A method of and system for making at least four types of animal feed products for various types of animals to maximize and use all of the components found in the whole stillage in an alcohol producing plant. The method includes liquefying, fermenting, distilling, performing a selective particle size separating into three streams, wherein the three streams contain a first stream of a large particle stream that is used to form a first animal feed suitable for ruminant animals, a second stream of a coarse protein stream that is used to form a second animal feed suitable for chicken and pigs, and a third stream of a fine particle stream that is used to form a third animal feed suitable for fish and pet. The third stream is further concentrated and enriched to have a syrup with 35%-80% of dry solid.

A dehydration system energy recycling system (17) and method whereby latent heat energy is transferred from a high proof vapor produced by a dehydration element (16) into a lower proof feed mixture received into the dehydration element. The high proof vapor is first compressed (48) downstream of a dehydration apparatus (18) to increase its saturation temperature, and is then condensed to release latent heat energy. The latent heat energy is used to heat the lower proof feed mixture upstream of the dehydration apparatus. A grain-to-alcohol plant incorporating the dehydration system energy recycling system requires little or no virgin boiler steam to drive the dehydration system, while an associated evaporation element (24) of the plant can be driven by heat energy captured in a dryer exhaust energy recycling (DEER) system (40).

Disclosed herein are methods for the recovery of target bio-based products using a sorption-based technology with a mixed elution solvent optimized for minimized downstream distillation energy input.

Disclosed is a process to produce a purified vapor comprising dialkyl-furan-2,5-dicarboxylate (DAFD). Furan-2,5-dicarboxylic acid (FDCA) and an alcohol in an esterification zone to generate a crude diester stream containing dialkyl furan dicarboxylate (DAFD), unreacted alcohol, 5-(alkoxycarbonyl)furan-2-carboxylic acid (ACFC), and alkyl furan-2-carboxylate (AFC). The esterification zone comprises at least one reactor that has been previously used in an DMT process.

We have discovered that addition of water to a mixture of oxygenates increases their volatility relative to methanol. A process and apparatus are disclosed for separating methanol from other oxygenates. Water is separated from a stream comprising water, methanol and at least one other oxygenate to provide a water rich stream and a methanol and oxygenate rich stream. The methanol and oxygenate rich stream and water are fed to a column to provide an oxygenate rich stream and a methanol and water extract stream. The methanol and water can then be readily separated from each other.

A process of isolating 1,4-butanediol (1,4-BDO) from a fermentation broth includes separating a liquid fraction enriched in 1,4-BDO from a solid fraction comprising cells, removing water from said liquid fraction, removing salts from said liquid fraction, and purifying 1,4-BDO. A process for producing 1,4-BDO includes culturing a 1,4-BDO-producing microorganism in a fermentor for a sufficient period of time to produce 1,4-BDO. The 1,4-BDO-producing microorganism includes a microorganism having a 1,4-BDO pathway having one or more exogenous genes encoding a 1,4-BDO pathway enzyme and/or one or more gene disruptions. The process for producing 1,4-BDO further includes isolating 1,4-BDO.

A process of purifying 1,4-butanediol (1,4-BDO) from a fermentation broth including separating solid materials, salts and water, and subjecting the resulting material to a two, three or four column distillation system, that can include a wiped film evaporator to produce a purified 1,4-butanediol.

Energy efficiency is improved in a grain alcohol production plant (60) by capturing heat energy that otherwise would be lost to the environment when stillage evaporator last effect vapors (22) are condensed to recycle their water content. The low temperature/pressure heat energy of these vapors is efficiently recovered and reused by placing the vapors in direct physical contact (301, 402) with a working fluid (38) to form heated working fluid (54, 66), then using the heated working fluid directly in a process of the plant. In an embodiment, cook water used for the plant fermentation process is preheated by direct contact with stillage evaporator overhead vapor via one or more direct contact heat exchangers (301, 401) and/or a thermocompressor (402).

The present disclosure provides processes and systems for ethanol production. In one embodiment, a first beer column receives a first portion of a feed mixture including ethanol and water to form a first beer column bottom stream and a first beer column vaporous overhead stream. A beer column receives a second portion of the feed mixture. A first portion of the first beer column bottom stream is forwarded to a first beer column reboiler. A second portion of the first beer column bottom stream is forwarded to a plurality of evaporators. A condensed portion of the first beer column vaporous overhead stream is forwarded to a stripper column. The stripper column forms a feed stream, which is contacted with a separation system, thereby forming a permeate and a retentate. The permeate is forwarded directly to at least one selected from the first beer column and the stripper column.

A method is disclosed for improving the energy efficiency of biorefinery drying operations through integration of a dryer that utilizes the heat of condensation of process vapors to dry material whose emissions are captured with energy recovery. The dryer separates clean process vapors (e.g., ethanol) and steam from vapors containing volatile organic compounds and entrained materials, to minimize the need for vapor cleanup. An indirect dryer condenses vapors in a tube dryer similar to a steam tube dryer, but utilizing compressed process vapors, transferring the heat to wet material undergoing drying. The resulting exhaust vapors are either directed to a process stage that requires heat (e.g., distillation) and minimizes the need for vapor cleanup or to an out-of-contact heat exchanger that produces vapors for process use, or to another dryer as an additional effect. Mechanical-vapor recompression or thermal-vapor recompression are employed to produce vapors that optimize overall energy recovery.