B29K2001/08

METHOD FOR PRODUCING LYOCELL STAPLE FIBERS
20220275537 · 2022-09-01 ·

The invention relates to a method for the production of lyocell staple fibers, comprising the steps in the following order: a) extruding filaments from a solution of cellulose in an organic solvent; b) precipitating the cellulose for the formation of continuous cellulose filaments; c) washing the cellulose filaments; d) contacting the cellulose filaments with a crosslinking agent; e) reacting the cellulose filaments with the crosslinking agent in a reaction chamber; f) washing the treated cellulose filaments; g) cutting the washed cellulose filaments into staple fibers; h) forming a nonwoven fleece from the staple fibers and pressing the nonwoven fleece; and i) finishing the nonwoven fleece and pressing the nonwoven fleece.

Use of molar mass controlled cellulose

According to an example aspect of the present invention, there is provided a use of molar mass controlled cellulose in injection molding, extrusion and three dimensional printing applications.

Apparatus and method for realizing a web of fibrous material
11390994 · 2022-07-19 ·

An apparatus for producing a web of fibrous material includes a roll having incisions with a depth of 0.01-2.00 mm, a width of 0.01-2.00 mm, and a pitch 0.01-10.00 mm, and rotated at a peripheral velocity v.sub.1 equal to the velocity of an upstream apparatus unit; a belt stretched between transmission rollers that advances at a velocity v.sub.2 less than v.sub.1, wherein v.sub.1/v.sub.2 lies between 1.05 and 1.40; a presser roller rotating at a peripheral velocity v.sub.2, associated with a presser system acting to press the belt against the metal roll with a pressure of 1-200 kg per centimeter; and a system that feeds a sheet of pliable fibrous material between the belt and the roll, the belt having a longitudinal elongation of no more than 5%, dimensional stability along its entire length, a thickness of 1-10 cm, and a hardness 24-70° Shore A.

Compositions and resulting hard capsules comprising hydrophilic coloring foodstuff concentrates

An aqueous composition for making dip-molded comestible hard capsules comprising a film forming capsule base material and one or more colorants each consisting of a hydrophilic coloring foodstuff concentrate.

Cellulose filament process

The present invention provides a process for the viable production of lyocell cellulose continuous filament yarns.

EXTRUDED TUBULAR FILMS AND PROCESSES FOR MANUFACTURING TUBULAR FILMS
20220212390 · 2022-07-07 ·

A process for manufacturing a tubular film such as an edible casing film or a packaging film. The process includes the steps of providing a preblended powder composition containing a polymer matrix, a plasticizer, and water; feeding the preblended powder composition to an extruder; heating the preblended powder composition to a temperature above 100 degrees Celsius for a sufficient time to fully hydrate the polymer matrix and to convert the powder composition to a flowable mass; and extruding the flowable mass through a tubular die of the extruder to form the tubular film. The tubular film comprises: about 40-75 wt % polymer matrix; about 10-35 wt % plasticizer; and about 10-35 wt % water. The polymer matrix component is fully hydrated under the temperature, pressure and shear conditions inside the extruder, and may have a component which is only fully hydrated at temperatures above about 100 degrees Celsius.

HYDROXYPROPYL METHYL CELLULOSE ACETATE SUCCINATE, METHOD FOR PRODUCING THE SAME, AND COMPOSITION FOR HOT-MELT EXTRUSION
20220106410 · 2022-04-07 ·

There is provided a method for efficiently produce hydroxypropyl methyl cellulose acetate succinate (HPMCAS) having excellent flowability, where acetic acid in a reaction product mixture subjected to a wash and recovery step can be reduced. More specifically, there is provided a method for producing HPMCAS including an esterification step of esterifying hydroxypropyl methyl cellulose (HPMC) with acetic anhydride and succinic anhydride in acetic acid as a solvent to obtain a reaction product solution containing HPMCAS; a water addition step of adding water to the reaction product solution to obtain a water-added reaction product solution; an acetic acid removal step of removing at least a portion of both the solvent acetic acid and acetic acid derived from the acetic anhydride from the water-added reaction product solution to obtain a mixture having an acetic acid content reduced; and a wash and recovery step of washing the mixture and recovering the HPMCAS.

Gastric retentive devices

Provided are devices that are configured for gastric retention for a period of at least six hours (or at least three hours if the subject is in the fasted state) while maintaining their structural integrity and releasing or holding an active or diagnostic agent into or in gastric fluid of a human subject over that period, as well as methods of delivering an agent over an extended period by orally administering such devices to a subject, uses of an enteric polymer in the formation of devices that deliver an agent over an extended period of time, and methods of making such devices.

CELLULOSE DERIVATIVE BASED BIODEGRADABLE SUPPORT STRUCTURES FOR 3D PRINTING
20210317328 · 2021-10-14 ·

The present disclosure relates to support structures for three dimensional (3D) printing, methods of preparing the support structures, and methods of using the support structures. In particular, the support structures comprise a hydrogel comprised of a cellulose derivative. Preferably, the support structures are biodegradable and easily removed without generating toxic waste.

Aqueous composition comprising dispersed esterified cellulose ether

An aqueous composition which is useful for producing coatings and capsule shells comprises a) dispersed particles of an esterified cellulose ether comprising (i) groups of the formula —C(O)—R—COOA or (ii) a combination of aliphatic monovalent acyl groups and groups of the formula —C(O)—R—COOA, wherein R is a divalent hydrocarbon group and A is hydrogen or a cation, and the total degree of ester substitution is more than 0.70, and b) an esterified cellulose ether comprising aliphatic monovalent acyl groups and groups of the formula —C(O)—R—COOH, R being a divalent hydrocarbon group, wherein I) the degree of neutralization of the groups —C(O)—R—COOH is not more than 0.4, II) the total degree of ester substitution is from 0.03 to 0.70, and III) the esterified cellulose ether b) has a solubility in water of at least 2.0 weight percent at 2° C.