A device for the thermal treatment of material comprises a housing having a heatable housing jacket, which surrounds a treatment chamber and forms a rotationally symmetrical treatment surface extending in an axial direction, and a drivable rotor, which is arranged in the treatment chamber and extends coaxially. The rotor comprises a shaft, arranged in a manner distributed over the circumference of which are spreading elements. The device also comprises a condensation space, in which a condenser is formed and into which gaseous material components escaping from the material during the thermal treatment can pass, a condensate outlet for discharging the material components condensed in the condensation space, and a vacuum connection, which is fluidically connected to the condensation space. The vacuum connection is arranged in a region of the housing that lies downstream of the treatment surface, as viewed in the transport direction of the material.

The present invention relates to a rotary evaporator (1) comprising an evaporator flask (10) and a heating bath (20), wherein the evaporator flask (10) can be dipped into the heating bath (20), further comprising a dipping control device (40) for controlling the dipping depth of the evaporator flask (10) into the heating bath (20), wherein the dipping control device (40) is set up to determine the level (25) of the heating bath (20) and wherein the dipping control device (40) is set up to control the dipping depth of the evaporator flask (10) into the heating bath (20) in dependence on the level (25) of the heating bath (20).

Herein, a cleaning device for a rotary evaporator (2) is provided. The rotary evaporator (2) comprises at least a rotatably arranged rotary flask (4) for receiving a substance to be evaporated and a condenser (5) for condensing the evaporated substance during operation of the rotary evaporator (2). The cleaning device (1) comprises at least a supply line (16, 16) for supplying a cleaning agent, a cleaning agent supply (13) for storing the cleaning agent and a pressure generating means (15) for generating a pressure in the cleaning agent in order to supply a pressurized cleaning agent from the cleaning agent supply (13) through the supply line (16, 16) to the rotary flask (4) and/or to the condenser (5).

In a system for performing a multi-step process for selectively purifying various pharmacologically-relevant components of a source plant such as cannabis, an initial step of the process provides a low-temperature, robust process for dehydrating and decarboxylating the starting productfresh raw cannabisby means of a vacuum-assisted microwave distillation process. An important by-product of the dehydration/decarboxylation is a terpene-rich distillate. By doing the terpene capture under vacuum, distillation temperature may be kept low. The low distillation temperature maximizes yields of thermally-sensitive components such as terpenes and cannabinoids.

Provided herein are integrated distillation apparatuses configured as stand-alone fully integrated systems having a reduced footprint. Integrated distillation apparatuses can have a rotary evaporator, a condenser, and an integrated refrigeration system or chiller, as well as an integrated water bath and vacuum pump, all of which can be integrated into a central frame and/or housing assembly. Integrated distillation apparatuses can be configured such that the rotary evaporator is movably attached to a frame structure and configured to be vertically translatable in position, whereas the condenser can be affixed to the structure by an arm extending from the structure and adjacent to the rotary evaporator, and wherein the refrigeration system can be in fluid communication with the condenser.

Methods and apparatus consistent with the present disclosure may provide electrical energy and thermal to extraction or separation equipment. Methods and apparatus consistent with the present disclosure may extract and concentrate essential elements plant matter. An amount of wasted heat energy collected from a engine that powers an electrical generator may be provided to an evaporation or separation process when electrical power is provided to extraction or separation processing equipment. Computers or electronics that control equipment consistent with the present disclosure may be remotely controlled via a mobile electronic device, when desired. Such computers or electronics may receive sensor data related to the operation of plat matter extractors, related separation equipment, or other equipment may be used to manage a production line. As such, methods and apparatus consistent with the present disclosure may extract essential elements from cannabis plant matter and process those essential elements into cannabis extracts or isolates.

The present invention discloses a methanol-mediated method for separating an alkaline solution of hemicellulose, and an ethanol-mediated method for separating an alkaline solution of hemicellulose, where methanol/ethanol is added into the alkaline solution in which hemicellulose is dissolved, and stirred thoroughly until the mixture is homogeneous, to destroy the hydrated layer effect formed between the hemicellulose and the alkaline solution through the methanol/ethanol-mediated hydrophobic effect, such that hemicellulose is precipitated from the solution system, and then the mixture is subjected to separation by sedimentation, centrifugation or filtration to obtain a precipitate of hemicellulose and an alkaline solution of methanol/ethanol; and by using the prompting effect of an alkaline condition on evaporation and gasification separation of methanol/ethanol from water, a reduced-pressure distillation (rectification) or gasification membrane is used to separate methanol/ethanol from the alkaline solution, and the obtained alkaline solution and methanol/ethanol are reused for dissolution and separation of hemicellulose. By the complete reuse of the alkaline solution and methanol/ethanol in the method of the present invention, it achieves efficient, clean and economical production of alkaline dissolution and separation of hemicellulose, and the separation and recovery efficiency of the hemicellulose dissolved in the alkaline exceeds 99%.

A rotary evaporator for evaporating a substance contained in an initial substance comprises an evaporation flask (2) for receiving the initial substance, a device (3) for heating the substance, a condenser (4) for condensing the vaporized substance, a collection container (6) for receiving the re-liquefied substance and at least one device (5) for generating a low pressure and/or an excess pressure. In order to remove the re-liquefied substance an excess pressure can be generated at least within the collection container (6) and/or in order to remove residues of the initial substance an excess pressure can be generated at least within the evaporation flask (2).

Methods and apparatus consistent with the present disclosure may provide electrical energy and thermal to extraction or separation equipment. Methods and apparatus consistent with the present disclosure may extract and concentrate essential elements plant matter. An amount of wasted heat energy collected from a engine that powers an electrical generator may be provided to an evaporation or separation process when electrical power is provided to extraction or separation processing equipment. Computers or electronics that control equipment consistent with the present disclosure may be remotely controlled via a mobile electronic device, when desired. Such computers or electronics may receive sensor data related to the operation of plat matter extractors, related separation equipment, or other equipment may be used to manage a production line. As such, methods and apparatus consistent with the present disclosure may extract essential elements from cannabis plant matter and process those essential elements into cannabis extracts or isolates.

The present invention provides a rotary evaporator capable of accurately quantifying concentrated liquid and/or distillate. A distillation flask is improved into a structure having a liquid discharge opening formed at the bottom, and/or a spherical collecting flask is improved into a structure having a liquid release opening formed at the bottom. Concentrated liquid and/or distillate can be discharged without dismounting the distillation flask and/or the collecting flask. In addition, fine metering scale tubes and quantitative capacity increase units are disposed at the liquid discharge opening and/or the liquid release opening, there is a valve on the top and another valve on the bottom of each tube, so that the constant subtle changes of the amount of concentrated liquid and/or distillate can be observed, and an accurate amount of concentrated liquid and/or distillate can be discharged.