A composite structure is disclosed comprising a neutron-absorbing metal hydride phase contained within a matrix having a density of greater than 95%. In various embodiments the metal hydride is a hydride of one or more of the following: Gadolinium, Hafnium, Europium, Samarium. The composite structure is utile as a shield for fusion or fission reactors.

Disclosed are a device and method for continuously performing grain boundary diffusion and heat treatment, characterized in that the alloy workpiece or the metal workpiece are arranged in a relatively independent processing box together with a diffusion source; the device comprises, in successive arrangement, a grain boundary diffusion chamber, a first cooling chamber, a heat treatment chamber, and a second cooling chamber, and a transfer system provided between various chambers for delivering the processing box; each of the first cooling chamber and the second cooling chamber uses an air cooling system, and the cooling air temperature of the first cooling chamber is above 25° C. and at least differs by 550° C. from the grain boundary diffusion temperature of the grain boundary diffusion chamber; the cooling air temperature of the second cooling chamber is above 25° C. and at least differs by 300° C. from the heat treatment temperature of the heat treatment chamber; and the cooling chamber has a pressure of 50 kPa to 100 kPa. The device provided by the present invention can increase the cooling rate and production efficiency, and improve product consistency.

Disclosed herein are embodiments of mechanically alloyed powder feedstock and methods for spheroidizing them using microwave plasma processing. The spheroidized powder can be used in metal injection molding processes, hot isostatic processing, and additive manufacturing. In some embodiments, mechanical milling, such as ball milling, can be used to prepare high entropy alloys for microwave plasma processing.

Disclosed herein are embodiments of mechanically alloyed powder feedstock and methods for spheroidizing them using microwave plasma processing. The spheroidized powder can be used in metal injection molding processes, hot isostatic processing, and additive manufacturing. In some embodiments, mechanical milling, such as ball milling, can be used to prepare high entropy alloys for microwave plasma processing.

Selective laser solidification apparatus is described that includes a powder bed onto which a powder layer can be deposited and a gas flow unit for passing a flow of gas over the powder bed along a predefined gas flow direction. A laser scanning unit is provided for scanning a laser beam over the powder layer to selectively solidify at least part of the powder layer to form a required pattern. The required pattern is formed from a plurality of stripes or stripe segments that are formed by advancing the laser beam along the stripe or stripe segment in a stripe formation direction. The stripe formation direction is arranged so that it always at least partially opposes the predefined gas flow direction. A corresponding method is also described.

Selective laser solidification apparatus is described that includes a powder bed onto which a powder layer can be deposited and a gas flow unit for passing a flow of gas over the powder bed along a predefined gas flow direction. A laser scanning unit is provided for scanning a laser beam over the powder layer to selectively solidify at least part of the powder layer to form a required pattern. The required pattern is formed from a plurality of stripes or stripe segments that are formed by advancing the laser beam along the stripe or stripe segment in a stripe formation direction. The stripe formation direction is arranged so that it always at least partially opposes the predefined gas flow direction. A corresponding method is also described.

A method of surface modification of a metal or metal alloy powder includes the steps of providing a metal or metal alloy powder including copper, gold, or silver and having an average diameter in the micron range; providing a powder having an alloying element to form an alloying element powder. The alloying element powder particles have an average diameter less than 10 micron and no more than half the average diameter of the metal or metal alloy powder particles; mixing the powders to form a mixed powder; heating the mixed powder in an atmosphere of reducing gas to a first temperature T1; after temperature T1 is reached, replacing the reducing gas atmosphere with an inert gas atmosphere and maintaining the temperature at a second temperature T2 for a predetermined time. The alloying element is capable of diffusing in the metal or metal alloy element at temperature T2.

A method of surface modification of a metal or metal alloy powder includes the steps of providing a metal or metal alloy powder including copper, gold, or silver and having an average diameter in the micron range; providing a powder having an alloying element to form an alloying element powder. The alloying element powder particles have an average diameter less than 10 micron and no more than half the average diameter of the metal or metal alloy powder particles; mixing the powders to form a mixed powder; heating the mixed powder in an atmosphere of reducing gas to a first temperature T1; after temperature T1 is reached, replacing the reducing gas atmosphere with an inert gas atmosphere and maintaining the temperature at a second temperature T2 for a predetermined time. The alloying element is capable of diffusing in the metal or metal alloy element at temperature T2.

A thermoelectric material of the present invention includes copper, tin, and sulfur, wherein a ratio A/B of the number A of copper atoms to the number B of tin atoms is 0.5 to 2.5 and a content of a metal element other than copper and tin is 5 mol % or less with respect to total metal elements. Additionally, the thermoelectric material of the present invention has a thermal conductivity less than 1.0 W/(m.Math.K) at 200 to 400° C.

An ejector for jetting modified metal is disclosed. The ejector for jetting modified metal also includes a nozzle orifice in connection with the inner cavity and configured to eject one or more droplets of liquid metal. The ejector for jetting modified metal includes a first gas source associated with the inner cavity and an external portion of the nozzle. The ejector for jetting modified metal also includes a second gas source coupled to the first gas source and in proximity to an external portion of the nozzle orifice.