B01D3/106

RAPID BOTANICAL OIL DISTILLATION DEVICE UTILIZING MICROWAVE AGENT
20210284928 · 2021-09-16 ·

Various aspects of the disclosure relate to methods and systems for extracting plant oil from plant material. A system may comprise a microwave emitter, an extraction chamber, and a cooling chamber. Microwave radiation emitted by the microwave emitter may dielectrically heat a microwave absorbing agent, which may heat the plant oil of the plant material. Plant oil of the plant material may be volatized in the extraction chamber and may be directed into the cooling chamber to be condensed.

Method of distilling dimethyl sulfoxide and multistage distillation tower

A method of distilling a liquid containing dimethyl sulfoxide using a distillation system, including mixing sodium carbonate with a liquid containing dimethyl sulfoxide at a bottom of the distillation system such that sodium carbonate accounts for 0.005% to 25% by weight relative to 100% by weight of the liquid containing dimethyl sulfoxide and sodium carbonate in total at the bottom of the distillation system and heating the bottom; and obtaining a distillate containing dimethyl sulfoxide at a position lower than a position at which the liquid containing dimethyl sulfoxide is introduced and higher than a position of the heating portion.

Rapid botanical oil distillation device utilizing microwave agent
11021674 · 2021-06-01 · ·

Various aspects of the disclosure relate to methods and systems for extracting plant oil from plant material. A system may comprise a microwave emitter, an extraction chamber, and a cooling chamber. Microwave radiation emitted by the microwave emitter may dielectrically heat a microwave absorbing agent, which may heat the plant oil of the plant material. Plant oil of the plant material may be volatized in the extraction chamber and may be directed into the cooling chamber to be condensed.

Vacuum distillation apparatus and methods
11027215 · 2021-06-08 ·

Vacuum distillation apparatus and methods are provided. In an embodiment, an apparatus is provided that includes an evaporation chamber having a bottom flow rate control (FRC) surface that is curved to provide multiple flow rates to a solution as it flows across the bottom surface. The apparatus also includes a wiper that is curved to match the curve of the bottom FRC surface and wipes the bottom FRC surface to distribute the solution. A heater heats the bottom FRC surface to evaporate one or more components from the moving solution.

METHOD FOR RECOVERING CO2 IN THE RECTISOL PROCESS AND RECOVERY SYSTEM

A method for recovering CO.sub.2 in the Rectisol process. The method includes at least the following steps: performing reduced-pressure flash distillation treatment on the CO.sub.2-rich methanol liquid, and outputing the CO.sub.2 desorbed gas obtained after the reduced-pressure flash distillation treatment as a product gas; performing heat exchange flash distillation treatment on a first methanol treatment liquid obtained after the reduced-pressure flash distillation treatment, and outputing the CO.sub.2 desorbed gas obtained after the heat exchange flash distillation treatment as a product gas; performing vacuum flash distillation treatment on a second methanol treatment liquid obtained after the heat exchange flash distillation treatment, and outputing the CO.sub.2 desorbed gas obtained after the vacuum flash distillation treatment as a product gas. Reduced-pressure flash distillation treatment, heat exchange flash distillation treatment and vacuum flash distillation treatment are sequentially performed on the CO.sub.2-rich methanol liquid in this method.

System, Method and Apparatus for Cannabinoid Tincture Separation and Solvent Recovery
20210139448 · 2021-05-13 · ·

A system for processing cannabinoids and recovering solvent has a vessel for a mixture of cannabinoids and solvent. A pump forms a vacuum in the system to draw the mixture into a first heat exchanger to pre-heat the mixture. A falling film evaporator receives the mixture from the first heat exchanger, and boils the mixture to form a solvent vapor. The falling film evaporator collects the cannabinoids from the mixture as a crude oil. The first heat exchanger receives the solvent vapor. Heat is transferred to incoming mixture of the system, and cools and condenses the solvent vapor to form solvent condensate and vapor. A second heat exchanger receives and further cools the solvent condensate and vapor to form further condensed solvent and some solvent vapor. The pump receives the further condensed solvent and some solvent vapor and increases pressure to form solvent liquid and recovers solvent liquid for reuse.

METHOD AND APPARATUS FOR EFFECTIVE PREPARATION OF TRIFLUOROAMINE OXIDE

The present invention relates to a preparation method of trifluoroamine oxide which comprises the steps of producing an intermediate product by reacting nitrogen trifluoride and nitrous oxide in the presence of a reaction catalyst wherein the unreacted gas containing nitrogen (N.sub.2) produced in the course of the reaction is removed and instead nitrogen trifluoride and nitrous oxide are injected additionally; and producing trifluoroamine oxide by reacting the intermediate product with sodium fluoride.

Molten salt system and method and apparatus of transformation for multi-carbon production by using the same

This invention relates to a novel molten salt system in chemical transformation of saccharides and a method as well as an apparatus for multi carbon production by the molten salt system. It is found that an eutectic molten salt composition is advantageous for multi-carbon productions through chemical transformation under mild conditions. This invention further provides a method and an apparatus for preparing 5-hydroxymethylfurfural (HMF) and HMF-derived chemicals from saccharides by the said molten salt system.

APPARATUS AND METHOD FOR A DRILL MUD PLANT

A remediation plant for remediating drilling mud, cuttings, and fluids. The preferred plant includes a reboiler that is adapted to provide heat to the drilling mud, cuttings, and fluid, a mud drum that is operatively connected to the reboiler, a distillation column that is operatively connected to the reboiler, a heat exchanger that is operatively connected to the reboiler, a condenser that is operatively connected to the distillation column, a condenser tank that is operatively connected to the condenser, an oil-water separator that is operatively connected to the condenser tank, and a pump that is operatively connected to the oil-water separator. The preferred remediation plant is adapted to remove synthetic drilling fluid from drilling mud, cuttings, and fluids. A method for remediating drilling mud, cuttings, and fluid.

System, method and apparatus for cannabinoid mixture separation and solvent recovery
10899728 · 2021-01-26 · ·

A system for processing cannabinoids and recovering solvent has a vessel for a mixture of cannabinoids and solvent. A pump forms a vacuum in the system to draw the mixture into a first heat exchanger to pre-heat the mixture. A falling film evaporator receives the mixture from the first heat exchanger, and boils the mixture to form a solvent vapor. The falling film evaporator collects the cannabinoids from the mixture as a crude oil. The first heat exchanger receives the solvent vapor. Heat is transferred to incoming mixture of the system, and cools and condenses the solvent vapor to form solvent condensate and vapor. A second heat exchanger receives and further cools the solvent condensate and vapor to form further condensed solvent and some solvent vapor. The pump receives the further condensed solvent and some solvent vapor and increases pressure to form solvent liquid and recovers solvent liquid for reuse.