B01D11/0292

Extraction of cannabinoids, curcuminoids and ginsenosides
10946307 · 2021-03-16 · ·

An example method for extracting phytochemical oil from plant parts includes freezing plant parts from at least one of Cannabis sativa, Curcuma longa, Panax ginseng, and Panax quinquefolius. The frozen plant parts are reduced to a plant powder, which is suspended in an aqueous buffer. The aqueous buffer containing the suspended plant powder is incubated with at least one pectinase and at least one cellulase. An aqueous phase of the incubated aqueous buffer is evaporated through steam heating to obtain a steam dried product. Phytochemical oil, which includes at least one of cannabinoids, curcuminoids, and ginsenosides, is extracted from the steam dried product.

CARBON DIOXIDE EXTRACTION PROCESSES, DEVICES, METHODS, AND SYSTEMS
20210069610 · 2021-03-11 · ·

A CO.sub.2 extraction process for cannabis sativa that uses liquid CO.sub.2 in combination with co-solvent admixtures to purify cannabis botanicals in high yield and purity. The extraction process allows for multiple extractions, or washes, to be performed with the same solvent CO.sub.2, which may be seamlessly recycled and purified between subsequent extraction cycles. A variety of in-line filtration vessels, pumps, vacuums, and controllable valves are used to yield a pure product while allowing a high level of user control over the process.

Solvent-based extraction methods
10946306 · 2021-03-16 · ·

Solvent-based methods for the extraction and concentration of cannabinoids and other target compounds from large-scale harvests of cannabis and hemp crops. Select portions of cannabis or hemp plants are harvested, ground to a desired particle size and ultimately powderized where the powder is mixed with a solvent, preferably ethanol or water, to form a slurry that is subjected to at least two, and preferably five or more separate inverting filter centrifugation steps until cannabinoid extraction is maximized. The filtrate from the first inverting centrifugation step is isolated and purified to derive an extract whereas the powderized filtride is subjected to further centrifugation steps. Fresh solvent is introduced at the last inverting centrifugation step and subsequently used upstream in sequentially-earlier centrifugation steps until ultimately utilized in a first inverting filter centrifugation step.

DYNAMIC INTERFACE SYSTEM AND ITS APPLICATION IN SUPERCRITICAL FLUID EXTRACTION AND CHROMATOGRAPHY

The present invention provides a dynamic interface system between an extraction device and a chromatographic purification device for separating and purifying substance(s) from a mixture or matrix. One embodiment is the Supercritical Fluid Interface (SFI) between Supercritical Fluid Extraction (SFE), and Supercritical Fluid Chromatography (SFC). The SFI is capable of interfacing; gas, subcritical and supercritical fluid extraction methods and pair with gas, subcritical and supercritical fluid chromatography technologies that operate within the pressure and temperature parameters of the SFI. The SFI can operate up to 200 degrees celsius and 5000 psi. This interface technology allows for an inline oil extraction and chromatographic separation, the SFI can pair extraction and chromatography with the same solvent in different mobile phases, whereas the extraction can be performed using CO.sub.2 as a solvent in sub-critical phase and the SFI can receive the subcritical solution and then increase pressure and/or temperature to achieve supercritical state as required for injection into supercritical fluid chromatography technologies. The SFI coupling between SFE and SFC can to extract and refine cannabinoids from the cannabis industrious, hemp, plant and can also be applied to improve efficiency in an industry that extracts and refines oils, through chromatography, from organic materials using a gas, or sub/supercritical fluid as a solvent and mobile phase.

Amphiphilic asphaltene ionic liquids as demulsifiers for heavy petroleum crude oil-water emulsions

Provided herein are amphiphilic asphaltene ionic liquids and methods of making and using the amphiphilic asphaltene ionic liquids, e.g. as demulsifiers for petroleum crude oil-water emulsions.

Method and Apparatus for Curing Plant-Based Extracts

Equipment and processes for curing and decarboxylating botanical oils, and in particular oils such as cannabidiol (CBD) and tetrahydrocannabinol (THC) from plants of the genus Cannabis (including both THC-lacking industrial hemp and THC-bearing varieties) are described. Lower temperatures, extended cure cycles and inert-gas processing improve product quality and reduce undesired oxidation, resulting in clear, homogenous oils with less tendency to crystallize.

Separation of copper and molybdenum sulfides from pyrite using a sea water/desalinated water hybrid process

A copper/molybdenum separation system uses sea water in the roughing circuit and desalinated water in cleaning circuit. In both roughing circuit and cleaning circuit, hydrophobic engineered media are used to recover the mineral particles of interest. The cleaning circuit includes a molybdenum loading stage configured to contact the conditioned pulp with the engineered media in an agitated reaction chamber, and load the hydrophobic molybdenite on the engineered media.

SYSTEM AND METHOD FOR EXTRACTING LIQUID AND SOLID HYDROCARBONS AND THEIR DERIVATIVES
20210207034 · 2021-07-08 · ·

A system and method for extracting liquid and solid hydrocarbons and their derivatives from natural and man-made hydrocarbon sources, including but not limited to oil sands, bitumen, asphalt, roofing shingles, and other hydrocarbon articles of manufacture. The hydrocarbon sources are prepared by dissolving, crushing and/or grinding. The prepared hydrocarbon sources are subjected to agitation where the solvent and hydrocarbon source as thoroughly mixed. The results of the agitation are then separated in one or both of a mesh screen shaker and a centrifuge. The mesh screen shaker subjects the materials to medium frequency oscillations. The centrifuge subjects the materials to high G-forces. The combined processes separate the hydrocarbons from solids and residual solids to less than 0.2% by weight.

Vapor trap
10898827 · 2021-01-26 ·

A method of capturing a vaporized component or components, and apparatus for same is provided. The method involves vaporization of desired components, and capture of the vaporized components in a material using a vapor trap device. Once captured, the material with the component stored therein may be used for any number of purposes including ingestion, topical administration, and/or aromatization.

Extracting Apparatus, and Extracting-Unit Manufacturing Method
20210016203 · 2021-01-21 ·

An extracting apparatus includes: a first phase transition section that causes a phase transition of an extraction solvent from a gas to a liquid; a second phase transition section that causes a phase transition of the extraction solvent from a liquid to a gas; a treatment tank that stores a treated material, and receives an inflow of the extraction solvent that has been liquefied in the first phase transition section; a first valve that is provided between the second phase transition section and the treatment tank; and a second valve that is provided between the first phase transition section and the treatment tank. The second phase transition section is connected with a recovery valve.