B22F3/02

METHOD FOR MANUFACTURING R-T-B BASED SINTERED MAGNET, AND R-T-B BASED SINTERED MAGNET

A method for manufacturing an R-T-B based sintered magnet according the present disclosure comprises: a step for preparing a coarse ground powder which is made from an alloy for R-T-B based sintered magnets and which has an average particle size of 10-500 μm; a step for obtaining a fine powder having an average particle size of 2.0-4.5 μm, by feeding the coarse ground powder to a jet mill device that has a grinding chamber filled with inert gas and grinding the coarse ground powder; and a step for producing a sintered body of the fine powder, wherein the inert gas has been humidified, and the oxygen content of the R-T-B based sintered magnet is 1000-3500 ppm by mass.

METHOD FOR MANUFACTURING R-T-B BASED SINTERED MAGNET, AND R-T-B BASED SINTERED MAGNET

A method for manufacturing an R-T-B based sintered magnet according the present disclosure comprises: a step for preparing a coarse ground powder which is made from an alloy for R-T-B based sintered magnets and which has an average particle size of 10-500 μm; a step for obtaining a fine powder having an average particle size of 2.0-4.5 μm, by feeding the coarse ground powder to a jet mill device that has a grinding chamber filled with inert gas and grinding the coarse ground powder; and a step for producing a sintered body of the fine powder, wherein the inert gas has been humidified, and the oxygen content of the R-T-B based sintered magnet is 1000-3500 ppm by mass.

ISOSTATIC PRESSURE SPARK PLASMA SINTERING (IP-SPS) NET SHAPING OF COMPONENTS USING NANOSTRUCTURED MATERIALS

A method of forming a consolidated component having a complex shape includes providing a first component having a first shape similar to the complex shape. The method further includes placing the first component in a chamber and surrounding the first component with a medium. The method further includes applying pressure and at least one of heat or electricity into the chamber to process the first component to form a consolidated component having the complex shape.

ISOSTATIC PRESSURE SPARK PLASMA SINTERING (IP-SPS) NET SHAPING OF COMPONENTS USING NANOSTRUCTURED MATERIALS

A method of forming a consolidated component having a complex shape includes providing a first component having a first shape similar to the complex shape. The method further includes placing the first component in a chamber and surrounding the first component with a medium. The method further includes applying pressure and at least one of heat or electricity into the chamber to process the first component to form a consolidated component having the complex shape.

HARD PARTICLE POWDER FOR SINTERED BODY

The present invention relates to a hard particle powder for a sintered body, the powder including, in terms of mass %, 0.01≤C≤1.0, 2.5≤Si≤3.3, 0.1≤Ni≤20.0, 5.0≤Cr≤15.0, and 35.0≤Mo≤45.0, with the balance being Fe and inevitable impurities, in which the powder before performing sintering comprises an alloy phase comprising a hexagonal crystal structure of C14 type Laves phase.

HARD PARTICLE POWDER FOR SINTERED BODY

The present invention relates to a hard particle powder for a sintered body, the powder including, in terms of mass %, 0.01≤C≤1.0, 2.5≤Si≤3.3, 0.1≤Ni≤20.0, 5.0≤Cr≤15.0, and 35.0≤Mo≤45.0, with the balance being Fe and inevitable impurities, in which the powder before performing sintering comprises an alloy phase comprising a hexagonal crystal structure of C14 type Laves phase.

Sm-Fe-N MAGNET

A Sm—Fe—N magnet includes Sm—Fe—N particles, wherein an inter-particle metal phase is present between at least two of the Sm—Fe—N particles, an average particle diameter of the Sm—Fe—N particles is less than 2.0 μm, and a percentage of the Sm—Fe—N particles having an aspect ratio of 2.0 or more is 10% or less, the inter-particle metal phase includes a Fe.sub.3Zn.sub.10 phase and an α-Fe phase in a particle form, and in the inter-particle metal phase, an area ratio of the Fe.sub.3Zn.sub.10 phase is 80% or more.

Sm-Fe-N MAGNET

A Sm—Fe—N magnet includes Sm—Fe—N particles, wherein an inter-particle metal phase is present between at least two of the Sm—Fe—N particles, an average particle diameter of the Sm—Fe—N particles is less than 2.0 μm, and a percentage of the Sm—Fe—N particles having an aspect ratio of 2.0 or more is 10% or less, the inter-particle metal phase includes a Fe.sub.3Zn.sub.10 phase and an α-Fe phase in a particle form, and in the inter-particle metal phase, an area ratio of the Fe.sub.3Zn.sub.10 phase is 80% or more.

Grain boundary engineering of sintered magnetic alloys and the compositions derived therefrom
11557411 · 2023-01-17 · ·

The present disclosure is directed at methods of preparing rare earth-based permanent magnets having improved coercivity and remanence, the method comprising one or more steps comprising: (a) homogenizing a first population of particles of a first GBM alloy with a second population of particles of a second core alloy to form a composite alloy preform, the first GBM alloy being substantially represented by the formula: AC.sub.bR.sub.xCo.sub.yCu.sub.dM.sub.z, the second core alloy being substantially represented by the formula G.sub.2Fe.sub.14B, where AC, R, M, G, b, x, y, and z are defined; (b) heating the composite alloy preform particles to form a population of mixed alloy particles; (c) compressing the mixed alloy particles, under a magnetic field of a suitable strength to align the magnetic particles with a common direction of magnetization and inert atmosphere, to form a green body; (d) sintering the green body; and (e) annealing the sintered body. Particular embodiments include magnets comprising neodymium-iron-boron core alloys, including Nd.sub.2Fe.sub.14B.

Grain boundary engineering of sintered magnetic alloys and the compositions derived therefrom
11557411 · 2023-01-17 · ·

The present disclosure is directed at methods of preparing rare earth-based permanent magnets having improved coercivity and remanence, the method comprising one or more steps comprising: (a) homogenizing a first population of particles of a first GBM alloy with a second population of particles of a second core alloy to form a composite alloy preform, the first GBM alloy being substantially represented by the formula: AC.sub.bR.sub.xCo.sub.yCu.sub.dM.sub.z, the second core alloy being substantially represented by the formula G.sub.2Fe.sub.14B, where AC, R, M, G, b, x, y, and z are defined; (b) heating the composite alloy preform particles to form a population of mixed alloy particles; (c) compressing the mixed alloy particles, under a magnetic field of a suitable strength to align the magnetic particles with a common direction of magnetization and inert atmosphere, to form a green body; (d) sintering the green body; and (e) annealing the sintered body. Particular embodiments include magnets comprising neodymium-iron-boron core alloys, including Nd.sub.2Fe.sub.14B.