A method for manufacturing particles including (a) bringing at least one starting material into a reactor, (b) subjecting the at least one starting material to a thermal treatment of a pulsating process gas stream in a treatment zone of the reactor, (c) forming particles, and (d) bringing the particles which are obtained in steps (b) and (c) out of the reactor. The at least one starting material is thermally treated in the treatment zone at a treatment temperature of 100° C. to 3000° C. and a retention time in the range of 0.1 s to 25 s, and temperature regulation of the process gas stream is decoupled from the generation and maintenance of a pulsation of the process gas stream. Also provided is a reactor for manufacturing particles according to the method.

Device for metering powder, in particular in clean-rooms, which includes a vessel containing powder and a sealing head with a septum for the vessel, wherein the sealing head is connectable powder-tight with the vessel and the septum powder-tight with the sealing head and the device further includes a vessel holder, which serves to hold the sealing head of the vessel, and the vessel with its opening points downwards, so that the powder can flow out of the vessel, wherein a gap is provided between the sealing head and a holding bowl of the vessel holder, in which a gas flow between the holding bowl and the sealing head can be created. The invention also relates to a use of the device and a metered addition method.

Device for metering powder, in particular in clean-rooms, which includes a vessel containing powder and a sealing head with a septum for the vessel, wherein the sealing head is connectable powder-tight with the vessel and the septum powder-tight with the sealing head and the device further includes a vessel holder, which serves to hold the sealing head of the vessel, and the vessel with its opening points downwards, so that the powder can flow out of the vessel, wherein a gap is provided between the sealing head and a holding bowl of the vessel holder, in which a gas flow between the holding bowl and the sealing head can be created. The invention also relates to a use of the device and a metered addition method.

A chemical synthesis device includes a reaction vessel, a waste liquid tank and an intermediate container. A chemical is supplied to the reaction vessel. The waste liquid tank is configured to hold waste liquid discharged from the reaction vessel. The intermediate container has a smaller capacity than the waste liquid tank. The intermediate container is provided between the reaction vessel and the waste liquid tank, via a waste liquid pipe. The pressure of the intermediate container is adjusted to adjust the flow supplied to the reaction vessel and the flow discharged from the reaction vessel.

A method of remediating pesticides from an agricultural oil includes mixing a reaction solvent, a reducing agent, and an agricultural oil into a reaction mixture in a reaction vessel, controlling the temperature of the reaction mixture, producing a pre-neutralization mixture including a separation solvent, transferring the pre-neutralization mixture into a neutralization reactor that contains a neutralization agent, mixing the pre-neutralization mixture with the neutralization agent and allowing separation into an aqueous layer and a separation solvent layer, draining the aqueous layer, and distilling the separation solvent in the separation solvent layer from the remediated agricultural oils. A system has a reactor vessel, the reactor vessel having one or more inlets to allow a reducing agent, the agricultural oil, the separation solvent, and other additives as needed to produce a reaction mixture, a temperature control unit to control a temperature of the reaction mixture at a predetermined temperature for a predetermined time, a neutralization vessel fluidically connected to the reactor vessel to receive the reaction mixture from the reactor vessel, the neutralization vessel having an inlet to allow a neutralization agent to be introduced into the neutralization vessel to produce a neutralized reaction mixture, and a valve arranged at a bottom of the neutralization vessel to allow an aqueous phase of the reaction mixture to be drained from the neutralization vessel.

A method for minimizing the amount of catalyst inactivating agent that is present in a liquid fraction recovered from a slurry-based polymer production process, the liquid fraction comprising diluent used in the polymer production process, is disclosed. The method includes steps for controlling the pressure over the liquid fraction collected during diluent recovery so as to minimize the concentration of catalyst inactivating agent that is retained in the recovered liquid fraction. Embodiments of apparatus suitable for conducting the disclosed method are also provided.

Processes and apparatus for preparing bimodal polymers are provided. In some embodiments, processes include introducing a monomer, a first diluent, a catalyst, hydrogen, at a first hydrogen concentration, and optional comonomer, to a first loop reactor to produce, under polymerization conditions, a first slurry of polymer solids. Processes may also include continuously discharging the first slurry of polymer solids from the loop reactor as a first polymerization effluent to a first flash tank; separating the first polymerization effluent in the first flash tank to provide a first concentrated polymer slurry with significantly lower hydrogen concentration; and transferring the first concentrated polymer slurry from the flash tank to a re-slurry mixer. Processes may further include introducing a re-slurry mixer diluent to the first concentrated polymer slurry to form a second concentrated polymer slurry in the re-slurry mixer that can be pumped to a second slurry loop reactor.

A method of producing an organic peroxide includes introducing an organic solution and a peroxide solution into a mixing tank to form a mixture. The method further includes circulating the mixture over a fixed catalyst bed to form the organic peroxide and measuring a concentration of the organic peroxide in the mixture. Further, the method includes removing at least a portion of the mixture when the concentration reaches a set value.

An apparatus and a method to withdraw samples from a polymerization plant using a defined sequence of steps combined with locking devices for valves opened by a single key.

The present invention relates to a method for producing purified phosgene vapor, comprising the following steps: 1) providing a gas flow obtainable from the reaction of chlorine with carbon monoxide and comprising phosgene and carbon monoxide; 2) one-stage or multi-stage condensation of the gas flow and separation of non-condensable residue gases; 3) one-stage or multi-stage evaporation of the liquid phosgene obtained in step 2) and optional overheating of the produced phosgene vapour, wherein there is an energy integration between one or more of the condensation steps of step 2) and one or more of the evaporation steps in step 3) and the pressure in the last condensation step is between 0.2 and 6.0 bar higher than in the first evaporation step.