Patent classifications
B01J4/002
Process for preparing alkenylhalosilanes and reactor suitable therefor
Described is a method for producing alkenyl halosilanes by reacting alkenyl halide selected from the group comprising vinyl halide, vinylidene halide, and allyl halide with halosilane selected from the group comprising monohalosilane, dihalosilane, and trihalosilane in the gas phase in a reactor comprising a reaction tube (1) that has an inlet (2) at one end and an outlet (3) at the other end, said reactor further comprising an annular-gap nozzle (4) that is mounted on the inlet (2), extends into the reaction tube (1), and has a central supply duct (5) for one reactant (7) and a supply duct (6), which surrounds the central supply duct (5), for the other reactant (8). In order to carry out said method, alkenyl halide is injected into the reaction tube (1) through the central supply duct (5), halosilane is injected thereinto through the surrounding supply duct (6), and both substances flow through the reaction tube (1) in the direction of the outlet (3). The described method allows alkenyl halosilanes to be produced at a high yield and with great selectivity. The amount of soot formed is significantly lower than in conventional reactors. The invention also relates to a reactor for carrying out gas-phase reactions, said reactor being characterized by at least the following elements: A) a reaction tube (1) that has B) an inlet (2) at one end, C) an outlet (3) at the other end, and D) an annular-gap nozzle (4) which includes a central supply duct (5) for one reactant (7) and a supply duct (6), which surrounds the central supply duct (5), for another reactant (8), said nozzle being mounted on the inlet (2) and extending into the reaction tube (1).
Apparatus and methods for mixing reformable fuels and an oxygen-containing gas and/or steam
The present teachings provide apparatus and methods for mixing a reformable fuel and/or steam with an oxygen-containing gas and/or steam to provide a gaseous reforming reaction mixture suitable for reforming with a reformer and/or a fuel cell stack of a fuel cell unit and/or fuel cell system.
Mechanical system that continuously processes a combination of materials
The present application is directed towards systems and methods for continuously reacting a combination of materials by use of an acoustic agitator and a continuous process vessel. The system can react, fluidize, mix, coat, dry, combine or segregate materials. The continuous processing system can include an acoustic agitator capable of being removably coupled to a continuous process vessel. The continuous process vessel can include a first inlet for introducing at least one process ingredient, a plurality of plates configured for directing a flow of the at least one process ingredient through the continuous process vessel and capable of transferring acoustic energy generated by the acoustic agitator into the at least one process ingredient, an outlet for discharging a product of the at least one process ingredient, and a fastener for removable coupling the continuous process vessel to the acoustic agitator.
Reverse-phase polymerisation process
A reverse-phase suspension polymerization process for the manufacture of polymer beads comprising forming aqueous monomer beads comprising an aqueous solution of water-soluble ethylenically unsaturated monomer or monomer blend and polymerizing the monomer or monomer blend to form polymer beads while suspended in a non-aqueous liquid, and recovering polymer beads, in which the process comprises, providing in a vessel (1) a volume (2) of non-aqueous liquid wherein the volume of non-aqueous liquid extends between at least one polymer bead discharge point (3) and at least one monomer feed point (4), feeding the aqueous monomer or monomer blend through orifices (5) into, or onto, the non-aqueous liquid to form aqueous monomer beads, allowing the aqueous monomer beads to flow towards the polymer bead discharge point subjecting the aqueous monomer beads to polymerization conditions to initiate polymerization to form polymerizing beads, wherein the polymerizing beads have formed polymer beads when they reach the polymer bead discharge point, removing a suspension of the polymer beads in non-aqueous liquid from the vessel at the polymer bead discharge point and recovering water soluble or water swellable polymer beads from the suspension. The invention also relates to the apparatus suitable for carrying out a reverse-phase suspension polymerization and polymer beads obtainable by the process or employing the apparatus.
SYSTEMS AND METHODS FOR PROCESSING GASES
The invention includes a gas processing system for transforming a hydrocarbon-containing inflow gas into outflow gas products, where the system includes a gas delivery subsystem, a plasma reaction chamber, and a microwave subsystem, with the gas delivery subsystem in fluid communication with the plasma reaction chamber, so that the gas delivery subsystem directs the hydrocarbon-containing inflow gas into the plasma reaction chamber, and the microwave subsystem directs microwave energy into the plasma reaction chamber to energize the hydrocarbon-containing inflow gas, thereby forming a plasma in the plasma reaction chamber, which plasma effects the transformation of a hydrocarbon in the hydrocarbon-containing inflow gas into the outflow gas products, which comprise acetylene and hydrogen. The invention also includes methods for the use of the gas processing system.
METHOD FOR PREPARING AMMONIA BY USING AMMONIUM SALT AND SILICATE
Disclosed is a method for preparing ammonia gas through a reaction between an ammonium salt and a silicate. An aqueous solution of the ammonium salt in the form of atomized droplets is contacted with a silicate at a high temperature for a reaction to generate ammonia gas and a solid substance. The silicate can be solid particles, and forms a bed. The generated ammonia gas is collected, the solid substance is extracted, part of the same solid substance is mixed with a fresh silicate solid particle, and the mixture continuously reacts with the atomized droplets of the aqueous solution of the ammonium salt.
Method for producing graphene and new form of graphene
The invention provides a method for preparing graphene which method comprises the steps of: (a) forming a graphite/water mixture; and (b) introducing the graphite/water mixture into a cavitation reactor using at least two offset nozzles; a cavitation reactor for use in the method wherein the cavitation reactor has a cavitation chamber wherein the cavitation chamber has at least two offset inlet nozzles which are directed towards the centre of the cavitation chamber and at least one outlet; and graphene having a carbon content of at least about 98 wt %.
Method of Hydrocarbon Pyrolysis and Device for Implementing Same
A method of oxidative pyrolysis involves heating hydrocarbon feedstock, heating a steam-oxygen mixture, combusting hydrocarbon feedstock in vapors of a steam-oxygen mixture in a special reactor, rapidly cooling the obtained products of incomplete combustion of chemical reactions in two steps, after which the cooled steam-gas mixture is directed to the fractionation unit. A hydrocarbons pyrolysis device has a steam-oxygen mixture and feedstock mixing chamber, a pyrolysis chamber and a coking reactor, a device for heating hydrocarbon feedstock, a device for heating steam-oxygen mixture coupled to a mixing chamber, a coking reactor having a device for supplying coolant to the pyrogas flow, a separation unit coupled to the coking reactor, a fractionation unit with an additional coolant supply device. Disposal of heavy oil residues by rapid coking with high economic efficiency and environmental safely while obtaining high-quality coke and producing aromatic compounds occurs without construction or additional installations.
SYSTEM AND PROCESS WITH ASSISTED GAS FLOW INSIDE A REACTION CHAMBER
A processing system and method of producing a particulate material are provided. The processing system includes a system inlet connected to one or more gas lines to deliver one or more gases into the processing system, a buffer chamber, a dispersion chamber, a heating assembly, a reaction chamber and a system outlet for delivering particulate material out of the processing system. The method includes delivering one or more gases via a system inlet into a buffer chamber of a processing system, jetting a liquid mixture into one or more streams of droplets using one or more power jet modules into the processing system, delivering flows of one or more heated gases via a heating assembly, forming a reaction mixture and processing the reaction mixture at a reaction temperature into a product material inside the reaction chamber.
Taxane Particles and Their Use
Compositions are provided that include having at least 95% by weight of a taxane, or a pharmaceutically acceptable salt thereof, where the particles have a mean bulk density between about 0.050 g/cm.sup.3 and about 0.15 g/cm.sup.3, and/or a specific surface area (SSA) of at least 18 m.sup.2/g, 20 m.sup.2/g, 25 m.sup.2/g, 30 m.sup.2/g, 32 m.sup.2/g, 34 m.sup.2/g, or 35 m.sup.2/g. Methods for making and using such compositions are also provided.