Methods for extracting and recovering bioactive components from a biomass feedstock with pressurized aqueous solvent solutions comprising one or more organic solutes and/or one or more inorganic solutes. The methods comprise the steps of: (i) preparing a selected aqueous solvent solution for pressurizing; (ii) providing a flow of the prepared aqueous solvent solution to a plant biomass feedstock contained within a pressure-resistant temperature-controllable reactor vessel (iii) warming the flow of aqueous solvent solution and the contents of the reactor vessel to a selected temperature; (iv) pressurizing the flow of the aqueous solvent solution and the contents of the reactor vessel to a selected pressure; (v) controllably flowing the pressurized aqueous solvent solution through the reactor vessel while maintaining the contents of the reactor vessel at the selected pressure; and (vi) collecting a flow of the pressurized aqueous solvent solution egressing from the reactor vessel for a selected period of time.

An apparatus for extraction and recovery of components from biomass feedstocks with pressurized low polarity water. The apparatus is configured with four or more reaction columns, wherein each column is in separate communication with a supply of hot water, a first supply of pressurized heated water, a second supply of pressurized heated water, and a supply of pressurized cooling water. Components may be extracted concurrently from two or more batches of the biomass by, first placing the two batches of biomass into two selected columns, separately flooding the two columns with pressurized water, heating the columns and their contents to the point where the water becomes pressurized low polarity (PLP) water, recovering the PLP water comprising the extracted components from the two selected columns, cooling the columns with PLP water, and removing the spent biomass material from the columns.

A plant oil extraction system may include a reservoir tank, an agitator tank, a filtration system, a boiler tank, a condenser unit, and a vacuum chamber. The reservoir tank may hold a solvent to be used in the system process. The solvent may be deposited into the reservoir tank through a fill port. A pump may transfers the solvent from the reservoir tank to the agitator tank. The agitator tank may hold dry plant matter. The agitator tank may separate oil from the plant matter by use of solvent where the mixture of solvent and plant oil drains to the boiler tank through a filter system. The boiler tank comprise of a tank stack (condenser) used for separating extracted plant oil from the solvent by boiling off the solvent and a vacuum pump used to extract residual solvent from the extracted plant oil and generally purge the extracted plant oil.

An extraction, reaction, and purification apparatus that comprises an entire unit designed to react, extract, purify, and isolate compounds and individual analyte from one or more source material(s), which are contacted with a process fluid to form an absolute, the unwanted components are then further removed in a sequence of steps, using separation chambers, until a sufficient purified extract is obtained. The apparatus further comprises a high-speed solvent separation unit to evaporate the solvent from the extract. There are two methods for using different solvent/sequences to obtain between 90-99% pure extracted and purified material. The process also includes bioconversion of waste products, making it a waste free, environmentally friendly system.

The present invention provides a solid phase extraction method using a micro device having a dam forming portion including a dam, the solid phase extraction method comprising the steps of: (i) injecting a solvent and a filler into the micro device, moving the solvent to the dam forming portion, the dam allowing the solvent to flow therethrough and preventing the filler from passing therethrough, and adsorbing a material to be separated onto the filler in the dam forming portion; and (ii) extracting, from the filler, the adsorbed material, wherein the micro device is rotated with respect to a central axis during one of steps (i) and (ii), and the rotation of the micro device is performed at an angular velocity defined by equation 1.

In embodiments, a packing material for supported liquid extraction has a sorbent media that includes synthetic silica particles. In embodiments, the synthetic silica particles can have physical properties relating to one or more of particle surface area, shape, size, or porosity. In one embodiment, synthetic silica particles have a surface area less than about 30 m.sup.2/g. In another embodiment, the synthetic silica particles have an approximately uniform particle shape. In further examples, synthetic silica particles have a particle size in a range of about 30-150 m inclusive or greater than about 200 m. In another embodiment, synthetic silica particles are arranged to have a pore size greater than about 500 Angstroms. In an embodiment, an apparatus for supported liquid extraction includes a container and a sorbent media that includes synthetic silica particles. In a further embodiment, a method for extracting target analytes through supported liquid extraction is provided.

A portable supercritical fluid extraction apparatus, comprising: (i) a pressure vessel for generating a supercritical fluid therein; (ii) a liquid solvent supply tank; (iii) a means for interconnecting said pressure vessel and said liquid solvent supply tank at a predetermined angle for delivery therethrough of a liquid solvent from the liquid storage tank to the pressure vessel; and (iv) a heating component for heating contents of the pressure vessel to produce a supercritical fluid therein. The apparatus may additionally comprise a sample in fluid communication with the pressure vessel, and a receiving vessel in fluid communication with the pressure vessel. The pressure vessel may have a heating means for heating fluid contents therein, for example a heating wrap, a heating block, or a heating jacket.

Continuous extraction units (CEUs) are constructed that allow switching of extraction chambers (ECs) that contain extractable material (EM) and extract solution. Extraction chambers can be removable and replaceable, where the CEU has a fluid flow portion and a liquid transfer portion. Quick-connect valves allow exchange of ECs in the CEU while under flow without solvent loss. Alternatively, the CEU employs pairs of ECs where a first EC at equilibrium partitioning of an extract solution drains to an expansion chamber (EXC) with an expansion valve (EV) and a heat transfer tube situated proximal to or shared with a solvent condenser (SC) to form of a double phase change heat exchanger (HE). Solvent from the SC fills a paired EC containing EM. A second pair of ECs has a first EC with EM and solvent establishing equilibrium and a second EC that is emptied of spent EM, filled with fresh EM, and readied to receive solvent.

A system and method for extraction of cannabis oil from cannabis plant materials by further reducing the temperature of the extraction system effluent, which may be a mixture of solvent, the desired cannabinoids, and/or the undesired non-polar extracted waste from the plant material. This invention improves the extraction process by: 1) enhancing the rapid filtering of the waste material from the process stream, speeding up the overall process, and 2) improving the quality of the product, yielding a purer extract as evidenced, in part, by its lighter (yellow/gold) color as compared to less-pure green/brown extracts.

A method for extracting an analyte from a solid sample is described. The sample is sealed in a porous membrane bag, which is sonicated in an organic solvent. An extract of the analyte forms in the bag and diffuses into the organic solvent. The organic solvent containing the extract may then be concentrated and analyzed for an analyte with gas chromatography-mass spectrometry. The method does not the use of a solid sorbent material, and does not require a step of centrifuging or filtering.