalize the surface of the nanoparticles. Once the functionalized nanoparticles are produced, they may be combined with polymers to form polymer composites having both a polymer and the functionalized nanoparticles. Systems for producing these functionalized nanoparticles, coupled with downstream polymer processing equipment for forming the polymer composites, are also provided.

In one aspect, the present invention relates to a method of making multi-phase particles that include nanoparticulates and matrix, which maintains the nanoparticulates in a dispersed state. A flowing gas dispersion is generated that includes droplets of a precursor medium dispersed in a gas phase. The precursor medium contains liquid vehicle and at least a first precursor to a first material and a second precursor to a second material. The multi-phase particles are formed from the gas dispersion by removing at least a portion of the liquid vehicle from the droplets of precursor medium. The nanoparticulates in the multi-phase particles include the first material and the matrix in the multi-phase particles includes the second material.

A roller has an outer cylindrical surface having an array of holes, a central feed channel inside the roller, and vanes connecting the channel to the holes, forming a path for liquid between the channel and the holes. An atomization system having a fluid reservoir; a pair of rollers, at least one of the rollers having: a central feed channel, the channel fluidically connected to the fluid reservoir, an array of holes on a surface of the roller, and vanes connecting the channels to the holes, a nip formed between the rollers, and a receiving surface positioned to receive droplets formed when liquid exits the holes, stretches between the rollers as they counterrotate to form filaments and the filaments break into droplets.