This present disclosure relates to processes and apparatuses for toluene and benzene methylation in an aromatics complex for producing paraxylene. More specifically, the present disclosure relates to processes and apparatuses for toluene and benzene methylation within an aromatics complex for producing paraxylene wherein an embodiment uses a reactor having a refractory comprising a low iron content refractory.

Disclosed herein is a method and device for production of a new long-term storage-stable allotropic modification of oxygen, tetraoxygen O.sub.4, using a combination of known chemical reactions into one technological sequence, including chemical interaction of negative and positive oxidation state oxygen compounds.

The method involves production of dioxygen difluoride by oxidation of molecular oxygen with fluorine, followed by the reaction of dioxygen difluoride with alkali metal peroxide, forming tetraoxygen O.sub.4.

Tetraoxygen is stable in its liquid state up to a temperature of +40° C. and can be used for the oxidation of rocket fuel, long-term compact storage of oxygen, and many other purposes.

A refractory-lined equipment includes a vessel defining an interior at least partially lined with a refractory material, and a nozzle assembly coupled to the vessel and extending into the interior. The nozzle assembly includes an outer sleeve fixed to the sidewall and extending through an aperture defined in the sidewall, the outer sleeve defining a central passageway, and a nozzle cartridge assembly positionable within the central passageway and including an inner sleeve, a refractory lining disposed about the inner sleeve, and a nozzle positioned within the inner sleeve. The nozzle cartridge assembly is removably coupled to the outer sleeve external to the vessel.

A refractory-lined equipment includes a vessel defining an interior at least partially lined with a refractory material, and a nozzle assembly coupled to the vessel and extending into the interior. The nozzle assembly includes an outer sleeve fixed to the sidewall and extending through an aperture defined in the sidewall, the outer sleeve defining a central passageway, and a nozzle cartridge assembly positionable within the central passageway and including an inner sleeve, a refractory lining disposed about the inner sleeve, and a nozzle positioned within the inner sleeve. The nozzle cartridge assembly is removably coupled to the outer sleeve external to the vessel.

A process for large scale and energy efficient production of oxygenates from sugar is disclosed in which a sugar feedstock is introduced into a thermolytic fragmentation reactor comprising a fluidized stream of heat carrying particles which are separated from the reaction product and directed to a reheater comprising a resistance heating system.

The present invention relates to a pressure vessel system (1), comprising: —a pressure vessel (2) having a reaction chamber (3) in the form of a pressure chamber for initiating and/or promoting chemical and/or physical pressurized reactions of samples (P) received in the reaction chamber (3); and —a rail (50), which is rigidly connected to one pail of the pressure vessel (2) and has a first connection point (51) for admitting fluid, a second connection point (52) for discharging fluid and a fluid line (53), which fluidically connects the first connection point (51) to the second connection point (52), the fluid line (53) being fluidically connected to the reaction chamber (3) via the second connection point (52), and the rail (50) comprising at least one third connection point (55), which is fluidically connected to the fluid line (53) and can be connected to a device (56) such that the device (56) is fluidically connected to the fluid line (53) and thus to the reaction chamber (3).

The present invention relates to a pressure vessel system (1), comprising: —a pressure vessel (2) having a reaction chamber (3) in the form of a pressure chamber for initiating and/or promoting chemical and/or physical pressurized reactions of samples (P) received in the reaction chamber (3); and —a rail (50), which is rigidly connected to one pail of the pressure vessel (2) and has a first connection point (51) for admitting fluid, a second connection point (52) for discharging fluid and a fluid line (53), which fluidically connects the first connection point (51) to the second connection point (52), the fluid line (53) being fluidically connected to the reaction chamber (3) via the second connection point (52), and the rail (50) comprising at least one third connection point (55), which is fluidically connected to the fluid line (53) and can be connected to a device (56) such that the device (56) is fluidically connected to the fluid line (53) and thus to the reaction chamber (3).

A continuous tubular reactor includes a rotary reaction tube having a reactant inlet and a product outlet, and including a ceramic; a heating device disposed outside the rotary reaction tube; and an angle adjuster adjusting an angle of a rotation axis of the rotary reaction tube. The angle of the rotation axis is 75° or less with respect to a horizontal surface.

A continuous tubular reactor includes a rotary reaction tube having a reactant inlet and a product outlet, and including a ceramic; a heating device disposed outside the rotary reaction tube; and an angle adjuster adjusting an angle of a rotation axis of the rotary reaction tube. The angle of the rotation axis is 75° or less with respect to a horizontal surface.

A process for a continuous production of a boronic acid derivative and an apparatus of performing the process are disclosed.