An apparatus and process doubles the number of trays in a single fractionation column. A dividing wall is used to isolate a first side from a second side and fractionation on trays on each side is independent of the other. A transition vapor stream is ducted from a top of a first side to the bottom of the second side, and a transition liquid stream is ducted from a bottom of the second side to the top of the first side.

A method for phytochemical extraction includes providing a distillation vessel, providing a mixture of solvent and plant extract to the distillation vessel, placing the distillation vessel on a heat source, coupling the distillation vessel with a collector configured to collect condensed solvent, selecting an initial distillation temperature and outputting heat from the heat source at a heat source initial target temperature to heat the distillation vessel to a distillation vessel initial target temperature and boil the mixture in the distillation vessel at the initial distillation temperature and at an initial heat flux. With a vacuum pump, a distillation vessel initial target pressure is set within the distillation vessel.

A method and apparatus are presented for reducing the methanol content in a fermented solution to create forms healthier to human consumption, thereby reducing headaches and hangovers. In accordance with the disclosed embodiments, the fermented solution is placed in a vacuum vessel and heated to a fixed temperature. Pulling a fixed vacuum within the vessel lowers the boiling point of the solution, creating a vapor selectively of the low-end congeners, for example, methanol. The methanol-rich vapor is condensed and disposed leaving a healthier fermented solution with reduced methanol content. In some embodiments, the fixed temperature is lower than or equal to 32 degrees C. which preserves the aroma and taste of the fermented solution.

A vapor compression distillation assembly for distilling influent liquid, the vapor compression distillation assembly comprising a housing defining an interior and having an inlet for influent liquid, an evaporator and a condenser provided within the housing interior, an outlet for distillate, and at least one compressor fluidly coupled with the housing interior.

A method for phytochemical extraction includes providing a distillation vessel, providing a mixture of solvent and plant extract to the distillation vessel, placing the distillation vessel on a heat source, coupling the distillation vessel with a collector configured to collect condensed solvent, selecting an initial distillation temperature and outputting heat from the heat source at a heat source initial target temperature to heat the distillation vessel to a distillation vessel initial target temperature and boil the mixture in the distillation vessel at the initial distillation temperature and at an initial heat flux. With a vacuum pump, a distillation vessel initial target pressure is set within the distillation vessel.

A plant oil extraction system is disclosed utilizing a novel dual vapor recovery scheme and pressure differentials and valve timing conducive to continuous operation.

A method for producing hemp oil, comprising decarboxylation of CBDA in hemp oil; short-path evaporation of CBD from the decarboxylated hemp oil to produce CBD oil; selective THC to CBN conversion performed on the decarboxylated hemp oil.

The present invention relates to a method for producing anhydrosugar alcohol, and more particularly to a method of producing anhydrosugar alcohol using a solvent including at least two components that form an azeotrope with water at atmospheric pressure and that have significantly different boiling points. The method for producing anhydrosugar alcohol according to the present invention can increase the yield of anhydrosugar alcohol by efficiently controlling the reaction temperature by use of a solvent including at least two components that form an azeotrope with water at atmospheric pressure and that have significantly different boiling points.

A vacuum separator is used to separate a pitch stream from a slurry hydrocracking reactor upstream of the product fractionation column. The process and apparatus removes pitch from the product streams to enable easier separation of light VGO from heavy VGO in a fractionation column.

The present disclosure provides an apparatus and method for producing a policosanol having a specific chromatographic fingerprint. The apparatus of the present disclosure has a feed tank and receiving tanks which are connected to a vacuum system. The method of the present disclosure is carried out by a high vacuum rectification process and includes: firstly, feeding a saponified crude alkanol into a melting tank in which the material is melted and then flows into the feed tank, and then injecting the material into a rectifying still using a delivery pump, followed by first rectification under vacuum condition and sequential collection of fractions at different phases from the tower top and stillage residue from the tower bottom; and after the completion of the rectification of the first batch crude product, carrying out second feeding on the basis of consistent vacuum in the feed tank and the rectifying tower.