B01J25/02

MICRO-REACTION SYSTEM AND METHOD FOR PREPARING 2-METHYL-4-AMINO-5-AMINOMETHYL PYRIMIDINE
20210394148 · 2021-12-23 ·

A micro-reaction system and a method for preparing 2-methyl-4-amino-5-aminomethyl pyrimidine. A Raney nickel catalyst is modified with formalin, and the modified Raney nickel catalyst is filled into a micro-channel reactor of the micro-reaction system. A substrate solution containing 2-methyl-4-amino-5-cyanopyrimidine and a base and hydrogen are transported to the micro-mixer and the micro-channel reactor in sequence for continuous catalytic hydrogenation to obtain 2-methyl-4-amino-5-aminomethyl pyrimidine.

FULL CONTINUOUS FLOW PREPARATION METHOD OF 2-METHYL-4-AMINO-5-AMINOMETHYLPYRIMIDINE
20210394150 · 2021-12-23 ·

A full continuous flow preparation method of 2-methyl-4-amino-5-aminomethylpyrimidine. A mixed solution of cyanoacetamide, N,N-dimethylformamide and a catalyst is mixed with phosphorus oxychloride in a first micro-mixer, and then the reaction mixture undergoes continuous flow reaction in a microchannel reactor to obtain (dimethylaminomethylene) malononitrile. The reaction mixture is subjected to continuous quenching, extraction and separation, and the organic phase is concentrated, mixed with a methanol solution, and then reacted with an organic base to obtain 2-methyl-4-amino-5-cyanopyrimidine. After the mixed liquid is continuously filtered, the filter cake is dissolved in methanol, mixed with hydrogen in a second micro-mixer, and then transported to a fixed-bed reactor for hydrogenation reaction. The products are concentrated, dried and purified to obtain the desired 2-methyl-4-amino-5-aminomethylpyrimidine.

FULL CONTINUOUS FLOW PREPARATION METHOD OF 2-METHYL-4-AMINO-5-AMINOMETHYLPYRIMIDINE
20210394150 · 2021-12-23 ·

A full continuous flow preparation method of 2-methyl-4-amino-5-aminomethylpyrimidine. A mixed solution of cyanoacetamide, N,N-dimethylformamide and a catalyst is mixed with phosphorus oxychloride in a first micro-mixer, and then the reaction mixture undergoes continuous flow reaction in a microchannel reactor to obtain (dimethylaminomethylene) malononitrile. The reaction mixture is subjected to continuous quenching, extraction and separation, and the organic phase is concentrated, mixed with a methanol solution, and then reacted with an organic base to obtain 2-methyl-4-amino-5-cyanopyrimidine. After the mixed liquid is continuously filtered, the filter cake is dissolved in methanol, mixed with hydrogen in a second micro-mixer, and then transported to a fixed-bed reactor for hydrogenation reaction. The products are concentrated, dried and purified to obtain the desired 2-methyl-4-amino-5-aminomethylpyrimidine.

Branched Products
20210387933 · 2021-12-16 · ·

A process for producing isomerized olefins, branched aldehydes, branched alcohols, branched surfactants and other branched derivatives through isomerization, hydroformylation, hydrogenation, surfactant forming reactions and other derivative forming reactions.

Alcohols Production
20210380516 · 2021-12-09 · ·

A process for producing branched alcohols through isomerization, hydroformylation and hydrogenation.

Branched Products
20220176361 · 2022-06-09 · ·

A process for producing isomerized olefins, branched aldehydes, branched alcohols, branched surfactants and other branched derivatives through isomerization, hydroformylation, hydrogenation, surfactant forming reactions and other derivative forming reactions.

Hydrogen producing apparatus, method for separating solid product and system for discharging and recycling solid product
11332367 · 2022-05-17 · ·

To provide an apparatus and a system suitable for continuously and stably producing hydrogen by taking advantage of a direction composition reaction of hydrocarbons as well as a method for separating a solid product. Provided are a hydrogen producing apparatus using a nickel-based metal structure for the direct decomposition reaction of hydrocarbons and a discharging and recovering system comprising: a depressurization chamber communicating with a lower opening of the reaction chamber of hydrogen producing apparatus 1 via a ventilation hole; a first valve capable of opening and closing said ventilation hole; a collection box communicating with the depressurization chamber via a channel; a second valve capable of opening and closing said depressurization chamber; and a depressurization pump communicating with the collection box.

Acid-resistant alloy catalyst

An acid-resistant alloy catalyst, comprising nickel, one or more rare earth element, tin, aluminum and molybdenum. The catalyst is cheap and stable, does not need a carrier, can be stably applied in industrial continuous production, and can lower the production cost.

Method for producing 2,5-bis(aminomethyl)furan

The present invention is to provide a production method that can produce 2,5-bis(aminomethyl)furan efficiently. The production method for 2,5-bis(aminomethyl)furan includes reacting 5-(halogenated methyl)furfural with hydrogen and an amine compound using a hydrogenation catalyst to obtain 2,5-bis(aminomethyl)furan.

CASHEW NUT SHELL LIQUID DERIVATIVES AND METHODS FOR MAKING AND USING SAME

The present invention is directed to Cashew Nut Shell Liquid derivatives and methods for making and using same. The invention is also directed to Cashew Nut Shell Liquid based monomers and polymers for making antimicrobials, antioxidants, adhesives, coatings, corrosion retardants composites, cosmetics, detergents, soaps, de-icing products, elastomers, food, flavors, inks, lubricants, oil field chemicals, personal care products, polymers, structural polymers, engineered plastics, 3D printable polymers, techno-polymers, rubbers, sealants, solvents, surfactants and varnishes.