Permanent magnets and method of making the same are provided. The magnets include a magnetic layer having an insulation layer disposed thereon. The insulation layer is formed via additive manufacturing techniques such as laser melting such that that it has discrete phases including a magnetic phase and an insulating phase.

Components made of a metal matrix composite and methods for the manufacture thereof. The metal matrix composite contains TiB.sub.2 particles, Al.sub.3Ti particles, and particles of an intermetallic compound of aluminum and at least one rare earth element dispersed in an aluminum matrix. Methods include casting a first melt to produce an ingot, remelting the ingot to form a second melt, forming a powder from the second melt using an atomization process, and fabricating a component utilizing the powder in an additive manufacturing process. The ingot and the powder include an aluminum matrix that contains dispersions of TiB.sub.2 particles and Al.sub.3Ti particles.

Methods for manufacturing components that include casting a first melt to produce an ingot, remelting the ingot to form a second melt, forming a powder from the second melt using an atomization process, and fabricating a component utilizing the powder in an additive manufacturing process. The ingot and the powder include an aluminum matrix that contains dispersions of TiB.sub.2 particles and Al.sub.3Ti particles and the component is a metal matrix composite having an aluminum matrix that contains dispersions of TiB.sub.2 particles and Al.sub.3Ti particles. Optionally, the metal matrix composite may include particles of an intermetallic compound of aluminum and at least one alloying element.

A method of producing a sintered magnet is disclosed herein. In some embodiments, a method of producing a sintered magnet comprises, sintering a R—Fe—B based magnetic powder to produce a sintered magnet; wherein the R is Nd, Pr, Dy, Ce or Tb, and infiltrating a eutectic alloy into the sintered magnet, wherein the eutectic alloy contains Pr, Al, Cu and Ga, and wherein infiltration the eutectic alloy includes applying the eutectic alloy to the sintered magnet and heat-treating the sintered magnet to which the eutectic alloy is applied.

A method for producing a sintered R-T-B based magnet includes: preparing a sintered R-T-B based magnet work (R is a rare-earth element; and T is at least one selected from the group consisting of Fe, Co, Al, Mn and Si, and contains Fe with no exception); preparing an RL-RH-B-M based alloy; and a diffusion step of performing heat treatment while at least a portion of the RL-RH-B-M based alloy is attached to at least a portion of a surface of the sintered R-T-B based magnet work. In the RL-RH-B-M based alloy, the content of RL is 50 mass % or higher and 95 mass % or lower, the content of RH is 45 mass % or lower (including 0 mass %), the content of B is 0.1 mass % or higher and 3.0 mass % is lower; and the content of M is 4 mass % or higher and 49.9 mass % or lower.

A method for preparing a magnesium-based hydrogen storage material, includes: a Mg—Ce—Ni family amorphous alloy is prepared by a rapid cooling process; the amorphous alloy is pulverized, so as to obtain a amorphous powder; the amorphous alloy is activated, so as to obtain a MgH.sub.2—Mg.sub.2NiH.sub.4—CeH.sub.2.73 family nanocrystalline composite; the abovementioned composite is carried out a hydrogen absorption and desorption cycle, then the composite is placed in a pure Ar atmosphere for passivation, finally, the passivated composite is oxidized, so as to obtain a MgH.sub.2—Mg.sub.2NiH.sub.4—CeH.sub.2.73—CeO.sub.2 family nanocrystalline composite.

A step of, while a powder of an RLM alloy (where RL is Nd and/or Pr; M is one or more elements selected from among Cu, Fe, Ga, Co, Ni and Al) which is produced through atomization and a powder of an RH compound (where RH is Dy and/or Tb) are present on the surface of a sintered R-T-B based magnet, performing a heat treatment at a sintering temperature of the sintered R-T-B based magnet or lower is included. The RLM alloy contains RL in an amount of 65 at % or more, and the melting point of the RLM alloy is equal to or less than the temperature of the heat treatment. The heat treatment is performed while the RLM alloy powder and the RH compound powder are present on the surface of the sintered R-T-B based magnet at a mass ratio of RLM alloy:RH compound=9.6:0.4 to 5:5.

The present invention relates to a method for preparing a neodymium-iron-boron rare-earth permanent magnetic material, in particular to a hot press molding-based method for preparing a rare-earth permanent magnet. The problem that the residual magnetism and coercive force of a rare-earth permanent magnet prepared in the prior art cannot be both high is solved. An RTM alloy infiltrates same during an HD treatment. RTM sticks to the surface of coarse powder and infiltrates into the interior of the coarse powder along a grain boundary. The temperature of hot press sintering is relatively low, and grains barely grow. In the absence of Dy and Tb, a higher coercive force is obtained. If an alloy containing Dy and Tb is used for infiltration, these atoms diffuse into the surface layer of a main phase during preheating and heat treatment, achieving grain boundary hardening. Under the premise of a very small reduction in the residual magnetism, the coercive force is greatly improved.

A permanent magnet includes a rare earth element R; a transition metal element T; and B. The permanent magnet includes Nd as R. The permanent magnet includes Fe as T. The permanent magnet contains main phase grains and R-rich phases. The main phase grains include R, T, and B. The R-rich phases include R. The main phase grains observed in a cross section of the permanent magnet are flat. The cross section is parallel to an easy magnetization axis direction of the permanent magnet. Each of the R-rich phases is located between the main phase grains. An average value of intervals between the R-rich phases in a direction substantially perpendicular to the easy magnetization axis direction is from 30 μm to 1,000 μm. An average value of lengths of short axes of the main phase grains observed in the cross section is from 20 nm to 200 nm.

The disclosure refers to a preparation method for NdFeB permanent magnet including:

a) Preparing main alloy flakes consisting of (Pr.sub.2Nd.sub.8).sub.xFe.sub.100-x-y-zB.sub.yM.sub.z,where M is at least one of Al,Co,Cu,Ga,Ti and Zr, 28.5 wt. % ≤x≤31.0 wt. %,0.85 wt. %≤y≤0.98 wt. % and 0.5 wt. %≤z≤5.0 wt. %;

b) Preparing auxiliary alloy flakes consisting of L.sub.uFe.sub.100-u-v-wB.sub.vM.sub.w,where L is at least one ofPr and Nd,M is at least one of Al,Co,Cu,Ga,Ti and Zr, 35.0 wt. %≤u≤45.0 wt. %,0 wt. %≤v≤5.0 wt. % and 2.0 wt. %≤w≤10.0 wt. %;

c) Mixing the main alloy flakes and the auxiliary alloy flakes in predetermined rate, then performing hydrogen decrepitation to produce alloy pieces,and then crushing the alloy pieces to alloy powder by jet milling;

d) Preparing a powder mixture including the alloy powder and added heavy rare earth powder consisting of at least one of Dy and Tb;

e) Pressing the powder mixture to a green compact while applying a magnetic field, and thermal treatment of the green compact in a vacuum furnace to obtain the NdFeB permanent magnet.