The present invention relates to methods for treating cannabis biomass in order to isolate tetrahydrocannabinolic acid (THCA). In another aspect, the present invention relates to a process that involves purification followed by extraction of cannabis biomass to isolate and improve yields of high-purity crystalline extracts.

A Cannabis trichome separator. At least one storage vessels are provided, each vessel having an open top and adapted to receive a plant material and chilled or ice water mixture. A mechanism for agitating the mixture is also provided. Another mechanism raises, lowers, and pivots the agitating mechanism, so the agitating mechanism can be placed over the open top of each of the at least one storage vessels. The mixture can be agitated in each of the storage vessels, seriatim. Also disclosed is a method for processing raw plant material. A plant material and chilled or ice water is introduced into each of at least one storage vessels. The agitating mechanism agitates the mixture in a first of the storage vessels, pivoting the agitating mechanism from a first position to a second position, and agitating the mixture in subsequent storage vessels, seriatim.

A method of making CBD concentrate or CBD Isolate comprises (a) milling a raw material; (b) contacting the milled raw material with an extraction solvent and separating a solid waste material to form a filtered extract; (c) concentrating the filtered extract; (d) washing the concentrated extract to form an organic phase and an aqueous phase; (e) separating the aqueous phase from the organic phase to form a washed extract; (f) removing an organic solvent from the washed extract to form a concentrated washed extract; (g) decarboxylating the concentrated washed extract; (h) vacuum distilling the decarboxylated extract to form a distillate; (i) dewaxing the distillate to form a post-dewax filtrate; (j) applying a vacuum to the post-dewax filtrate to form a post-dewax concentrate; (k) degassing the post-dewax concentrate; and (l) vacuum distilling the degassed concentrate to form a CBD concentrate.

A method of producing an extract of an animal-derived or plant-derived biological material includes: extracting a component in the biological material using liquefied dimethyl ether for the biological material to obtain a liquefied dimethyl ether solution including the component; separating the solution from the biological material; and volatilizing or separating the liquefied dimethyl ether from the solution.

Methods of isolating phenols from phenol-containing media. The methods include combining a phospholipid-containing composition with the phenol-containing medium to generate a combined medium, incubating the combined medium to precipitate phenols in the combined medium and thereby form a phenol precipitate phase and a phenol-depleted phase, and separating the phenol precipitate phase and the phenol-depleted phase. The methods can further include extracting phenols from the separated phenol precipitate phase. The extracting can include mixing the separated phenol precipitate phase with an extraction solvent to solubilize in the extraction solvent at least a portion of the phenols originally present in the phenol precipitate phase.

A method for extracting compounds from plant material utilizing terpenes as a solvent is described. The invention includes the excitation of the plant material and terpene solvent with microwave, ultrasound, heat input, and physical agitation or combinations thereof. The invention particularly covers the process as it relates to the extraction of THC and CBD and their derivatives from cannabis and hemp for the use in products for medical and recreational use. The combinations of terpene saturant, plant material strain and process variables can be tuned in order to dial in the final resultant product for several variables including but not limited to terpene content, THC or CBD potency, ratios of THC or CBD and their derivatives, or flavor profile.

Provided is a multi-functional plugging agent for a coal mine and a preparation method thereof. The preparation method comprises: by taking Ecklonia Kurome Okam as a raw material, mixing an Ecklonia Kurome Okam suspension with phosphorus pentoxide for reaction, then performing biodegradation to obtain an Ecklonia Kurome Okam biological extract, adding urea for neutralization, mixing a neutralization product with an inorganic catalyst and melamine for reaction to obtain a bio-based plugging synergist solution, finally cooling the bio-based plugging synergist solution, and mixing the cooled bio-based plugging synergist solution with a certain amount of pentaerythritol and ammonium polyphosphate to obtain the multi-functional plugging agent for the coal mine based on the Ecklonia Kurome Okam biological extract. According to the invention, not only a coal crack can be effectively plugged for a long time, but also an efficient flame-retardant effect can be achieved in a complete period of coal spontaneous combustion.

A process of extracting bioactive compounds from one or more plant material is provided. The process includes agitation of one or more plant material in the presence of piperine and palmitoylethanolamide to produce a powder blend, supplying of a polar solvent to the powder blend and then adding a nonpolar solvent after at least 24 hours of infusion of the powder blend in the polar solvents to form a slurry. The slurry is further filtered to recover bioactive compounds in a liquid extract form.

The present invention provides for a method for obtaining an oil extract of cannabis. The method includes: (a) contacting cannabis biomass and an edible oil; (b) pressing between a pair of plates to provide spent cannabis and an oil extract of cannabis; and (c) separating the spent cannabis biomass and the oil extract of cannabis.

A method of isomerizing Δ9-tetrahydrocannabinol (“Δ9-THC”) to Δ10-tetrahydrocannabinol (“Δ10-THC”). The method includes the steps of: extracting Δ9-THC from cannabis biomass, which optionally contains one or more of the components found in fire retardant such as PHOS-CHEK®; dewaxing of crude extracts by winterization; pH-adjusting extracts by washing the extracts in heptane solution with aqueous solutions of: citric acid, sodium bicarbonate, and brine; isomerizing Δ9-THC to Δ10-THC by exposure to suitable conditions and in the presence of a catalyst based on the components of fire retardant; vacuum distillation of Δ10-THC at a predetermined temperature range and vacuum level; collecting the distillate and redistilling it up to three times to acquire distillate containing less than 60% Δ10-THC; and purification of the MO-THC to a purity of 99% or greater by crystallization from n-pentane solution.