A purification module configured to separate and purify a liquid solution is provided. The purification module may include a vessel configured to receive a predetermined amount of a liquid solution. The purification module may also include a heating apparatus configured to apply heat to the vessel at a temperature of a first boiling point, and a column apparatus configured to separate the liquid solution into a first liquid and a second liquid and purify the first liquid and the second liquid to a determined purity level. The column apparatus may include a first heating chamber, a second heating chamber, and a distillation chamber. The distillation chamber may be located between the first heating chamber and the second heating chamber. The first heating chamber and second heating chamber may be configured to receive a heat transfer liquid to apply heat to the distillation chamber at the temperature of the first boiling point.

A purification module configured to separate and purify a liquid solution is provided. The purification module may include a vessel configured to receive a predetermined amount of a liquid solution. The purification module may also include a heating apparatus configured to apply heat to the vessel at a temperature of a first boiling point, and a column apparatus configured to separate the liquid solution into a first liquid and a second liquid and purify the first liquid and the second liquid to a determined purity level. The column apparatus may include a first heating chamber, a second heating chamber, and a distillation chamber. The distillation chamber may be located between the first heating chamber and the second heating chamber. The first heating chamber and second heating chamber may be configured to receive a heat transfer liquid to apply heat to the distillation chamber at the temperature of the first boiling point.

A purification module configured to separate and purify a liquid solution is provided. The purification module may include a vessel configured to receive a predetermined amount of a liquid solution. The purification module may also include a heating apparatus configured to apply heat to the vessel at a temperature of a first boiling point, and a column apparatus configured to separate the liquid solution into a first liquid and a second liquid and purify the first liquid and the second liquid to a determined purity level. The column apparatus may include a first heating chamber, a second heating chamber, and a distillation chamber. The distillation chamber may be located between the first heating chamber and the second heating chamber. The first heating chamber and second heating chamber may be configured to receive a heat transfer liquid to apply heat to the distillation chamber at the temperature of the first boiling point.

A distillation apparatus has a cooling spiral surrounding at least a part of a vertical extent of a fraction collector in the disclosed technology. Connecting to and/or extending into an interior space of the fraction collector is an end of a vertically-extending passageway. This passageway is functionally connected at an other end to a lower-end entry portal. An outer cover substantially covers the cooling spiral, fraction collector, and a portion of the vertically-extending passageway, excepting for a top portal, a side exit portal, at least one cooling spiral intake, and at least one cooling spiral outtake.

A distillation apparatus has a cooling spiral surrounding at least a part of a vertical extent of a fraction collector in the disclosed technology. Connecting to and/or extending into an interior space of the fraction collector is an end of a vertically-extending passageway. This passageway is functionally connected at an other end to a lower-end entry portal. An outer cover substantially covers the cooling spiral, fraction collector, and a portion of the vertically-extending passageway, excepting for a top portal, a side exit portal, at least one cooling spiral intake, and at least one cooling spiral outtake.

In an improved method of distilling fluids, some or all of the fluid is recovered as distillate and the fluid is situated in the shell side of a first shell and tube heat exchanger. The fluid to be recovered as distillate is successively boiled, demisted, compressed and then introduced into upper ends of the tubes. A second shell and tube heat exchanger is located below the first heat exchanger, and distillate from upper ends of the tubes in the second heat exchanger are arranged to receive distillate liquid and/or vapor from the lower ends of tubes of the first heat exchanger. The fluid is located in the shell of the second heat exchanger and that fluid is heated but is not boiled. A mechanism is provided to supply at least some of the heated fluid to the shell of the first heat exchanger.

In an improved method of distilling fluids, some or all of the fluid is recovered as distillate and the fluid is situated in the shell side of a first shell and tube heat exchanger. The fluid to be recovered as distillate is successively boiled, demisted, compressed and then introduced into upper ends of the tubes. A second shell and tube heat exchanger is located below the first heat exchanger, and distillate from upper ends of the tubes in the second heat exchanger are arranged to receive distillate liquid and/or vapor from the lower ends of tubes of the first heat exchanger. The fluid is located in the shell of the second heat exchanger and that fluid is heated but is not boiled. A mechanism is provided to supply at least some of the heated fluid to the shell of the first heat exchanger.

A device for the thermal treatment of material comprises a housing having a heatable housing jacket, which surrounds a treatment chamber and forms a rotationally symmetrical treatment surface extending in an axial direction, and a drivable rotor, which is arranged in the treatment chamber and extends coaxially. The rotor comprises a shaft, arranged in a manner distributed over the circumference of which are spreading elements. The device also comprises a condensation space, in which a condenser is formed and into which gaseous material components escaping from the material during the thermal treatment can pass, a condensate outlet for discharging the material components condensed in the condensation space, and a vacuum connection, which is fluidically connected to the condensation space. The vacuum connection is arranged in a region of the housing that lies downstream of the treatment surface, as viewed in the transport direction of the material.

A device for the thermal treatment of material comprises a housing having a heatable housing jacket, which surrounds a treatment chamber and forms a rotationally symmetrical treatment surface extending in an axial direction, and a drivable rotor, which is arranged in the treatment chamber and extends coaxially. The rotor comprises a shaft, arranged in a manner distributed over the circumference of which are spreading elements. The device also comprises a condensation space, in which a condenser is formed and into which gaseous material components escaping from the material during the thermal treatment can pass, a condensate outlet for discharging the material components condensed in the condensation space, and a vacuum connection, which is fluidically connected to the condensation space. The vacuum connection is arranged in a region of the housing that lies downstream of the treatment surface, as viewed in the transport direction of the material.

The present invention describes chemical processes for making optically-clear, taste-masked, shelf-stable nano-emulsions containing essentially pure cannabinoids and other nutraceuticals.