The present disclosure relates to an apparatus and a method for measuring miscibility in oil using back titration. The apparatus includes: a flocculation solution storage unit; a flow cell including a UV transmitting member; a dissolving agent storage unit; a UV irradiation unit; and a measurement unit, wherein: a flocculation solution is stored in the flocculation solution storage unit; the flocculation solution circulates between the flocculation solution storage unit and the flow cell; the measurement unit measures the UV transmittance of the flocculation solution while the dissolving agent in the dissolving agent storage unit is supplied to the flocculation solution storage unit; the miscibility in the oil is calculated from the amount of dissolving agent supplied and a change in the UV transmittance measured by the measurement unit; and the miscibility is calculated based on a time point when the slope of increase in the UV transmittance changes.

Separation device (1) includes bottomed casing (2), rotating body (3), and blade (4). Casing (2) includes outer tubular portion (5) and inner tubular portion (6). Rotating body (3) is disposed inside inner tubular portion (6) and rotates about a rotation axis along an axial direction of inner tubular portion (6). Blade (4) is disposed between inner tubular portion (6) and rotating body (3), and rotates together with rotating body (3). Inner tubular portion (6) includes inner inflow port (61) and discharge port (63). Discharge port (63) discharges a solid contained in a fluid flowing into an inside of inner tubular portion (6) through inner inflow port (61) between inner tubular portion (6) and outer tubular portion (5). Outer tubular portion (5) includes a fluid outflow port and a solid discharge portion. The fluid outflow port causes the fluid flowing out from the inside of inner tubular portion (6) and flowing into the inside of outer tubular portion (5) to flow out to the outside of outer tubular portion (5). The solid discharge portion discharges the solid discharged from discharge port (63) of inner tubular portion (6) to the outside of outer tubular portion (5).

A portable unit and associated processing are described for clarifying process water used in oil and gas operations such as fracking or drill-out operations. In the portable unit, dirty water (402) is introduced into a clarifier (400). The dirty water (402) is directed to a bottom of the clarifier (400) where dissolved air 408 from a dissolved air flotation pump (410) is injected into the water (402). The water (402) then passes across the inclined plates (412). Particles are separated from the water (402) via interaction with the plates (412) and directed to collectors (414), at the bottom of the clarifier (404), by gravitation. In addition, a floc, enhanced by the injection of the dissolved air (408), is skimmed from the water surface. The result of this process flow is clarified water (430) that can be returned to the frack and post-frack completion process.

A portable unit and associated processing are described for clarifying process water used in oil and gas operations such as fracking or drill-out operations. In the portable unit, dirty water (402) is introduced into a clarifier (400). The dirty water (402) is directed to a bottom of the clarifier (400) where dissolved air 408 from a dissolved air flotation pump (410) is injected into the water (402). The water (402) then passes across the inclined plates (412). Particles are separated from the water (402) via interaction with the plates (412) and directed to collectors (414), at the bottom of the clarifier (404), by gravitation. In addition, a floc, enhanced by the injection of the dissolved air (408), is skimmed from the water surface. The result of this process flow is clarified water (430) that can be returned to the frack and post-frack completion process.

Treating an organic effluent is disclosed. The effluent is fed in a continuous flow at a rate q via a first chamber maintained at a first pressure and/or directly through a first narrowing to a second chamber or container maintained at a second medium pressure by the injection of air into the second chamber at a rate Q in order to obtain an emulsion in the second chamber. A head loss is generated in the emulsion optionally modified by a second and/or third narrowing or a feed valve for a third chamber maintained at a third pressure in the region immediately downstream of the second or third narrowing and/or valve. A flocculant is injected into the region of the third chamber. The emulsion at atmospheric pressure then being degasified and the emulsion thus degasified being recovered in a filtration or decanting device.

Treating an organic effluent is disclosed. The effluent is fed in a continuous flow at a rate q via a first chamber maintained at a first pressure and/or directly through a first narrowing to a second chamber or container maintained at a second medium pressure by the injection of air into the second chamber at a rate Q in order to obtain an emulsion in the second chamber. A head loss is generated in the emulsion optionally modified by a second and/or third narrowing or a feed valve for a third chamber maintained at a third pressure in the region immediately downstream of the second or third narrowing and/or valve. A flocculant is injected into the region of the third chamber. The emulsion at atmospheric pressure then being degasified and the emulsion thus degasified being recovered in a filtration or decanting device.

A feedwell design for a clarifier that may better dissipate the entrance energy of feed slurry liquid exiting the feedwell and entering the clarifier. Plates having a surface area twisted around a longitudinal axis may be provided at the bottom of the feedwell. The plates may cause a change in the flow direction of the feed, from being mostly horizontal to mostly vertical, to slow the slurry. The provision of plates at the bottom of a feedwell in a clarifier may advantageously reduce the velocity of the materials entering the clarifier, or may increase the uniformity of the flow rate of the materials while reducing or maintaining the amount of shear force, turbulence, or other forces that may have a detrimental effect on clarification. Likewise, this may improve the rate at which solids settle out of the feed slurry solution, and thus improve the clarity of the removed liquid.

An aim of the invention is to provide a bioreactor and a waste water treatment method that employs this tank, whereby anaerobic and aerobic microorganism treatment can be continuously carried out, even when the volume of the bioreactor is large, and whereby installation costs can be minimized. The invention comprises an outer tank (2), a cylindrical inner tank (3) disposed inside this outer tank and having openings above and below, a circulation rate control device (4) for controlling the circulation rate of water to be treated in the bioreactor, the circulation rate control device (4) being provided at an upper part of this cylindrical inner tank, a cylindrical control plate (5) for bringing about sedimentation of sludge, the cylindrical control plate (5) being provided at the outer circumference of an upper part of the cylindrical inner tank, a treated-water quality measurement device (6) that is provided outside and inside of the cylindrical inner tank, a waste water supply opening (10) that is provided in the circulation pathway of the water to be treated circulating through the outer tank and inner tank, a treated water discharge opening (11) that is provided in an upper part of the outer tank, and a sedimentation-solidification prevention device (12) for preventing sedimentation-solidification of sludge that has sedimented.

An aim of the invention is to provide a bioreactor and a waste water treatment method that employs this tank, whereby anaerobic and aerobic microorganism treatment can be continuously carried out, even when the volume of the bioreactor is large, and whereby installation costs can be minimized. The invention comprises an outer tank (2), a cylindrical inner tank (3) disposed inside this outer tank and having openings above and below, a circulation rate control device (4) for controlling the circulation rate of water to be treated in the bioreactor, the circulation rate control device (4) being provided at an upper part of this cylindrical inner tank, a cylindrical control plate (5) for bringing about sedimentation of sludge, the cylindrical control plate (5) being provided at the outer circumference of an upper part of the cylindrical inner tank, a treated-water quality measurement device (6) that is provided outside and inside of the cylindrical inner tank, a waste water supply opening (10) that is provided in the circulation pathway of the water to be treated circulating through the outer tank and inner tank, a treated water discharge opening (11) that is provided in an upper part of the outer tank, and a sedimentation-solidification prevention device (12) for preventing sedimentation-solidification of sludge that has sedimented.

Polymer flocculants are described comprising blends of high molecular weight polyethylene oxide and high molecular polyacrylamides. When introduced in desired amounts and with desired molecular weight ranges, excellent flocculation function is found that can be used to reduce polymer consumption to obtain a desired purity of clarified waste water. It has been found that the desirable polymer blends can be effectively added upstream from locations in which polyethylene oxide would generally be added so that the polymer blend can effectively mix with the slime flow to reduce or eliminate the need for excess polymer use to compensate for less effective mixing with the slime flow. Suitable waste treatment systems are described to provide for the delivery of the flocculants in the waste treatment process.