In an improved method of distilling fluids, some or all of the fluid is recovered as distillate and the fluid is situated in the shell side of a first shell and tube heat exchanger. The fluid to be recovered as distillate is successively boiled, demisted, compressed and then introduced into upper ends of the tubes. A second shell and tube heat exchanger is located below the first heat exchanger, and distillate from upper ends of the tubes in the second heat exchanger are arranged to receive distillate liquid and/or vapor from the lower ends of tubes of the first heat exchanger. The fluid is located in the shell of the second heat exchanger and that fluid is heated but is not boiled. A mechanism is provided to supply at least some of the heated fluid to the shell of the first heat exchanger.

A device for the thermal treatment of material comprises a housing having a heatable housing jacket, which surrounds a treatment chamber and forms a rotationally symmetrical treatment surface extending in an axial direction, and a drivable rotor, which is arranged in the treatment chamber and extends coaxially. The rotor comprises a shaft, arranged in a manner distributed over the circumference of which are spreading elements. The device also comprises a condensation space, in which a condenser is formed and into which gaseous material components escaping from the material during the thermal treatment can pass, a condensate outlet for discharging the material components condensed in the condensation space, and a vacuum connection, which is fluidically connected to the condensation space. The vacuum connection is arranged in a region of the housing that lies downstream of the treatment surface, as viewed in the transport direction of the material.

The present disclosure relates to a process for preparing polymers using a plug flow reactor. The process includes providing an aqueous monomer solution comprising amide monomers; evaporating the aqueous monomer solution to form a concentrated monomer solution; and polymerizing the concentrated monomer solution in a plug flow reactor comprising a shell side and a tube side to form a first process fluid comprising polymers. The concentrated monomer solution flows on the shell side from the inlet to the outlet.

In a system for performing a multi-step process for selectively purifying various pharmacologically-relevant components of a source plant such as cannabis, an initial step of the process provides a low-temperature, robust process for dehydrating and decarboxylating the starting productfresh raw cannabisby means of a vacuum-assisted microwave distillation process. An important by-product of the dehydration/decarboxylation is a terpene-rich distillate. By doing the terpene capture under vacuum, distillation temperature may be kept low. The low distillation temperature maximizes yields of thermally-sensitive components such as terpenes and cannabinoids.

A heat and mass transfer system configured to be a passive system using gravitational force to form a thin liquid film flow on an outer surface of a flow distribution head and downstream conduit member to subject the thin liquid film to heat transfer mediums. The at least partially spherical flow distribution head creates a uniform thin flow of liquid on the outer surface increasing the efficiency of the heat and mass transfer system. The heat and mass transfer system may include a heat transfer medium supply system in fluid communication with internal aspects of the downstream conduit such that a heat transfer medium flows within the downstream conduit while the liquid film flows on the outer surface of the downstream conduit. Rather than conventional sheet flow on inner surfaces of a conduit, the flow distribution head enables sheet flow to be formed on an outside surface of a component.

A distillation apparatus has a cooling jacket, in the shape of a halo, surrounding at least a part of a vertical extent of a fraction collector in the disclosed technology. Connecting to and/or extending into an interior space of the fraction collector is an end of a vertically-extending passageway. This passageway is functionally connected at an other end to a lower-end entry portal. An outer cover substantially covers the cooling jacket, fraction collector, and a portion of the vertically-extending passageway, excepting for a top portal, a side exit portal, at least one cooling jacket intake, and at least one cooling jacket outtake.

Described are a high pressure carbamate condenser, urea plant, and urea production process. The high pressure carbamate condenser as described is of the shell-and-tube heat exchanger type with a tube bundle and has a redistribution chamber connected to tubes of the tube bundle and to a duct. The duct extends between the redistribution chamber and the shell.

A system for brine water desalinization includes a first heat exchanger having an inlet plenum and an outlet plenum for a first fluid comprising a concentrate in a liquid. The first heat exchanger includes a shell side fluid inlet and a shell side fluid outlet for a second fluid comprising a higher concentrated liquid than the first fluid. The system also comprises pipes configured to direct the first fluid from the outlet plenum to a shell side fluid inlet of a second heat exchanger and to direct the second fluid from the shell side fluid outlet to an inlet plenum of the second heat exchanger. The system further includes pipes configured to produce desalinized water by a serial distillation of multiple steams from an nth number of heat exchangers into respective distillates thereof and a parallel product of brine waste thereof from the heat exchangers.

A distillation apparatus has a cooling jacket, in the shape of a halo, surrounding at least a part of a vertical extent of a fraction collector in the disclosed technology. Connecting to and/or extending into an interior space of the fraction collector is an end of a vertically-extending passageway. This passageway is functionally connected at an other end to a lower-end entry portal. An outer cover substantially covers the cooling jacket, fraction collector, and a portion of the vertically-extending passageway, excepting for a top portal, a side exit portal, at least one cooling jacket intake, and at least one cooling jacket outtake.

A heat and mass transfer system configured to be a passive system using gravitational force to form a thin liquid film flow on an outer surface of a flow distribution head and downstream conduit member to subject the thin liquid film to heat transfer mediums. The at least partially spherical flow distribution head creates a uniform thin flow of liquid on the outer surface increasing the efficiency of the heat and mass transfer system. The heat and mass transfer system may include a heat transfer medium supply system in fluid communication with internal aspects of the downstream conduit such that a heat transfer medium flows within the downstream conduit while the liquid film flows on the outer surface of the downstream conduit. Rather than conventional sheet flow on inner surfaces of a conduit, the flow distribution head enables sheet flow to be formed on an outside surface of a component.