A thermal distillation apparatus including evaporation surfaces that are wetted with a solution, and from which at least some of the volatile solvent contained in the solution evaporates, condensers having an external surface in close proximity to, but not touching, a corresponding one of the one or more evaporation surfaces, and on which vapors of the solvent condense, releasing thermal energy that heats a flow of the solution moving upward within the condensers, spacers that prevent contact between the evaporating surfaces and the condensers, wherein spaces between the evaporating surfaces and the condensers are filled with a gaseous mixture composed of solvent vapor and one or more non-condensable gases, and except for diffusion of the solvent vapor relative to the non-condensable gases, the gaseous mixture is stationary.

A thermal distillation apparatus including evaporation surfaces that are wetted with a solution, and from which at least some of the volatile solvent contained in the solution evaporates, condensers having an external surface in close proximity to, but not touching, a corresponding one of the one or more evaporation surfaces, and on which vapors of the solvent condense, releasing thermal energy that heats a flow of the solution moving upward within the condensers, spacers that prevent contact between the evaporating surfaces and the condensers, wherein spaces between the evaporating surfaces and the condensers are filled with a gaseous mixture composed of solvent vapor and one or more non-condensable gases, and except for diffusion of the solvent vapor relative to the non-condensable gases, the gaseous mixture is stationary.

Improvements in grain alcohol distillation plants by incorporating a novel internal arrangement in the wort column and the rectifying column with distributors and accumulators inside thereof, achieving a stable and safe process in wide ranges of operation, guaranteeing the productivity of the plant and the quality of the products. The wort column features detachable perforated plates, easy to access and clean through manholes. By having easily detachable plates and, also, a manhole for each plate with “holder” type connections, the access to the interior of the column for cleaning and maintenance purposes is facilitated. The rectifying column is a special filling column with flow distributors, it has an intermediate alcohol accumulator and a condenser which is an integral part of the column that prevents the use of pumps. The arrangement of distributors and accumulators within the rectifying column favors the operational stability of the plant, allowing a low scale equipment to work similarly to an industrial scale column. The improvements include an integrated automation system with Internet communication for self-management of the plant with remote monitoring and autonomous operation.

Improvements in grain alcohol distillation plants by incorporating a novel internal arrangement in the wort column and the rectifying column with distributors and accumulators inside thereof, achieving a stable and safe process in wide ranges of operation, guaranteeing the productivity of the plant and the quality of the products. The wort column features detachable perforated plates, easy to access and clean through manholes. By having easily detachable plates and, also, a manhole for each plate with “holder” type connections, the access to the interior of the column for cleaning and maintenance purposes is facilitated. The rectifying column is a special filling column with flow distributors, it has an intermediate alcohol accumulator and a condenser which is an integral part of the column that prevents the use of pumps. The arrangement of distributors and accumulators within the rectifying column favors the operational stability of the plant, allowing a low scale equipment to work similarly to an industrial scale column. The improvements include an integrated automation system with Internet communication for self-management of the plant with remote monitoring and autonomous operation.

A distillation apparatus has a cooling spiral surrounding at least a part of a vertical extent of a fraction collector in the disclosed technology. Connecting to and/or extending into an interior space of the fraction collector is an end of a vertically-extending passageway. This passageway is functionally connected at an other end to a lower-end entry portal. An outer cover substantially covers the cooling spiral, fraction collector, and a portion of the vertically-extending passageway, excepting for a top portal, a side exit portal, at least one cooling spiral intake, and at least one cooling spiral outtake.

A distillation apparatus has a cooling spiral surrounding at least a part of a vertical extent of a fraction collector in the disclosed technology. Connecting to and/or extending into an interior space of the fraction collector is an end of a vertically-extending passageway. This passageway is functionally connected at an other end to a lower-end entry portal. An outer cover substantially covers the cooling spiral, fraction collector, and a portion of the vertically-extending passageway, excepting for a top portal, a side exit portal, at least one cooling spiral intake, and at least one cooling spiral outtake.

A short path evaporator including a heatable double-walled evaporator pipe having an inner interspace, with a rotatable rotor system disposed within the evaporator pipe and with a condenser disposed centrally in the evaporator pipe, and with an inlet for a product leading into the evaporator pipe, an outlet for a concentrate of the product leading out of the evaporator pipe, and an outlet for distillate accumulating at the condenser, and an inlet and an outlet for supplying and discharging heating medium to or from the interspace of the evaporator pipe, wherein the evaporator pipe is formed by an outer pipe and an inner pipe which, leaving the interspace, is disposed within the outer pipe, which are fixed at their ends in a sealing manner between two flange plates clamped together, wherein an inlet channel for the inlet of the product and an outlet channel for the outlet of the concentrate, which communicate with the interior of the inner pipe, are formed in the flange plates, as well as inlet and outlet channels for supplying and discharging the heating medium, which communicate with the interspace.

A short path evaporator including a heatable double-walled evaporator pipe having an inner interspace, with a rotatable rotor system disposed within the evaporator pipe and with a condenser disposed centrally in the evaporator pipe, and with an inlet for a product leading into the evaporator pipe, an outlet for a concentrate of the product leading out of the evaporator pipe, and an outlet for distillate accumulating at the condenser, and an inlet and an outlet for supplying and discharging heating medium to or from the interspace of the evaporator pipe, wherein the evaporator pipe is formed by an outer pipe and an inner pipe which, leaving the interspace, is disposed within the outer pipe, which are fixed at their ends in a sealing manner between two flange plates clamped together, wherein an inlet channel for the inlet of the product and an outlet channel for the outlet of the concentrate, which communicate with the interior of the inner pipe, are formed in the flange plates, as well as inlet and outlet channels for supplying and discharging the heating medium, which communicate with the interspace.

The present invention relates to a process for reducing the content of MOSH and/or MOAH from a vegetable oil selected from the group consisting of palm-based oil, cocoa butter-based oil and any mixtures thereof, and wherein the process is comprising the step of subjecting a vegetable oil to a short-path evaporation, wherein the short-path evaporation is performed at a pressure of below 1 mbar, at an evaporator temperature in a range of from 235 and 290° C., and with a feed rate per unit area of evaporator surface of the short-path evaporation equipment in a range from 35 to 102 kg/h.Math.m.sup.2, and thus obtaining a retentate vegetable oil. Present invention further relates to use of short-path evaporation for reducing content of MOSH and/or MOAH from vegetable oil.

The present invention relates to a process for reducing the content of MOSH and/or MOAH from a vegetable oil selected from the group consisting of palm-based oil, cocoa butter-based oil and any mixtures thereof, and wherein the process is comprising the step of subjecting a vegetable oil to a short-path evaporation, wherein the short-path evaporation is performed at a pressure of below 1 mbar, at an evaporator temperature in a range of from 235 and 290° C., and with a feed rate per unit area of evaporator surface of the short-path evaporation equipment in a range from 35 to 102 kg/h.Math.m.sup.2, and thus obtaining a retentate vegetable oil. Present invention further relates to use of short-path evaporation for reducing content of MOSH and/or MOAH from vegetable oil.