A method embodiment involves preparing single metal or mixed transition metal chalcogenide using exfoliation of two or more different bulk transition metal dichalcogenides in a manner to form an intermediate hetero-layered transition metal chalcogenide structure, which can be treated to provide a single-phase transition metal chalcogenide.

A system for the exfoliation of a layered material is described, comprising in combination: an exfoliation station (14-22) operating on a volume of a dispersion of a layered precursor material, including a wet-jet milling device (10); and a collecting station (30, 40), located downstream of the exfoliation station (14-22), operating on a volume of a dispersion of the at least partly exfoliated material, in which the exfoliation station (14-22) and the collecting station (30, 40) are connected to each other through a fluid communication path (20) along which there are interposed flow regulating means (50) adapted to assume a first operating configuration in which the communication path (20) between the exfoliation station (14-22) and the collecting station (30, 40) is discontinued, where the exfoliation station (14-22) is adapted to subject a volume of dispersion of layered precursor material to a predetermined number of wet jet milling cycles; and a second operating configuration in which the communication path (20) between the exfoliation station (14-22) and the collecting station (30, 40) is continuous, where the exfoliation station (14-22) is adapted to convey a volume of previously milled dispersion including at least partly exfoliated material to the collecting station (30, 40) and is placed in communication with a supply chamber (12) to be fed with a further volume of a dispersion of layered precursor material that has to be exfoliated.

A system for the exfoliation of a layered material is described, comprising in combination: an exfoliation station (14-22) operating on a volume of a dispersion of a layered precursor material, including a wet-jet milling device (10); and a collecting station (30, 40), located downstream of the exfoliation station (14-22), operating on a volume of a dispersion of the at least partly exfoliated material, in which the exfoliation station (14-22) and the collecting station (30, 40) are connected to each other through a fluid communication path (20) along which there are interposed flow regulating means (50) adapted to assume a first operating configuration in which the communication path (20) between the exfoliation station (14-22) and the collecting station (30, 40) is discontinued, where the exfoliation station (14-22) is adapted to subject a volume of dispersion of layered precursor material to a predetermined number of wet jet milling cycles; and a second operating configuration in which the communication path (20) between the exfoliation station (14-22) and the collecting station (30, 40) is continuous, where the exfoliation station (14-22) is adapted to convey a volume of previously milled dispersion including at least partly exfoliated material to the collecting station (30, 40) and is placed in communication with a supply chamber (12) to be fed with a further volume of a dispersion of layered precursor material that has to be exfoliated.

Methods and systems for the preparation of conditioned micronized active agents. Additionally, methods and systems for in-process conditioning of micronized active agent particles and compositions comprising conditioned micronized materials.

Methods and systems for the preparation of conditioned micronized active agents. Additionally, methods and systems for in-process conditioning of micronized active agent particles and compositions comprising conditioned micronized materials.

A reactor may be configured to facilitate chemical reactions and/or comminution of solid feed materials. The reactor may be configured to make use of shockwaves created in a supersonic gaseous vortex. The reactor may include a rigid chamber having a substantially circular cross-section. A gas inlet may be configured to introduce a high-velocity stream of gas into the chamber. The gas inlet may be disposed and arranged so as to effectuate a vortex of the stream of gas circulating within the chamber. The vortex may rotate at a supersonic speed about a longitudinal axis of the chamber. A material inlet may be configured to introduce a material to be processed into the chamber. The material may be processed within the chamber by nonabrasive mechanisms facilitated by shockwaves within the chamber. An outlet may be configured to emit the gas and processed material from the chamber.

A reactor may be configured to facilitate chemical reactions and/or comminution of solid feed materials. The reactor may be configured to make use of shockwaves created in a supersonic gaseous vortex. The reactor may include a rigid chamber having a substantially circular cross-section. A gas inlet may be configured to introduce a high-velocity stream of gas into the chamber. The gas inlet may be disposed and arranged so as to effectuate a vortex of the stream of gas circulating within the chamber. The vortex may rotate at a supersonic speed about a longitudinal axis of the chamber. A material inlet may be configured to introduce a material to be processed into the chamber. The material may be processed within the chamber by nonabrasive mechanisms facilitated by shockwaves within the chamber. An outlet may be configured to emit the gas and processed material from the chamber.

A system, apparatus and method for separating hard contaminates of a compound from softer elements using a milling process wherein particle size reduction if effectuated on the softer elements. The milled material is then subjected to particle separation devices to remove the larger particles thereby reducing the percentage of hard particles in the remaining compound. Additional milling and separation steps are used to hard material concentration to less than a predetermined threshold.

A system, apparatus and method for separating hard contaminates of a compound from softer elements using a milling process wherein particle size reduction if effectuated on the softer elements. The milled material is then subjected to particle separation devices to remove the larger particles thereby reducing the percentage of hard particles in the remaining compound. Additional milling and separation steps are used to hard material concentration to less than a predetermined threshold.

An apparatus and a method are for separating a plastic-based insulation material from a concrete-based constructional element, to which the insulation material is attached. The apparatus has at least one fluid-jetting device which is in fluid communication with a pressure-generating device to produce a fluid jet with a pressure sufficient to release the insulation material from the constructional element. The apparatus is configured to allow relative motion between the fluid-jetting device and the constructional element.