The invention relates to a solid-material method for producing calcium dipropionate in a pressure-resistant solid-state mixing reactor by charging calcium oxide, calcium hydroxide or calcium carbonate or mixtures of these calcium compounds, and adding propionic acid by a reaction directly in the solid phase under a pressure that is increased above normal pressure.

There is provided a method of producing microparticles using an emulsion based synthesis route including: Providing a first fluid phase and a second fluid phase, wherein the first fluid phase is a continuous phase and the second fluid phase is a dispersed phase comprising a dispersed material, wherein the continuous phase is immiscible with the dispersed phase; Mixing the first continuous phase and the second dispersed phase in the presence of a surfactant in a shear device to form an emulsion of droplets of controllable size and having a narrow drop size distribution; Drying the emulsion to form microparticles of controllable size and having narrow size distribution, and wherein the microparticles may comprise spherical, crumpled, dimpled, porous or hollow microparticles morphology. Also provided is a system including shear device and drying arrangement. Also provided are micro particles of controllable size and morphology formed by the method.

Disclosed is a mixed reactor and a method for preparing electrothermal film precursor solution based on the mixed reactor. The mixed reactor includes a reaction kettle body, a reflux condensation mechanism, and a multifunctional stirring mechanism. The reflux condensation mechanism includes a condensate tank, a condensing coil is wound around inside of the condensate tank, two ends of the condensing coil are horizontally arranged, and hermetically and rotatably installed on both sides of the condensate tank, the condensing coil is driven by a coil driving motor; the multifunctional stirring mechanism includes a stirring shaft and a plurality of stirring blades driven by the stirring shaft. The bottom of the stirring shaft is fixedly sleeved with an isolation sleeve. Buffer rubber gaskets are hermetically connected between the mounting parts and the installation holes. It can effectively improve the quality of products and the quality controllability during the product preparation process.