The present disclosure provides systems and methods for forming block crystals of a metal compound. In some embodiments, a method for forming block crystals of a metal compound may comprise (a) introducing a source metal into a furnace; (b) forming a complete or partial vacuum in the furnace and increasing a temperature of the furnace above a melting point of the source metal to form a liquid flow of the source metal; (c) breaking the liquid flow to generate particles of the source metal; (d) ionizing the particles in an ionization chamber to form ionized particles, wherein the ionization chamber has a temperature above a decomposition temperature of the metal compound; and (e) introducing the ionized particles into a growth chamber comprising a reactive gas that is reactive with the ionized particles, to thereby form the block crystals of the metal compound.

The present invention is directed to a method to produce silver nanoparticles. The method includes the steps of dropwise addition of silver nitrate solution to a carboxymethyl cellulose solution (1%) while stirring. The solution is subjected to ultrasonic irradiation for 30 minutes. The first indication of silver nanoparticles being synthesized can be change in the color of the solution to yellowish-brown after Ultrasonication. The solution can thereafter be subjected to microwave irradiations. After the predetermined duration, the produced silver nanoparticles can be separated from the solution. The nanoparticles can be washed and freeze dried.

The present invention is directed to a method to produce silver nanoparticles. The method includes the steps of dropwise addition of silver nitrate solution to a carboxymethyl cellulose solution (1%) while stirring. The solution is subjected to ultrasonic irradiation for 30 minutes. The first indication of silver nanoparticles being synthesized can be change in the color of the solution to yellowish-brown after Ultrasonication. The solution can thereafter be subjected to microwave irradiations. After the predetermined duration, the produced silver nanoparticles can be separated from the solution. The nanoparticles can be washed and freeze dried.

Disclosed herein is a method comprising disposing a container containing a metal and/or ferromagnetic solid and abrasive particles in a static magnetic field; where the container is surrounded by an induction coil; activating the induction coil with an electrical current, to heat up the metallic or ferromagnetic solid to form a fluid; generating sonic energy to produce acoustic cavitation and abrasion between the abrasive particles and the container; and producing nanoparticles that comprise elements from the container, the metal and/or the ferromagnetic solid and the abrasive particles. Disclosed herein too is a composition comprising first metal or a first ceramic; and particles comprising carbides and/or nitrides dispersed therein. Disclosed herein too is a composition comprising nanoparticles comprising chromium carbide, iron carbide, nickel carbide, γ-Fe and magnesium nitride.

A method for checking a component to be produced in an additive manner, having the steps of mechanically exciting at least one additively constructed layer of the component during the additive production of the component, measuring a mechanical response signal of the component, and displaying a warning and/or interrupting the additive production of the component if the mechanical response signal lies outside of a specified tolerance range. A device for the additive production of a component, includes a device for mechanically exciting the at least one additively constructed layer of the component, a measuring unit for measuring the mechanical response signal of the component, and a control unit. The control unit is designed to display the warning and/or interrupt the additive production if the mechanical response signal lies outside of a specified tolerance range.

A method for checking a component to be produced in an additive manner, having the steps of mechanically exciting at least one additively constructed layer of the component during the additive production of the component, measuring a mechanical response signal of the component, and displaying a warning and/or interrupting the additive production of the component if the mechanical response signal lies outside of a specified tolerance range. A device for the additive production of a component, includes a device for mechanically exciting the at least one additively constructed layer of the component, a measuring unit for measuring the mechanical response signal of the component, and a control unit. The control unit is designed to display the warning and/or interrupt the additive production if the mechanical response signal lies outside of a specified tolerance range.

An additive manufacturing system configured to additively build an article can include an energy applicator, a build platform, and a powder nozzle configured to eject powder toward the build platform to be acted on by the energy applicator. The system can include a control module configured to control the energy applicator to create an amorphous structure forming at least a portion of the article.

An additive manufacturing system configured to additively build an article can include an energy applicator, a build platform, and a powder nozzle configured to eject powder toward the build platform to be acted on by the energy applicator. The system can include a control module configured to control the energy applicator to create an amorphous structure forming at least a portion of the article.

Methods and systems for producing feedstock powders, suitable for use in laser-based additive manufacturing, use laser ablation to vaporize a source material, which may be in bulk solid or solid coarse grain form. The source material is vaporized by a laser (or other focused energy source) in a vaporization chamber that is temperature controlled to provide a vertical thermal gradient. The vertical thermal gradient may be controlled to, in turn, control the nucleation, coagulation, and agglomeration of the vaporized molecules, enabling formation of microparticles that may then be used as feedstock powders in laser-based additive manufacturing. The produced feedstock powder particles may be of uniform composition, of uniform shape (e.g., substantially spherical), and of uniform phase or homogeneously-mixed phases.

Methods and systems for producing feedstock powders, suitable for use in laser-based additive manufacturing, use laser ablation to vaporize a source material, which may be in bulk solid or solid coarse grain form. The source material is vaporized by a laser (or other focused energy source) in a vaporization chamber that is temperature controlled to provide a vertical thermal gradient. The vertical thermal gradient may be controlled to, in turn, control the nucleation, coagulation, and agglomeration of the vaporized molecules, enabling formation of microparticles that may then be used as feedstock powders in laser-based additive manufacturing. The produced feedstock powder particles may be of uniform composition, of uniform shape (e.g., substantially spherical), and of uniform phase or homogeneously-mixed phases.