A supercentrifuge with a non-intrusive device for the extraction of solids, the supercentrifuge comprising a chamber or rotor for the clarification of liquids and a piston located within the chamber passing through it in order to discharge the solids, the piston being driven in its outward travel along the chamber by the injection of a pressurised fluid which pushes the piston, in which the supercentrifuge has a pneumatic pumping system for the generation of vacuum to bring about return movement of the piston along the chamber.

A supercentrifuge with a non-intrusive device for the extraction of solids, the supercentrifuge comprising a chamber or rotor for the clarification of liquids and a piston located within the chamber passing through it in order to discharge the solids, the piston being driven in its outward travel along the chamber by the injection of a pressurised fluid which pushes the piston, in which the supercentrifuge has a pneumatic pumping system for the generation of vacuum to bring about return movement of the piston along the chamber.

Provided is a centrifugal field-flow fractionation device in which a liquid sample is less likely to leak from a channel and attachment and detachment work of a channel member is facilitated. By integrally forming an outer peripheral surface 162 and an inner peripheral surface 163 of a channel member 16, the channel member 16 is configured as one hollow member having a channel 161 formed inside. Thus, pressure resistance performance of the channel member 16 is improved, formation of a gap in the channel 161 can be prevented, and deterioration in sealing performance due to secular change is not generated. Accordingly, a liquid sample is less likely to leak from the channel 161. Further, since the channel member 16 can be handled as one member, attachment and detachment work of the channel member 16 is facilitated.

Provided is a centrifugal field-flow fractionation device in which a liquid sample is less likely to leak from a channel and attachment and detachment work of a channel member is facilitated. By integrally forming an outer peripheral surface 162 and an inner peripheral surface 163 of a channel member 16, the channel member 16 is configured as one hollow member having a channel 161 formed inside. Thus, pressure resistance performance of the channel member 16 is improved, formation of a gap in the channel 161 can be prevented, and deterioration in sealing performance due to secular change is not generated. Accordingly, a liquid sample is less likely to leak from the channel 161. Further, since the channel member 16 can be handled as one member, attachment and detachment work of the channel member 16 is facilitated.

A system operating as a centrifugal, liquid-liquid separator may be controlled, and even optimized, by automatic control of back pressure to establish an optimum position of the dispersion band therein. Optimizing to minimize impurities (from each other) in each of two separated phases is possible, even simultaneously, by reliance on a processor setting the settling lengths of both heavy and light phases at the same value. Settling length, defined in accordance with the invention, reflects a settling velocity multiplied by a residence time. Equating these lengths, for droplets of each in the other liquid, provides superior results over conventional settling theory maximizing settling area. Equalization of residence times did not provide an improvement over conventional settling theory.

A system operating as a centrifugal, liquid-liquid separator may be controlled, and even optimized, by automatic control of back pressure to establish an optimum position of the dispersion band therein. Optimizing to minimize impurities (from each other) in each of two separated phases is possible, even simultaneously, by reliance on a processor setting the settling lengths of both heavy and light phases at the same value. Settling length, defined in accordance with the invention, reflects a settling velocity multiplied by a residence time. Equating these lengths, for droplets of each in the other liquid, provides superior results over conventional settling theory maximizing settling area. Equalization of residence times did not provide an improvement over conventional settling theory.

A centrifugal field-flow fractionation device includes an annular rotor, an arc-shaped channel member, a rotation drive unit, and a restriction unit. A channel member 16 is provided along an inner peripheral surface of the rotor, has therein a channel 161 for a liquid sample by laminating a plurality of layers, and has an inlet for the liquid sample to the channel 161 and an outlet for the liquid sample from the channel 161. By rotating the rotor, particles in the liquid sample in the channel 161 are classified by centrifugal force. A restriction spacer 64 restricts the channel 161 from being compressed to a height less than a certain height when the channel member 16 is compressed and deformed in a laminating direction.

A centrifugal field-flow fractionation device includes an annular rotor, an arc-shaped channel member, a rotation drive unit, and a restriction unit. A channel member 16 is provided along an inner peripheral surface of the rotor, has therein a channel 161 for a liquid sample by laminating a plurality of layers, and has an inlet for the liquid sample to the channel 161 and an outlet for the liquid sample from the channel 161. By rotating the rotor, particles in the liquid sample in the channel 161 are classified by centrifugal force. A restriction spacer 64 restricts the channel 161 from being compressed to a height less than a certain height when the channel member 16 is compressed and deformed in a laminating direction.

In a continuous centrifuge, a core end surface component separated from a core body is arranged inside a rotor, an air trap mechanism which automatically captures bubbles inside a sample is formed, and the bubbles are removed by centrifugal separation before the sample is sent to an outer circumferential portion having a high liquid pressure. In addition, when viewed in the axial direction, the core body and an upper rotor cover abut each other, and the core end surface component and a lower rotor cover abut each other, with appropriate pressure by biasing the core end surface component and the core body with a spring. Because a flow path between the rotor core and the rotor covers is maintained in a perfect state and the bubbles in liquid are also removed, the flow path may not be blocked by the bubbles and the centrifugal separation can be stably performed.

In a continuous centrifuge, a core end surface component separated from a core body is arranged inside a rotor, an air trap mechanism which automatically captures bubbles inside a sample is formed, and the bubbles are removed by centrifugal separation before the sample is sent to an outer circumferential portion having a high liquid pressure. In addition, when viewed in the axial direction, the core body and an upper rotor cover abut each other, and the core end surface component and a lower rotor cover abut each other, with appropriate pressure by biasing the core end surface component and the core body with a spring. Because a flow path between the rotor core and the rotor covers is maintained in a perfect state and the bubbles in liquid are also removed, the flow path may not be blocked by the bubbles and the centrifugal separation can be stably performed.